C.J. Sutcliffe

Selective Laser Melting: a regular unit cell approach for the manufacture of porous, titanium, bone in-growth constructs, suitable for orthopedic applications.

In this study, a novel porous titanium structure for the purpose of bone in-growth has been designed, manufactured and evaluated. The structure was produced by Selective Laser Melting (SLM); a rapid manufacturing process capable of producing highly intricate, functionally graded parts. The technique described utilizes an approach based on a defined regular unit cell to design and produce structures with a large range of both physical and mechanical properties. These properties can be tailored to suit specific requirements; in particular, functionally graded structures with bone in-growth surfaces exhibiting properties comparable to those of human bone have been manufactured. The structures were manufactured and characterized by unit cell size, strand diameter, porosity, and compression strength. They exhibited a porosity (10-95%) dependant compression strength (0.5-350 Mpa) comparable to the typical naturally occurring range. It is also demonstrated that optimized structures have been produced that possesses ideal qualities for bone in-growth applications and that these structures can be applied in the production of orthopedic devices.

Experimental investigation of nanosecond pulsed Nd : YAG laser re-melted pre-placed powder beds

Describes the effects of the major process variables (Q‐switch pulse frequency, laser power, scan speed, scan spacing and scan length) on the production of single layer coupons. Results are compiled as a list of qualitative effects on the samples, such as degree of melting, shock compression effects, thermal stress cracking, etc. The results show that at certain pulse frequencies, evaporation recoil forces overcome the surface tension forces acting on the melt, improving cohesion compared to continuous wave (CW) lasing regime. The advantages lie in greater scan spacing and scan speeds enabling faster processing times for metallic objects built in this manner. The results also show the effect of power, scan speed, scan spacing and scan length on the morphology of the samples.

The Influence of Processing Parameters on the Mechanical Properties of Selectively Laser Melted Stainless Steel Microlattice Structures

The rapid manufacturing process of selective laser melting has been used to produce a series of stainless steel 316L microlattice structures. Laser power and laser exposure time are the two processing parameters used for manufacturing the lattice structures and, therefore, control the quality and mechanical properties of microlattice parts. An evaluation of the lattice material was undertaken by manufacturing a range of struts, representative of the individual trusses of the microlattices, as well as, microlattice block structures. Low laser powers were shown to result in significantly lower strand strengths due to the presence of inclusions of unmelted powder in the strut cross-sections. Higher laser powers resulted in struts that were near to full density as the measured strengths were comparable to the bulk 316L values. Uniaxial compression tests on microlattice blocks highlighted the effect of manufacturing parameters on the mechanical properties of these structures and a linear relationship was found between the plateau stress and elastic modulus relative to the measured relative density.

High density net shape components by direct laser re-melting of single-phase powders

Direct Metal Laser Re-Melting is a variant of the Selective Laser Sintering process, a Rapid Prototyping (RP) technology. This tool-less manufacturing technology has the potential of producing complex, high quality components from single-phase metal powders in short time scales. This is made possible by the production of consecutive two-dimensional layers. Unfortunately, finished components manufactured by this technique have their integrity and material properties dictated by the porosity within the laser re-melted structure. In order to maintain structural integrity comparable to conventionally produced components, metal components produced by the rapid prototyping method should exhibit a porosity of the order of maximum of ∼2% with corresponding bulk material properties. To achieve these objectives, process and laser parameters require optimisation for maximum densities to be attained. This paper reports on the development of a scanning strategy that produces stainless steel (316L) laser re-melted components which exhibit porosities of <1%, while maintaining the concept of rapid prototyping.

The Mechanical Properties of Sandwich Structures Based on Metal Lattice Architectures

A range of metallic lattice structures were manufactured using the selective laser melting (SLM) rapid prototyping technique. The lattices were based assemblies of repeating unit-cells with their strands oriented at 0°, ±45°, and 90° to the vertical when viewed from the front. Mechanical tests on the strands and the lattice blocks showed that these systems exhibit a high level of reproducibility in terms of their basic mechanical properties. An examination of the compression failure mechanisms showed that the [±45°] and [±45°, 90°] lattices failed in bending and stretching modes of failure, whereas the [0°, ±45°] lattices failed as a result of buckling of the vertical pillars. Sandwich structures were manufactured by binding woven carbon-fiber reinforced plastic to the lattice structures. Subsequent three-point bend tests on these structures identified the principal failure mechanisms under flexural loading conditions. Here, cell crushing, hinge rotation, and gross plastic deformation in the strands were observed directly under the point of loading. Low-velocity impact tests were conducted on the sandwich beams and a simple energy-balance model was used to understand how energy is absorbed by the sandwich structures. The model suggests that the majority of the incident energy of the projectile was absorbed in indentation effects, predominantly in the core material, directly under the steel indenter.

