Characterization of cellulose fibers in Thespesia populnea barks: Influence of alkali treatment.

Abstract

Natural fibers are emerging as best alternatives for synthetic materials in selective applications. These fibers may not have the required properties in its raw form and hence needs some alterations in its characteristics. Likely, this article reports enhancement in surface and structural properties of Thespesia populnea bark fiber treated with NaOH under various concentration and soaking period. Fibers treated with 5% NaOH for 60\u2009min yields noteworthy mechanical strength (678.41\u2009±\u200948.91\u2009MPa) owing to its relatively high cellulose fraction (76.42%). Fourier transform infrared spectra endorses the removal of non-cellulosic compounds and X-ray diffraction studies reveals 13.6% growth in the size of cellulose crystals on optimally treated fibers. Weibull distribution model statistically interprets the reliability of acquired tensile test results. Finally, microscopic examinations with scanning electron microscopy and atomic force microscopy explore that fiber surface turns rough after alkali treatment and makes it appropriate for reinforcement in polymer matrices.