A. Iadicicco

Thinned fiber Bragg gratings as high sensitivity refractive index sensor

In this work, the numerical and experimental analysis on the use of thinned fiber Bragg gratings as refractive index sensors have been carried out. Wet chemical etching in a buffered hydrofluoric acid solution was used for sensor fabrication. Experimental characterization for an almost full etched cladding sensor is presented demonstrating good agreement with numerical results and resolutions of /spl ap/10/sup -5/ and /spl ap/10/sup -4/ for outer refractive index around 1.45 and 1.333, respectively.

Mode transition in high refractive index coated long period gratings

In this work, the numerical and experimental investigation of the cladding modes re-organization in high refractive index (HRI) coated Long Period Gratings (LPGs) is reported. Moreover, the effects of the cladding modes re-organization on the sensitivity to the surrounding medium refractive index (SRI) have been outlined. When azimuthally symmetric nano-scale HRI coatings are deposited along LPGs devices, a significant modification of the cladding modes distribution occurs, depending on the layer features (refractive index and thickness) and on the SRI. In particular, if layer parameters are properly chosen, the transition of the lowest order cladding mode into an overlay mode occurs. As a consequence, a cladding modes re-organization can be observed leading to relevant improvements in the SRI sensitivity in terms of wavelength shift and amplitude variations of the LPGs attenuation bands.

High-sensitivity optical chemosensor based on coated long-period gratings for sub-ppm chemical detection in water

In this work, the use of fiber long-period gratings (LPGs)—coated with nanoscale overlays of Syndiotactic Polystyrene (sPS) in the nanoporous crystalline δ form as specific and highly sensitive chemical sensors for in water monitoring—is proposed. The approach presented here, combines the excellent sorption properties of δ form sPS as a chemosensitive layer with the excellent refractive index sensitivity of LPG-based sensors as ideal transducers. In particular, when overlays with a high refractive index compared with the cladding one are deposited along the grating region, as in this case, the refraction-reflection regime at the cladding-overlay interface occurs. As result of this mechanism, the attenuation bands of coated LPGs would respond to the optical changes induced in the sensitive overlay due to chemical sorption by a significant modification of the peak central wavelength and intensity. The sensitivity depends strongly on the overlay thickness and the grating coupled cladding mode. Here, sensor p...

Thinned fiber Bragg gratings as refractive index sensors

In this work, highly sensitive refractive index measurements have been experimentally demonstrated by using thinned fiber Bragg grating (FBG) sensors. When the cladding diameter is reduced, significant changes in the effective refractive index occur due to surrounding medium refractive index modifications, leading to Bragg wavelength shifts. Uniformly thinned FBGs have been obtained by using wet chemical etching in hydrofluoric acid solutions. In order to prove sensor sensitivity, experimental tests have been carried out by using glycerine solutions with well-known refractive indices. Obtained results agree well with the numerical analysis carried out by using the three-layer fiber model. If the cladding layer is completely removed, resolutions of /spl ap/10/sup -5/ and /spl ap/10/sup -4/ for the outer refractive index around 1.450 and 1.333, respectively, are possible. Finally, a novel approach based on the selective etching along the grating region has been analyzed, leading to high-sensitivity refractive index sensors based on intensity measurements.

Refractive index sensor based on microstructured fiber Bragg grating

In this work, an all-fiber high-resolution refractive index sensor based on a microstructured fiber Bragg grating is presented. The proposed structure relies on a partial and localized etching of the cladding layer along a standard grating. The main spectral changes of the structured grating are the increasing of the stopband and the formation of a narrow allowed band strongly dependent on the etching features and the surrounding refractive index. A sensor prototype has been fabricated by using wet etching and a proper masking procedure; experimental results reveal the possibility to carry out low-cost refractive index measurements with a resolution of 4/spl middot/10/sup -5/.