Selective laser melting: A unit cell approach for the manufacture of porous, titanium, bone in-growth constructs, suitable for orthopedic applications. II. Randomized structures

In this study, the unit cell approach, which has previously been demonstrated as a method of manufacturing porous components suitable for use as orthopedic implants, has been further developed to include randomized structures. These random structures may aid the bone in-growth process because of their similarity in appearance to trabecular bone and are shown to carry legacy properties that can be related back to the original unit cell on which they are ultimately based. In addition to this, it has been shown that randomization improves the mechanical properties of regular unit cell structures, resulting in anticipated improvements to both implant functionality and longevity. The study also evaluates the effect that a post process sinter cycle has on the components, outlines the improved mechanical properties that are attainable, and also the changes in both the macro and microstructure that occur.

Micromachining of copper using Nd:YAG laser radiation at 1064, 532, and 355 nm wavelengths

Abstract The interaction phenomena of nanosecond time period Q-switched diode-pumped Nd:YAG laser pulses using 1064, 532 and 355 nm with 0.25 mm thick pure-copper foil was investigated at an incident laser intensity range of 0.5– 57.9 GW / cm 2 . For each sample, etch rate and surface structure were determined. Analysis of the results of the tests included scanning electron microscopy (SEM). A maximum etch rate of 13.3 μm per pulse was obtained for the etch rate tests carried out at 532 nm . The maximum etch rate obtainable for 1064 nm was 2.21 μm per pulse, and for 355 nm , 6.68 μm per pulse. The dramatic decrease in etch rate observed when processing at 1064 nm is thought to occur due the highly reflective nature of copper as the interaction wavelength is increased, plus the nature of the plasma formed above the material during the high-intensity laser–material interaction. This plasma then imparts energy to the surface of the processed area leading to surface melting of the area surrounding the hole as can be seen by the SEM photographs.

The production of copper parts using DMLR

The relationship between the major process variables (laser power, laser scan speed, scan length, beam overlap and Q‐switch pulse frequency) of direct metal laser re‐melting and their effect on the structure of single‐ and multi‐layer copper coupons has been investigated. The work successfully produced selectively fused copper powder layers and simple three‐dimensional copper structures with suitable laser parameters being identified for the production of parts, including thin‐walled cubic structures. It was shown that the specific energy density needed to melt thick powder beds was less than that to melt multi‐layer builds and that the type of substrate material used significantly affected the process parameters. Thus, the substrate and its thermal properties have a significant effect on the melt pool size and freezing rate.

Hierarchical tailoring of strut architecture to control permeability of additive manufactured titanium implants.

Porous titanium implants are a common choice for bone augmentation. Implants for spinal fusion and repair of non-union fractures must encourage blood flow after implantation so that there is sufficient cell migration, nutrient and growth factor transport to stimulate bone ingrowth. Additive manufacturing techniques allow a large number of pore network designs. This study investigates how the design factors offered by selective laser melting technique can be used to alter the implant architecture on multiple length scales to control and even tailor the flow. Permeability is a convenient parameter that characterises flow, correlating to structure openness (interconnectivity and pore window size), tortuosity and hence flow shear rates. Using experimentally validated computational simulations, we demonstrate how additive manufacturing can be used to tailor implant properties by controlling surface roughness at a microstructual level (microns), and by altering the strut ordering and density at a mesoscopic level (millimetre).

Development of quadrupole mass spectrometers using rapid prototyping technology

In this report, we present a prototype design of a quadrupole mass filter (QMF) with hyperbolic electrodes, fabricated at the University of Liverpool using digital light processing (DLP), a low-cost and lightweight 3D rapid prototyping (RP) technique. Experimental mass spectra are shown for H2+, D2+, and He+ ions to provide proof of principle that the DLP mass filter is working as a mass analyzer in the low-mass range (1 to 10 amu). The performance of the DLP QMF has also been investigated for individual spectral peaks. Numerical simulations of the instrument were performed by coupling CPO and Liverpool QMS-2 programs to model both the ion source and mass filter, respectively, and the instrument is shown to perform as predicted by theory. DLP thus allows miniaturization of mass spectrometers at low cost, using hyperbolic (or other) geometries of mass analyzer electrodes that provide optimal ion manipulation and resolution for a given application. The potential of using RP fabrication techniques for developing miniature and microscale mass analyzers is also discussed.