Francisco Melo

Elastic response and wrinkling onset of curved elastic membranes subjected to indentation test

Abstract.Starting from a polymeric-fluid droplet, by vulcanization of the fluid free surface, curved elastic membranes, several nanometers thick and a few millimeters in diameter, which enclose a constant fluid volume, are produced. In an indentation-type test, carried out by pushing the membrane along its normal by means of a micro-needle, under some conditions, wrinkles are likely to appear around the contact region. Interestingly, we observe that the instability does not significantly alter the force-displacement relation: the relation between the force and the displacement remains linear and the associated stiffness is simply proportional to the tension of the membrane. In addition, we determine that the wrinkles develop when the stretching modulus of the membrane compares with its tension, which provides a useful method to estimate the elastic constant.

How Hertzian Solitary Waves Interact with Boundaries in a 1D Granular Medium

We perform measurements, numerical simulations, and quantitative comparisons with available theory on solitary wave propagation in a linear chain of beads without static preconstraint. By designing a nonintrusive force sensor to measure the impulse as it propagates along the chain, we study the solitary wave reflection at a wall. We show that the main features of solitary wave reflection depend on wall mechanical properties. Since previous studies on solitary waves have been performed at walls without these considerations, our experiment provides a more reliable tool to characterize solitary wave propagation. We find, for the first time, precise quantitative agreements.

Conical dislocations in crumpling

A crumpled piece of paper is made up of cylindrically curved or nearly planar regions folded along line-like ridges, which themselves pivot about point-like peaks; most of the deformation and energy is focused into these localized objects. Localization of deformation in thin sheets is a diverse phenomenon, and is a consequence of the fact that bending a thin sheet is energetically more favourable than stretching it. Previous studies considered the weakly nonlinear response of peaks and ridges to deformation. Here we report a quantitative description of the shape, response and stability of conical dislocations, the simplest type of topological crumpling deformation. The dislocation consists of a stretched core, in which some of the energy resides, and a peripheral region dominated by bending. We derive scaling laws for the size of the core, characterize the geometry of the dislocation away from the core, and analyse the interaction between two conical dislocations in a simple geometry. Our results show that the initial stages of crumpling (characterized by the large deformation of a few folds) are dominated by bending only. By considering the response of a transversely forced conical dislocation, we show that it is dynamically unstable above a critical load threshold. A similar instability is found for the case of two interacting dislocations, suggesting that a cascade of related instabilities is responsible for the focusing of energy to progressively smaller scales during crumpling.

Solitary wave trains in granular chains: experiments, theory and simulations

The features of solitary waves observed in horizontal monodisperse chain of barely touching beads not only depend on geometrical and material properties of the beads but also on the initial perturbation provided at the edge of the chain. An impact of a large striker on a monodisperse chain, and similarly a sharp decrease of bead radius in a stepped chain, generates a solitary wave train containing many single solitary waves ordered by decreasing amplitudes. We find, by simple analytical arguments, that the unloading of compression force at the chain edge has a nearly exponential decrease. The characteristic time is mainly a function involving the grains’ masses and the striker mass. Numerical calculations and experiments corroborate these findings.

Experimental evidence of shock mitigation in a Hertzian tapered chain.

We present an experimental study of the mechanical impulse propagation through a horizontal alignment of elastic spheres of progressively decreasing diameter phi(n): namely, a tapered chain. Experimentally, the diameters of spheres which interact via the Hertz potential are selected to keep as close as possible to an exponential decrease, phi(n+1) = (1-q)phi(n), where the experimental tapering factor is either q(1) approximately equal to 5.60% or q(2) approximately equal to 8.27%. In agreement with recent numerical results, an impulse initiated in a monodisperse chain (a chain of identical beads) propagates without shape changes and progressively transfers its energy and momentum to a propagating tail when it further travels in a tapered chain. As a result, the front pulse of this wave decreases in amplitude and accelerates. Both effects are satisfactorily described by the hard-sphere approximation, and basically, the shock mitigation is due to partial transmissions, from one bead to the next, of momentum and energy of the front pulse. In addition when small dissipation is included, better agreement with experiments is found. A close analysis of the loading part of the experimental pulses demonstrates that the front wave adopts a self-similar solution as it propagates in the tapered chain. Finally, our results corroborate the capability of these chains to thermalize propagating impulses and thereby act as shock absorbing devices.

