Antti Järvenpää

Microstructural modification of pure Mg for improving mechanical and biocorrosion properties

In this study, the effect of microstructural modification on mechanical properties and biocorrosion resistance of pure Mg was investigated for tailoring a load-bearing orthopedic biodegradable implant material. This was performed utilizing the friction stir processing (FSP) in 1-3 passes to refine the grain size. Microstructure was examined in an optical microscope and scanning electron microscope with an electron backscatter diffraction unit. X-ray diffraction method was used to identify the texture. Mechanical properties were measured by microhardness and tensile testing. Electrochemical impedance spectroscopy was applied to evaluate corrosion behavior. The results indicate that even applying a single pass of FSP refined the grain size significantly. Increasing the number of FSP passes further refined the structure, increased the mechanical strength and intensified the dominating basal texture. The best combination of mechanical properties and corrosion resistance were achieved after three FSP passes. In this case, the yield strength was about six times higher than that of the as-cast Mg and the corrosion resistance was also improved compared to that in the as-cast condition.

Mechanical Properties of Laser Heat Treated 6 mm Thick UHSS-Steel

In this work abrasion resistant (AR) steel with a sheet thickness of 6 mm was heat treated by a 4 kW Nd:YAG and a 4 kW Yb:Yag–laser, followed by self‐quenching. In the delivered condition, test material blank (B27S) is water quenched from 920° C. In this condition, fully martensitic microstructure provides excellent hardness of over 500 HB. The test material is referred to AR500 from now onwards. Laser heat treatment was carried out only on top surface of the AR500 sheet: the achieved maximum temperature in the cross‐section varies as a function of the depth. Consequently, the microstructure and mechanical properties differ between the surfaces and the centre of the cross‐section (layered microstructure). For better understanding, all layers were tested in tensile tests. For a wide heat treatment track, the laser beam was moved by scanning. Temperatures were measured using thermographic camera and thermocouples. Laser heat treated AR500 samples were tested in hardness tests and by air bending using a pres...

Passive Laser Assisted Bending of Ultra-High Strength Steels

Formability of ultra-high strength steels is poor causing problems in bending and stretch forming. The target of this work was to improve the formability of ultra-high strength steel sheets by controlled local laser heat treatments. Three steel grades, a bainitic-martensitic 4 mm DQ960 and two martensitic WR500 with 6 mm and 10 mm thicknesses were heated by controlled thermal cycles using a 4 kW Yb:Yag –laser, followed by self-cooling. Sheets with the thicknesses of 4 and 6 mm were treated on one side only by heating up to the austenitizing temperature. The 10 mm thick WR500 sheet was heat treated separately on the both surfaces by heating to a lower temperature range to produce a shallow tempered layers. The tensile and bendability tests as well as hardness measurements indicated that laser heat treatment can be used to highly improve the bendability locally without significant strength losses.

Enhancing Mechanical Properties and Formability of AISI 301LN Stainless Steel Sheet by Local Laser Heat Treatment

This study demonstrates applying local laser heat treatment to produce ultrafine-grained austenite (UFGA) structures in an AISI 301LN type commercial austenitic steel. Pieces of 50% cold-rolled sheets containing more than 90% strain-induced martensite were heated locally by a laser beam to various peak temperatures to obtain different degrees of martensite reversion to austenite. Mechanical properties and formability of grain-refined and coarse-grained structures were measured by tensile and Erichsen cup tests. In addition to standard Erichsen cup test, additional interrupted tests were carried out, where cups were first stretched close to the critical strain. Drawn cups were then heated locally by a laser beam to revitalize the structure and thereby enhance the formability in the following cupping test until failure. Results showed that local laser heat treatment is suitable for the reversion treatment to refine the austenite grain size. Various structures were produced: completely reverted microstructures (T > 700 °C) with grain sizes 0.9 - 2 µm in addition to partially reverted structure (T < 700 °C) containing nano- and ultrafine-grained austenite (0.6 µm) with some martensite. The grain refinement by local annealing improved the strength properties. The Erichsen cup tests showed that the formability was equal in the completely reverted ultrafine-grained structures to that of the coarse-grained sheets. It was demonstrated that the local laser treatment restored formability of the drawn cups, allowing stretching to be continued. The second forming step after the laser-treatment provided an enhancement of 19 and 14% in the cup depths in coarse-grained and ultrafine-grained steels, respectively, even though the laser-treatment parameters were not optimized yet.

Bendability and Microstructure of Direct Quenched Optim® 960QC

Use of ultra-high-strength steels (UHSS) in weight critical constructions is an effective way to save energy and minimize carbon footprint in the end use. On the other hand, the demands for reducing manufacturing costs and energy consumption of the steelmaker are increasing. This has led to development of energy efficient direct quenching (DQ) steelmaking process as an alternative to the conventional quenched and tempered or thermomechanical rolling and accelerate cooled processes. Ruukki has employed thermomechanical rolling and direct quenching process (TM + DQ) for a novel type of ultra-high-strength strip and plate steels since 2001. Advantages of the ultra-high-strength level (>900MPa) can be fully utilized only if fabricated properties are on a sufficient level. Bending is one of the most important workshop processes and a good bendability is essential for a structural steel. Hence, the metallurgy and bendability of Ruukki ́s TM + DQ strip steel Optim® 960QC have been investigated closely. It was found that by optimizing process parameters and chemical composition, a good combination of strength and ductility can be achieved by a modification of martensitic-bainitic microstructure. Despite of smaller total elongation, the bendability of Optim® 960QC is at least on the same level as on conventionally manufactured 960MPa steels. However, it is important to pay special attention to bending process (tool parameters, springback, bending force, material handling) when bending UHSS. It was also found that the bendability of Optim® 960QC can be significantly enhanced by local laser heat treatments or roll forming.

