Hajime Matsumoto

β to ω phase transformation due to aging in a Ti-Mo alloy deformed in impact compression

Abstract We investigated the roles of vacancies and their clusters introduced in a Ti–20mass% Mo alloy by high-speed compression in the formation of aged ω-phase crystals. Specimens were deformed by a static compression mode and a high-speed compression mode, and were then aged. The relationships between morphology of aged ω-phase crystals and deformation modes are discussed along with the roles of vacancies and their clusters in the nucleation and growth of aged ω-phase crystals. Aged ω-phase crystals were found to be smaller but of higher density in a high-speed deformation specimen. These results suggest that vacancies and their clusters easily become nucleation sites of aged ω-phase crystals. Several aged ω-phase crystals in a high-speed deformation specimen were of string-like shape. High-resolution electron microscopy confirmed that the string-like crystals have the ω-phase crystal structure. One of the roles of vacancies of and their clusters introduced by high-speed deformation is considered to be relief of compressive stress, which is predicted to arise in the course of transformation.

Annihilation Behaviors of Athermal omega-Phase Crystals Due to Electron Irradiation.

Annihilation behaviors of athermal omega-phase crystals formed by cooling at 131 K for 10.8 ks under four different electron irradiation conditions of acceleration voltages of 200 kV and 160 kV, and beam currents of approximately 20 pA/cm(2) and 5 pA/cm(2) were investigated using in situ dark field and HREM observation methods at 131 K. The effect of acceleration voltages on the lifetimes is recognized, i.e., in the case of approximately equal electron beam current, lifetimes at 200 kV become shorter than those at 160 kV. Also, lifetimes depend on the electron beam current at 200 kV, i.e., the higher the beam currents, the shorter the lifetimes become. However, no distinct dependence can be seen at 160 kV. Since annihilations of athermal omega-phase crystals begin after the electron irradiation for a certain period in each condition, which depends on acceleration voltages and beam currents, it is suggested that the annihilation behaviors have incubation periods.