Wave localization in strongly nonlinear Hertzian chains with mass defect

We report observations of mechanical energy localization in a strongly nonlinear discrete lattice. The experimental setup we consider is a one-dimensional nonloaded horizontal chain of identical spheres interacting via the nonlinear Hertz potential which contains a mass defect. Our experiments show that the interaction of a solitary wave with a light intruder excites a nonlinear localized mode. In agreement with dimensional analysis, we find that the frequency of localized oscillations exceeds the incident wave frequency spectrum and nonlinearly depends on incident wave strength and on mass and size of the intruder. The absence of tensile stress between grains allows some gaps to open, which in turn induces a significant enhancement of the amplitude of oscillations. We performed numerical simulations that precisely describe our observations without any adjusting parameters.

Periodic, aperiodic, and transient patterns in vibrated granular layers

Experiments on vertically vibrated granular layers in evacuated containers reveal a variety of patterns for acceleration amplitudes above a critical value (≈2.5g). Stripes, squares, hexagons, spirals, triangles, and targets, as well as particle-like localized excitations (“oscillons”) and fronts (“kinks”) between regions with different vibrational phase are observed as the layer depth and the container oscillation frequency and amplitude are varied. A zig-zag instability, unstable hexagons, phase-disordered patterns, and “two-phase” squares are also observed. With a few noteworthy exceptions, the patterns are essentially independent of the lateral boundary conditions.

Self-Replicating Cracks: A Collaborative Fracture Mode in Thin Films

Straight cracks are observed in thin coatings under residual tensile stress, resulting into the classical network pattern observed in china crockery, old paintings, or dry mud. Here, we present a novel fracture mechanism where delamination and propagation occur simultaneously, leading to the spontaneous self-replication of an initial template. Surprisingly, this mechanism is active below the standard critical tensile load for channel cracks and selects a robust interaction length scale on the order of 30 times the film thickness. Depending on triggering mechanisms, crescent alleys, spirals, or long bands are generated over a wide range of experimental parameters. We describe with a simple physical model, the selection of the fracture path and provide a configuration diagram displaying the different failure modes.

Fulvic acid inhibits aggregation and promotes disassembly of tau fibrils associated with alzheimer's disease

Alzheimers disease is a neurodegenerative disorder involving extracellular plaques (amyloid-β) and intracellular tangles of tau protein. Recently, tangle formation has been identified as a major event involved in the neurodegenerative process, due to the conversion of either soluble peptides or oligomers into insoluble filaments. At present, the current therapeutic strategies are aimed at natural phytocomplexes and polyphenolics compounds able to either inhibit the formation of tau filaments or disaggregate them. However, only a few polyphenolic molecules have emerged to prevent tau aggregation, and natural drugs targeting tau have not been approved yet. Fulvic acid, a humic substance, has several nutraceutical properties with potential activity to protect cognitive impairment. In this work we provide evidence to show that the aggregation process of tau protein, forming paired helical filaments (PHFs) in vitro, is inhibited by fulvic acid affecting the length of fibrils and their morphology. In addition, we investigated whether fulvic acid is capable of disassembling preformed PHFs. We show that the fulvic acid is an active compound against preformed fibrils affecting the whole structure by diminishing length of PHFs and probably acting at the hydrophobic level, as we observed by atomic force techniques. Thus, fulvic acid is likely to provide new insights in the development of potential treatments for Alzheimers disease using natural products.

Experimental evidence of solitary wave interaction in Hertzian chains

We study experimentally the interaction between two solitary waves that approach one another in a linear chain of spheres interacting via the Hertz potential. When these counterpropagating waves collide, they cross each other and a phase shift in respect to the noninteracting waves is introduced as a result of the nonlinear interaction potential. This observation is well reproduced by our numerical simulations and is shown to be independent of viscoelastic dissipation at the bead contact. In addition, when the collision of equal amplitude and synchronized counterpropagating waves takes place, we observe that two secondary solitary waves emerge from the interacting region. The amplitude of the secondary solitary waves is proportional to the amplitude of incident waves. However, secondary solitary waves are stronger when the collision occurs at the middle contact in chains with an even number of beads. Although numerical simulations correctly predict the existence of these waves, experiments show that their respective amplitudes are significantly larger than predicted. We attribute this discrepancy to the rolling friction at the bead contact during solitary wave propagation.