Cladding mode reorganization in high-refractive-index-coated long-period gratings : effects on the refractive-index sensitivity

We theoretically and experimentally investigated the reorganization of cladding modes in high-refractive-index- (HRI-) coated long-period gratings (LPGs), focusing on the influence of refractive-index sensitivity. When azimuthally symmetric nanoscale HRI coatings are deposited along LPG devices, a significant modification of the distribution of cladding modes occurs, depending on the layers features (refractive index and thickness) and on the external refractive index. In particular, if these parameters are properly chosen, a transition between cladding modes and overlay modes occurs. Numerical and experimental effects of the mode transition on the sensitivity of the surrounding refractive index are described.

Coated long-period fiber gratings as high-sensitivity optochemical sensors

In this paper, the numerical and the experimental analyses of coated long-period fiber gratings (LPFGs) as a high-sensitivity optochemical sensor are presented. The proposed structure relies on LPFGs coated with nanoscale high refractive index chemical-sensitive overlays. The deposition of overlays with refractive index higher than the cladding one leads to a modification of the cladding-mode distribution. If the overlay features are properly chosen, a strong field enhancement within the overlay occurs, leading to an excellent sensitivity of the cladding-mode distribution to the coating properties. The effects of overlay thickness and cladding-mode order on sensor performances have been numerically and experimentally investigated. In order to provide a high-sensitivity and species-specific optochemical sensor, this mechanism has been proved with nanoscale overlays of syndiotactic polystyrene (sPS) in the nanoporous crystalline /spl delta/ form. The sensitive material has been chosen in light of its selectivity and high sorption properties towards chlorinated and aromatic compounds. Sensor probes were prepared by using dip-coating technique and an adequate procedure to obtain the /spl delta/-form sPS. Experimental demonstration of the sensor capability to perform subparts-per-million detection of chloroform in water at room temperature is also reported.

Optical chemo-sensor based on long period gratings coated with /spl delta/ form syndiotactic polystyrene

In this work, a long period grating (LPG) is coated with a thin film of syndiotactic polystyrene (sPS) in the nanoporous crystalline /spl delta/ form in order to obtain a species-specific chemical sensor. The combination of the intrinsic and high refractive index sensitivity of the LPGs with the high sorption properties toward chlorinated and aromatic compounds of sPS /spl delta/ form allows detecting very low concentrations (in the range of few parts per million) of chloroform in water. Chemical detection is carried out by measuring the wavelength shift and the amplitude changes in the attenuation band of the LPG due to analyte sorption.

Nonuniform thinned fiber Bragg gratings for simultaneous refractive index and temperature measurements

In this work, a novel method for simultaneous measurements of temperature and refractive index employing fiber Bragg gratings is presented. The principle of operation relies on the use of a single nonuniform thinned grating, where the cladding layer is partially or completely removed only in a part of the grating. The perturbation leads to a wavelength-splitting of the spectral response of the unperturbed structure in two separate peaks. The first one, corresponding to the thinned region, is sensitive to the local temperature and the surrounding refractive index changes, while the other one, related to the unperturbed part, would respond only to thermal changes. Here, wet chemical etching in a buffered hydrofluoric acid solution was used for sensor fabrication. Experimental characterization of the sensitivities to the external refractive index and temperature, varying in the range 1.33-1.45 and 15/spl deg/C-50/spl deg/C, respectively, is presented for a 7.6-/spl mu/m etched cladding sensor. The same approach can be efficiently used as key element for the development of sensors array for chemical sensing in practical applications.

Sensitivity characteristics in nanosized coated long period gratings

This work presents an experimental analysis of the sensitivity characteristics to the surrounding refractive index (SRI) in long period gratings coated with polymeric overlay with high refractive index and thickness values ranging in hundreds of nanometers. The presence of the coating induces the cladding to overlay mode transition depending on the overlay features and the SRI. The immediate consequence is a drastic modification of the sensitivity characteristics from the sublinear monotone behavior to a resonantlike shape. Here, the sensitivity characteristics of coated long period gratings have been investigated to outline their dependence on the overlay thickness and order mode.