C P Foley

Why NanoSQUIDs are important: an introduction to the focus issue

Nano-scale superconducting interference devices, known as nanoSQUIDs, are an emerging research area that has been attracting a lot of attention in recent years. This is an introduction to this special edition of Superconductor Science and Technology to place the following papers into context by briefly outlining the various methods of fabrication and the wide range of potential applications.

Fabrication and characterisation of YBCO single grain boundary step edge junctions

We use ion beam etching techniques to fabricate YBCO step edge junctions (SEJ) on MgO substrates. Argon ion-beam etching (IBE) of the substrate at angles other than at normal incidence is used to define the step height and angle. Thin (/spl sim/300 nm) magnetron sputtered YBCO films are deposited over the step and patterned using microlithography and cold substrate ion-beam etching techniques. The critical current, I/sub c/ of these SEJs can be controlled by varying the angle of the step etched into the substrate. Fabrication techniques are described which produce one grain boundary at the top of the step and include a smooth return path thereby avoiding a second grain boundary at the bottom of the step. At 77 K, the current-voltage (I-V) characteristics show resistively shunted junction behaviour. These junctions routinely demonstrate reasonably large I/sub C/R/sub N/ products (0.1-0.6 mV), making them suitable for applications in high temperature SQUID devices.

Superconductivity and the environment: a Roadmap

There is universal agreement between the United Nations and governments from the richest to the poorest nations that humanity faces unprecedented global challenges relating to sustainable energy, clean water, low-emission transportation, coping with climate change and natural disasters, and reclaiming use of land. We have invited researchers from a range of eclectic research areas to provide a Roadmap of how superconducting technologies could address these major challenges confronting humanity.Superconductivity has, over the century since its discovery by Kamerlingh Onnes in 1911, promised to provide solutions to many challenges. So far, most superconducting technologies are esoteric systems that are used in laboratories and hospitals. Large science projects have long appreciated the ability of superconductivity to efficiently create high magnetic fields that are otherwise very costly to achieve with ordinary materials. The most successful applications outside of large science are high-field magnets for magnetic resonance imaging, laboratory magnetometers for mineral and materials characterization, filters for mobile communications, and magnetoencephalography for understanding the human brain.The stage is now set for superconductivity to make more general contributions. Humanity uses practically unthinkable amounts of energy to drive our modern way of life. Overall, global power usage has been predicted to almost double from 16.5 to 30?TW in the next four decades (2011 Equinox Summit: Energy 2030 http://wgsi.org/publications-resources).The economy with which electrons carry energy compels the continued quest for efficient superconducting power generation, energy storage, and power transmission. The growing global population requires new arable land and treatment of water, especially in remote areas, and superconductivity offers unique solutions to these problems. Exquisite detectors give warning of changes that are otherwise invisible. Prediction of climate and disasters will be helped by future supercomputer technologies that support huge amounts of data and sophisticated modeling, and with the aid of superconductivity these systems might not require the energy of a large city.We present different sections on applications that could address (or are addressing) a range of environmental issues. The Roadmap covers water purification, power distribution and storage, low-environmental impact transport, environmental sensing (particularly for the removal of unexploded munitions), monitoring the Earth?s magnetic fields for earthquakes and major solar activity, and, finally, developing a petaflop supercomputer that only requires 3% of the current supercomputer power provision while being 50 times faster.Access to fresh water. With only 2.5% of the water on Earth being fresh and climate change modeling forecasting that many areas will become drier, the ability to recycle water and achieve compact water recycling systems for sewage or ground water treatment is critical. The first section (by Nishijima) points to the potential of superconducting magnetic separation to enable water recycling and reuse.Energy. The Equinox Summit held in Waterloo Canada 2011?(2011 Equinox Summit: Energy 2030 http://wgsi.org/publications-resources) identified electricity use as humanity?s largest contributor to greenhouse gas emissions. Our appetite for electricity is growing faster than for any other form of energy. The communiqu? from the summit said ?Transforming the ways we generate, distribute and store electricity is among the most pressing challenges facing society today?. If we want to stabilize CO2 levels in our atmosphere at 550 parts per million, all of that growth needs to be met by non-carbon forms of energy? (2011 Equinox Summit: Energy 2030 http://wgsi.org/publications-resources). Superconducting technologies can provide the energy efficiencies to achieve, in the European Union alone, 33?65% of the required reduction in greenhouse gas emissions according to the Kyoto Protocol (Hartikainen et?al 2003 Supercond. Sci. Technol. 