Aline Cristina Mendes de Farias

Characterization of waste of soda-lime glass generated from lapping process to reuse as filler in composite materials as thermal insulation

The beneficiation plate process by soda-lime glass lapping in the glass industry generates, an untapped residue (waste). The waste of this material is sent to landfills, causing impact on the environment. This work aimed to characterize and evaluate the waste of soda-lime glass (GP) lapping. After its acquisition, the GP was processed by grinding and sieving and further characterized by the chemical/mineralogical analysis (XRF, EDS and XRD), SEM morphology, particle size by laser diffraction, thermogravimetric analyses (TGA and DSC) and thermophysical analyses. It was observed that the GP particles are irregular and micrometric with the predominant presence of Na, Si and Ca elements characteristic of amorphous soda-lime glass. The assessment of the chemical/mineralogical, morphological, thermophysical and thermal gravimetric characteristics of GP suggest its reuse as reinforcing fillers or filler in composite materials to obtain thermal insulation.

Micro and nanometric wear evaluation of metal discs used on determination of biodiesel fuel lubricity

The contact of diesel fuel with engine subsystems demands a good wear resistance. Lubricity is an important feature for integrity of injection system and the sulphur composites are primarily responsible for lubrication of the injector nozzle. Biodiesel is responsible for partially restoring the lubricity of diesel fuel that presents low levels of sulphur composites and, furthermore, it causes less pollution than diesel fuel. The lubricity is measured through the wear scar diameter following the ASTM D 975 standards. However, the friction and wear with light loads of micro/nanocomponents are highly dependent on surface interactions that can be evaluated by microscopy techniques. This study aimed to measure and to analyze the biodiesel lubricity and their blends (B5, B20) with diesel by observing the wear scars of discs using the scanning electronic microscopy (SEM), atomic force microscopy (AFM) and micro roughness techniques. The fuels performance was evaluated using HFRR tribometer. The tests conditions were based on standard ADTM D-6079-04. The coefficient of friction was measure during the test. After the test, the worn ball and disc were analyzed by SEM, AFM and profilometer. The results showed that the addition of biodiesel in diesel improve the tribological performance of fuel. Also, the just WSD value is not sufficient to evaluate the lubrication ability of a fuel. Analysis of the worn disc surfaces proved to be compatible with WSD number and also more sensitive to these kinds of fuels, showing mainly the form and intensity of the wear.

Correlation Between Fuel Lubricity and Vibration Signals Obtained in Ball-disc Analysis Using Fourier Transform

During the contact between metallic surfaces in mechanical systems, some dynamic characteristics present significant changes as the vibration signal patterns. The acquisition and characterization of these signals, by the use of Fourier Transform (FT), are non-intrusive tools in the evaluation of lubricity. This study aimed to evaluate dynamically the fuels lubricity (diesel S50, biodiesel and its blends) by the reciprocating sliding of a ball against a flat disc (AISI 52100 steel). After that, the vibration signals were evaluated by statistical test and FFT (Fast Fourier Transform) and STFT (Short-Time Fourier Transform) analyses and verified their associations with parameters supplied by ASTM D6079. The results present a correlation between lubricity, frequency spectrum and the parameters of profiles from the worn disc surface. In addition, the evolution of wear scars presented an influence of the biodiesel content in these fuels.