Efendi Mabruri

Tensile properties of the modified 13Cr martensitic stainless steels

This paper reports the influence of Mo and Ni on the tensile properties of the modified 13Cr martensitic stainless steels in tempered condition. Four steels with different content of Mo and Ni were prepared by induction melting followed by hot forging, quenching and tempering. The experimental results showed that the addition of about 1% and 3% Mo has a beneficial effect to increase both the tensile strength and the elongation of the steels. On the contrary, the addition of about 3% Ni into the martensitic stainless steel results in decreasing of both the tensile strength and the elongation. Among the alloys investigated the 13Cr3Mo type steel exhibited largest tensile strength of 1348 MPa and largest elongation of 12%. The observation on the tensile fractured surfaces by using scanning electron microscope supported these findings.

The effect of tempering temperature on pitting corrosion resistance of 420 stainless steels

The AISI Type 420 stainless steels are commonly used to steam generators, mixer blades, etc. These stainless steels are most prone to pitting in dissolved Cl− containing environments. In this paper, the effect of tempering temperature on pitting corrosion resistance of AISI Type 420 stainless steels was studied. The AISI Type 420 stainless steels specimens were heat treated at the temperature of 1050°C for 1 hour to reach austenite stabilization and then quench in the oil. After that, the specimens were tempered at the temperature of 150, 250, 350 and 450°C for 30 minutes and then air cooled to the room temperature. The electrochemical potentiodynamic polarization test was conducted at 3.5% sodium chloride solution to evaluate corrosion rate and pitting corrosion behaviour. The Scanning Electron Microscope (SEM), Energy Dispersive X-Ray Spectroscopy (EDS) were used to evaluate the pitting corrosion product. The result have shown that highest pitting potential was found in the sample tempered at 250°C and ...

Study of electroless Ni-W-P alloy coating on martensitic stainless steel

Electroless nickel phospor (Ni-P) is widely used in many industries due to their corrosion and wear resistance, coating uniformity, and ability to coat non-conductive surfaces. The unique properties of tungsten such as high hardness, higher melting point, lower coefficient of linear thermal expansion, and high tensile strength have created a lot of interest in developing ternary Ni-W-P alloys. This article presents the study of electroless Ni-W-P alloys coating using acid or alkaline bath on martensitic stainless steel. Nickel sulfate and sodium tungstate were used as nickel and tungsten sources, respectively, and sodium hypophosphite was used as a reducing agent. Acid or alkaline bath refer to bath pH condition was adjusted by adding sulfuric acid. Martensitic stainless steel was immersed in Ni-W-P bath for 15, 30, and 60 minutes. The substrate of martensitic stainless steel was subjected to pre-treatment (polishing and cleaning) and activation prior to electroless plating. The plating characteristics we...

The hardness, microstructure, and pitting resistance of austenitic stainless steel Fe25Ni15Cr with the addition of tungsten, niobium, and vanadium

In this work, the effect of 2% W, 1%Nb, and 1% V addition on the hardness, microstructure, and pitting resistance to austenitic stainless steel Fe25Ni15Cr was investigated. The specimens were prepared in induction melting furnace, followed by homogenizing at 1100⁰C for 24 h. Then, the specimens were solution treated at 975⁰C for 2 h followed by water quenching and aging at 725⁰C for 15 h. The hardness was measured by using Rockwell hardness B, and metallographic observation was conducted using optical microscope and SEM-EDS. The results show that the increament of W, Nb, and V in the austenitic stainless steel Fe25Ni15Crby increased the hardness. The metal carbide precipitation occurred at grain boundaries in niobium free alloy. The addition of Nb in the alloy promotes the Laves phase transformation, and addition of V increase Nb content in the Laves phase. Laves phase formation in alloys containing niobium during aging heat treatments lead to an increase in hardness. Addition of W, Nb, and V also increase pitting resistance of the Fe25Ni15Cr austenitic stainless steel. This can be attributed to an increasing level of niobium in the matrix.In this work, the effect of 2% W, 1%Nb, and 1% V addition on the hardness, microstructure, and pitting resistance to austenitic stainless steel Fe25Ni15Cr was investigated. The specimens were prepared in induction melting furnace, followed by homogenizing at 1100⁰C for 24 h. Then, the specimens were solution treated at 975⁰C for 2 h followed by water quenching and aging at 725⁰C for 15 h. The hardness was measured by using Rockwell hardness B, and metallographic observation was conducted using optical microscope and SEM-EDS. The results show that the increament of W, Nb, and V in the austenitic stainless steel Fe25Ni15Crby increased the hardness. The metal carbide precipitation occurred at grain boundaries in niobium free alloy. The addition of Nb in the alloy promotes the Laves phase transformation, and addition of V increase Nb content in the Laves phase. Laves phase formation in alloys containing niobium during aging heat treatments lead to an increase in hardness. Addition of W, Nb, and V also increas...

STUDI EQUAL CHANNEL ANGULAR PRESSING (ECAP) SUHU NITROGEN CAIR PADA PADUAN Al-Mg-Si (Al 6061) [A Study On Equal Channel Angular Pressing At Liquid Nitrogen Temperature Of Al – Mg – Si (Al 6061) Alloys]

A STUDY ON EQUAL CHANNEL ANGULAR PRESSING AT LIQUID NITROGEN TEMPERATURE OF Al-Mg-Si (Al 6061) ALLOYS. The recent paper reports the effect of ECAP at liquid nitrogen temperature on the mechanical properties of Al-Mg-Si (Al 6061) alloys and compared to the room temperature ECAP. The ECAP experiments with route Bc were conducted on solution treated alloys using dies with internal channel angel of 120 o for 1 to 4 passes. The XRD (x-ray diffraction) analysis showed that after ECAP the peak broadening occurred on all peaks and the peak intensity strength of (111) plane was highest as it considered as the active slip plane in the Al 6061 alloys. At high deformation strain (pass 3 and 4) the ECAP at liquid nitrogen temperature resulted in higher tensile strength and higher elongation to break compared to those of room temperature ECAP. Further, the dimples of tensile fracture surface of Al 6061 processed by liquid nitrogen temperature ECAP have mean size smaller than that of Al 6061 processed by room temperature ECAP.