16 963). New technologies would include superconducting energy storage systems to effectively store power generation from renewable sources as well as high-temperature superconducting systems used in generators, transformers and synchronous motors in power stations and heavy-industry facilities. However, to be effective, these systems must be superior to conventional systems and, in reality, market penetration will occur as existing electrical machinery is written off. At current write-off rates, to achieve a 50% transfer to superconducting systems will take 20?years (Hartikainen et?al 2003 Supercond. Sci. Technol. 16 963).The Roadmap next considers dc transmission of green power with a section by Eckroad and Marian who provide an update on the development of superconducting power transmission lines in view of recent sustainability studies. The potential of magnetic energy storage is then presented by Coi and Kim, who argue that a successful transition to wind and solar power generation must be harmonized with the conventional electrical network, which requires a storage technology with a fast response and long backup times.Transport. Superconducting Maglev trains and motors for international shipping have the potential to considerably reduce the emissions that contribute to greenhouse gases while improving their economic viability by reducing losses and improving efficiencies. International shipping, alone, contributes 3% of the greenhouse gas emissions. Three sections of the Roadmap identify how high-speed rail can be a major solution to providing fast, low energy, environmentally-friendly transport enabling reduction in automobile and aircraft travel by offering an alternative that is very competitive. With maritime international environmental regulations tightening, HTS motors with the characteristics of high torque and compactness will become important devices for high-performance and low-emission electric ship propulsion systems. A section on the development of a megawatt-class superconducting motor for ship propulsion is presented by Umemoto.Monitoring in manufacturing for waste reduction. Environmental impact from the waste created by the manufacturing sector and the need to make manufacturing efficient can be addressed by terahertz imaging. This technology has great potential in non-destructive testing, industrial process monitoring and control to greatly improve the industry process efficiency and reliability by reducing waste materials and toxic by-products. The section by Du shows how terahertz imaging can provide process and property information such as rust levels under paint that can assist with the reduction of waste in manufacturing and maintenance.Monitoring for naturally occurring disturbances. The environmental and social impact of natural disasters is mounting. Febvre provides the Roadmap for the use of ultra-sensitive magnetometry to understand geomagnetic phenomena and Earth?ionosphere couplings through the study of very small variations of the magnetic field. This magnetic monitoring has many implications for understanding our environment and providing new tools for early warning of natural hazards, either on Earth or in space which will enable us to be better prepared for natural disasters.Restoring environments after military use. Throughout the world, there are many areas confirmed or suspected of being contaminated by unexploded munitions known as unexploded ordnance (UXO). Its presence is the result of wars and training of military forces. Areas affected by UXO contamination are hazardous to the public and have a major influence on the nature of land use. UXO has impact in developed as well as developing nations. For example, the USA has UXO dating back to the American Civil War and countries such as Cambodia are living with landmines as a daily issue due to more recent wars. Underwater UXO has caused severe impacts such as the explosion in 1969 in the waters of Kent in the UK that caused a reading of 4.5 on the Richter scale for earthquake monitors. Another example was a land-based detonation of a 500?kg World War II bomb in Germany killing three people in 2010. There is countless UXO from recent conflicts worldwide. Detection and accurate location with 100% reliability is required to return land to safe civilian use. Keenan provides details of a prototype magnetic gradiometer developed for this purpose.Reducing power needs for high-end IT. Supercomputers are so large that they are close to requiring their own small power plant to support the energy needed to run the computer. For example, in 2011 Facebook data centers and operations used 532 million kW hours of energy. Mukhanov explores the potential of reducing the power dissipation for future supercomputers from more than 500?MW for Exascale systems to 0.2?MW by using superconducting-ferromagnetic Josephson junctions for magnetic memory and programmable logic.Clearly superconductivity is an ultimate energy-saving technology, and its practical implementation will contribute to the reduction of CO2 emissions, improved water purification, reduction of waste and timely preparedness for natural disasters or significant events. This Roadmap shows how the application of superconducting technologies will have a significant impact when they are adopted.

