Baolong Zheng

Spark Plasma Sintering of Cryomilled Nanocrystalline Al Alloy - Part I: Microstructure Evolution

Aluminum alloys are widely used because they are lightweight and exhibit high strength. In recent years, spark plasma sintering (SPS) technology has emerged as a viable approach to sinter materials due to its application of rapid heating and high pressure. In this study, SPS was chosen to consolidate dense ultrafine-grained (UFG) bulk samples using cryomilled nanostructured Al 5083 alloy (Al-4.5Mg-0.57Mn-0.25Fe, wt pct) powder. Both bimodal microstructure and banded structure were observed through transmission electron microscopy (TEM) investigation. The evolution of such microstructures can be attributed to the starting powder and the process conditions, which are associated with the thermal, electrical, and pressure fields present during SPS. A finite element method (FEM) was also applied to investigate distributions in temperature, current, and stress between metallic powder particles. The FEM results reveal that the localized heating, deformation, and thermal activation occurring at interparticle regions are associated with the formation of the special microstructure.

High-strain induced reverse martensitic transformation in an ultrafine-grained Ti-Nb-Ta-Zr alloy

Abstract We report on a novel phenomenon, that is a high-strain-induced reverse martensitic transformation in an ultrafine-grained Ti–36Nb–2Ta–3Zr (wt.%) alloy processed by equal channel angular pressing (ECAP) at room temperature. Our results show that a martensitic transformation from body-centred cubic β matrix to orthorhombic α″ martensite occurs under low-strain ECAP conditions and that a large portion (~34%) of martensite transforms into a matrix phase (i.e. reverse martensitic transformation) with increasing ECAP strain to a high value of 4 (i.e. 6 passes) with a corresponding reduction in the α″-lath thickness and a refinement of grain size in the matrix phase.