A Novel Heat Treatment Line for Processing of Tailored Small Batch Steels

This study describes design and construction of a novel flexible heat treatment line for processing customer-oriented small batch steels. The induction heater (600 kW) developed is suitable for the sheet thickness in the range 3.2 30 mm and the width of 85 1250 mm. Sheets are fed using an electrical motor (1.5 kW) and a chain drive, the speed being in the range 0.3 7 m/min, depending on the power and the sheet dimensions. At this study, 4.5 (WR-1) and 10 mm (WR-2) thick wear resistant steels were tempered at different peak temperatures to compare the effect of rapid tempering on mechanical properties. Results showed that the heat treatment line is capable of producing tempered steel grades with adequate properties at industrial product rate. For example, 4.5 thick WR-1 tempered at 550 oC provided a yield strength (YS) over 1000 MPa with minimum bending radius of 6 mm (in the delivered condition YS = 1605 MPa and Rmin = 12). Tempering of WR-1 at 700 oC provided YS of 762 MPa and Rmin of 1 mm. Results were similar between two test materials, but the enhancement in bendability was slightly more effective with the thinner sheet.

Designing and Manufacturing of a Flexible Longitudinally Laminated Sandwich Panel Forming Tool

The main aim of the study was to develop forming tools for wide (over 1.2 meter) sandwich panels. Longitudinal laminating technology was selected for tool manufacturing due to its flexibility and cost efficiency. Laminating technology enables easy modification of the tool dimensions afterwards. The function to optimize or vary the dimensions of the tool was set as a secondary objective for the study. Forming tools for sandwich panels are usually complicated structures and joining of the plates can be difficult in some cases. Typically sandwich forming tools are capable to produce only narrow panels (less than 1 meter) and optimization must be done during designing of the tool. In this study, a rapid designing and manufacturing of a flexible sandwich panel forming tool was investigated. Sandwich panels are usually applied in light structures or voice covers due to their very low weight, high stiffness, durability and production cost savings. Designing of the forming tool was made by using a 3D CAD program. Conventional steel plates were used for the forming tool and the assembly was done by fixing the plate parts longitudinally together (laminating). Most important criterion for the forming tool was its capability to produce high quality geometry for the core. Laser welding assembly showed that the quality of the core was good enough for welding the lap joints properly. Both of the objectives were fulfilled: 1) forming tools were suitable for forming of wide cores (1.2 meter) and 2) the structure of the laminated tool enables to change or add new plate parts to change the dimensions of the final product.

Mechanical Properties of a Metal Sandwich Panel Manufactured Using Longitudinally Laminated Forming Tools

Sandwich panel structures are increasingly used in applications where the most important demands are the weight saving and long service life. Utilizing sandwich panels, extremely light-weight, stiff and robust structures can be manufactured. In this study, sandwich panels were produced by specially designed cost-effective forming tools. Various kind of test materials were used for corrugated cores and skin plates: conventional low-carbon steel grade EN 10130 and ferritic stainless steel grade 1.4509 with plate thicknesses of 0.6 and 0.75 mm. A common S355 structural steel was used as a reference for bending strength comparison.For measuring the stiffness, MTS tensile and fatigue testing machine was selected to determine the bending resistance of the sandwich panels. The bending force, needed for yielding and fracture, related to the bending length and intensity was compared with the results from bending of the reference plates. Results showed that the bending force of the panels is significantly higher than that of a plate having similar intensity. The best results were obtained with the stainless steel (SS) panel that had 27% higher bending force at the yield point than 5 mm thick S355 plate having 3 times larger intensity. The carbon steel panel was approximately 40% weaker than the SS-panel and both panel types lost strength when loading direction was changed from transverse to 45 degree and further to 90 degree load (longitudinal).

Effect of high-pressure torsion on microstructure, mechanical properties and corrosion resistance of cast pure Mg

High-pressure torsion (HPT) processing was applied to cast pure magnesium, and the effects of the deformation on the microstructure, hardness, tensile properties and corrosion resistance were evaluated. The microstructures of the processed samples were examined by electron backscatter diffraction, and the mechanical properties were determined by Vickers hardness and tensile testing. The corrosion resistance was studied using electrochemical impedance spectroscopy in a 3.5% NaCl solution. The results show that HPT processing effectively refines the grain size of Mg from millimeters in the cast structure to a few micrometers after processing and also creates a basal texture on the surface. It was found that one or five turns of HPT produced no significant difference in the grain size of the processed Mg and the hardness was a maximum after one turn due to recovery in some grains. Measurements showed that the yield strength of the cast Mg increased by about seven times whereas the corrosion resistance was not significantly affected by the HPT processing.

Optimization of Local Laser Heat Treatment Process Using a Simple FE-Model

Local laser heat treatment is an efficient method to manufacture tailored heat-treated steel strips. It can be applied to soften narrow zones of the strip in order to improve its formability on desired areas. However, the properties achieved are dependent on several process parameters. An objective is to develop a predictive model to optimize the heat treatment parameters instead of using experimental trials. In the present study, a finite element model was applied to predict the maximum temperature and heating and cooling rates, as well as the heat distribution along the heat treated area. To develop the model and to test its feasibility, experiments were performed, in which process parameters were varied to study their effects on temperature distribution in a 6 mm thick abrasion resistant steel grade. Scanning of a laser beam was used to optimize the width and depth of the heat-affected zone.In practice, local laser heat treatment process parameters have to be optimized with care for successful results. The most important task is to minimize the temperature gradient between the surfaces and to keep the peak temperatures close to the austenitizing temperature. The results indicate that a simple model can be used to predict the outcome of the heat treatment, so that finite element modeling can be adopted as a suitable tool for design of local heat treatments, allowing more advanced treatments and applications with complex geometries.