YBCO step-edge junctions with highIcRn

Step-edge junctions represent one type of grain boundary Josephson junction employed in high-temperature superconducting junction technology. To date, the majority of results published in the literature focus on [001]-tilt grain boundary junctions (GBJs) produced using bicrystal substrates. We investigate the step morphology and YBCO (yttrium barium copper oxide) film structure of YBCO-based step-edge junctions on MgO [001] substrates which structurally resemble [100]-tilt junctions. High-resolution electron microscopy reveals a clean GBJ interface of width ~ 1?nm and a single junction at the top edge. The dependence of the transport properties on the MgO step-edge and junction morphology is examined at 4.2?K, to enable direct comparison with results for other junction studies such as [001]-tilt and [100]-tilt junctions and building on previously published 77?K data. MgO step-edge junctions show a slower reduction in critical current density with step angle compared with [001]-tilt junctions. For optimized step parameters, transport measurements revealed large critical current and normal resistance (IcRN) products (~3?5?mV), comparable with the best results obtained in other kinds of [100]-tilt GBJs in YBCO at 4.2?K. Junction-based devices such as SQUIDs (superconducting quantum interference devices) and THz imagers show excellent performance when MgO-based step-edge junctions are used.

Field trials using HTS SQUID magnetometers for ground-based and airborne geophysical applications

Since December 1992, CSIRO and BHP have been field trialing rf HTS SQUID magnetometers for mineral prospecting applications. Ten field trials in widely varying environments(from -16/spl deg/C to +40/spl deg/C ambient temperatures) in mostly remote locations saw the development of a system which can be operated in many configurations including ground based and airborne Transient ElectroMagnetics (TEM). The magnetometer system has been developed to a point where, at late times in TEM applications, the SQUID system has a higher signal-to-noise level than the competing traditional coil technology. In some trials, a SQUID magnetometer detected anomalies at later times than were observed with the coil system, indicating an enhanced ability to detect highly conductive targets. This paper reviews development of our 3-axis SQUID magnetometer. SQUID systems as B field sensors have advantages over coils which are dB/dt type sensors. We will discuss the importance of these advantages for mineral prospecting in regions with a conducting soil cover or overburden typical of the Australian landscape.

Terahertz imaging at 77 K

Terahertz (THz) technology is receiving increasing attention around the world due to its important potential in many application areas. Novel compact solid-state sources and detectors are being sought for?THz radiation and detection. We report the realization of a?THz imager based on a high- Tc superconducting (HTS) Josephson detector working above liquid nitrogen temperature (77?K). The detector, made of a YBa2Cu3O7?x (YBCO) step-edge Josephson junction, is coupled to a thin-film ring-slot antenna and a hemispheric silicon lens. Images of high visual quality are obtained which demonstrate unique properties of?THz radiation such as the sensitivity to water content and the ability to penetrate packaging materials. The results should stimulate further research leading to the development of a HTS superconducting?THz imaging system.

A SQUID-based metal detector?comparison to coil and x-ray systems

The presence of foreign metal bodies and fragments in foodstuff and pharmaceutical products is of major concern to producers. Further, hidden metal objects can pose threats to security. In particular, stainless steel is difficult to detect by conventional coil metal detectors due to its low conductivity. We have employed an HTS SQUID magnetometer for the detection of stainless steel particles which is based on the measurement of the remanent magnetization of the particle. Our aim was to determine the detection limits of HTS SQUID-based remote magnetometry, especially for food inspection purposes, and to make a comparison of this technique to commonly used eddy current coil and x-ray inspection systems. We show that the SQUID systems sensitivity to stainless steel fragments is significantly higher than that of coil systems if the samples are magnetized in a 100 mT magnetic field prior to detection. Further, it has a higher sensitivity than x-ray systems, depending on the density distribution of the product under inspection. A 0.6 mg piece of grade-316 stainless steel (a fragment of a hypodermic needle 0.5 mm long and 0.65 mm diameter) represents the detection limit of our system with a 150 × 150 mm2 inspection orifice.

The effects of step angle on step edge Josephson junctions on MgO

We have fabricated step edge junctions using MgO substrates and YBCO thin films. By varying the angle of the step edge over a range of angles up to 45/spl deg/, we have obtained 3 distinct step edge morphologies: a deep trench junction, a double junction and a single junction. We found that only the step angle and morphology affected the critical current density (I/sub c/) and that the film thickness-to-step height ratio had no effect over the range 0.2-1.1. Noise measurements indicated that the single junction steps had the lowest level of critical current fluctuations and the highest values of dynamic resistance. We have also studied the variation of I/sub c/ with temperature and found it follows the Ambergaokar-Baratoff model with a lower zero energy gap. We use this information to confirm that the junction parameters are affected by the c-axis tilt and the in-plane orientations proposed by others and consider the transport mechanisms across the junction.

Operation of a geophysical HTS SQUID system in sub-Arctic environments

Transient ElectroMagnetic geophysical prospecting using SQUID sensors has demonstrated potential for improved target detection at late response times compared to conventional coil sensors. We have developed a three-axis, rf SQUID sensor system which has been extensively operated in sub-Arctic conditions by a geophysics contractor. Due to the harsh environmental and operating conditions, the system is designed to operate in sub-zero temperatures (as low as minus 40/spl deg/C) and is ruggedly packaged whilst still remaining quite portable. Auto-tuning of the rf electronics has been implemented by adjusting the rf SQUID control parameters via a microprocessor controller. After a small amount of training, regular field crews have operated two of these systems in the field continuously for periods of months at a time. An example, comparing SQUID B field data to coil dB/dt data, is presented in this paper.

Inductive superconducting transition-edge detector for single-photon and macro-molecule detection

We present a new type of transition-edge sensor for single-photon and macro-molecule detection. In our detector the absorber element is an isolated, passive absorber of extremely low thermal mass, maintained close to, but below, its superconducting–normal transition, and strongly inductively coupled to a SQUID sensor. Incoming particles or photons are sensed in terms of a transient change in the inductive coupling, rather than a change in resistance. The detectors energy sensitivity and response time can be defined by the thermal mass of the absorber and its thermal contact with a substrate, independently of any electrical connections. We have modelled the energy sensitivity of our inductive superconducting transition-edge sensor using a sub-micron SQUID as an inductive read-out device. An ultimate energy resolution of order 10−25 J Hz−1 is theoretically estimated based on the properties of the read-out SQUID and the dimensions of the absorber. We also report our initial work on fabrication of the Nb nanoscale SQUID where we have used the same material deposited on top of the SQUID as a thin-film absorber.