Bülent Kurt

Investigation of Microabrasion Wear Behavior of Boronized Stainless Steel with Nanoboron Powders

In this study, 304 stainless steel was boronized using nano boron powders using a solid-state box boronizing technique. Boronizing processes were carried out at temperatures of 950 and 1000°C for 2 and 4 h of treatment. Nano boron was used as a source of boron and KBF4 salt was used as an activator. The boxes in which boron was processed were made of 304 stainless steel plates. A free-ball microabrasion test was performed on the boronized samples. Silicon carbide (SiC) abrasive powders (5 μm) were used in the abrasion experiments. The ball rotational speed was 73.7, 102.5, and 147.4 rpm in the free-ball microabrasion test. Boronized steels showed an improvement in abrasive wear resistance. Microstructures and wear surfaces of the samples were inspected using scanning electron microscopy (SEM) and optical microscopy. It was observed from SEM and optical examinations that boronizing time and temperature had an important effect on the thickness of the boride layer on steel surfaces. The presence of boride formed in the boride layer at the surface of the steels was determined by X-ray diffraction (XRD) analysis and (FeB, Fe2B) iron boride phases were observed. The microhardness values of the iron borides was up to 1626 HV. The abrasion rate for the boronized samples was quite high for abrasive and adhesive conditions due to a brittle layer with a nonuniform crystalline structure on the outer surface. Microchannels and rolling abrasions, which are characteristic of microabrasion, were determined as the abrasion mechanism.

Microabrasion Wear Behavior of VC and CrC Coatings Deposited by Thermoreactive Diffusion Technique

Thermal reactive diffusion (TRD) coating on a DIN 1.2367 die steel substrate was performed in a powder mixture consisting of ferrovanadium, ferrochromium, ammonium chloride, alumina, and naphthalene at temperatures of 1000, 1050, and 1100°C for 2–4 h. The carbide layers were characterized using the microstructure, microhardness, X-ray diffraction, and chemical analysis. Wear scars were analyzed on scanning electron microscopy (SEM) micrographs with an energy-dispersive X-ray spectroscopy module. Depending on the coating process time and temperature, the thicknesses of the vanadium carbide and the chromium carbide layers formed on the substrate were obtained in a range from 7 to 30 μm and 5 to 17 μm, respectively. The maximum hardness values of vanadium carbide and chromium carbide layers were measured as 2537 and 1973 HV, respectively. The test samples coated using the TRD method were analyzed with regard to abrasive wear behavior using three different loads (1, 2, and 3 N) and speeds of 40, 80, and 160 rpm in fixed-ball micro-abrasion tests. Depending on the load and speed values applied, the grooving and rolling mechanisms were found to be predominant abrasion mechanisms on the worn surfaces.

The investigation of corrosion behavior of borided AISI 304 austenitic stainless steel with nanoboron powder

In this study, corrosion behavior and mechanical properties of AISI 304 austenitic stainless steel, which was borided with Nanoboron powder, was investigated. The commercially available steel was subjected to a boriding treatment with a size of 10–50 nm Nanoboron powders, at the temperatures of 1223 K to 1273 K with boriding durations of 2 to 4 h. Microstructure characterization of the steel was carried out with optical microscopy, scanning electron microscopy, microhardness and X-ray diffraction analyses. Corrosion tests were made by static immersion into a 10% H2SO4 acid solution and weight loss calculations as well as salt spray tests were carried out in accord with the ASTM B-117 standard. Boriding thermal treatment, increased the corrosion resistance of the steel against the acid solution, up to about 4.3 times while in the salt spray tests, weight loss corrosion resistance increased up to tier 2. However, anti-corrosion resistance decreased by 40%, its untreated value.

The effect of process conditions in heat-assisted boronizing treatment on the tensile and bending strength characteristics of the AISI-304 austenitic stainless steel

In this study, AISI 304 austenitic stainless steel surface was boronized with nanoboron and ekabor-III powders at 950 and 1000°C for 2 and 4 hours period by solid-state box boronizing method. Then, behaviors of the boronized specimen in the microstructure, three-point bending, and tensile strength characteristics were investigated. As a result of the boriding process, the boride layer thickness in the range of 23–67 µm and microhardness value in the range of 1020–2200 HV have been obtained according to the increase in processing time and temperature and to the particle size of the boron source (0, 1). The coating layer on boronized specimens did not exhibit any sign of reaction caused by the tensile strength applied until the yield point was in both tests. Although the particle size of the boron agents was more effective on the boronized specimen’s bending and tensile strength behaviors, it was observed that processing temperature and its duration are effective as well.

Microstructural Characteristic of Co-Cr-Mo Powder Alloy Coating on Stainless Steel by Plasma Transferred Arc Weld Surfacing

Abstract In this study, Co-Cr-Mo powder was coated on the surface of AISI 304 stainless steel by the plasma transfer arc (PTA) process at 80, 90 and 100 A current values and argon gas was used for both plasma and protective. Deposition layers were examined with optical microscopy, SEM, EDX, XRD analysis and microhardness test. The thickness of the coating increased with current density. No cracks or pores were detected in the interface and coating layer. Higher current levels resulted in higher dilution levels and also in melting/burning of the substrate.