Hisaji Kikuchi

Evaluation of different bonded investments for dental titanium casting

The properties of several different investments were investigated including phosphate bonded, magnesia bonded, and alumina cement investments.Measurements included the setting expansion, thermal expansion, and compressive strength of investments, as well as the tensile strength, elongation, Vickers hardness (VHN) and surface roughness of titanium castings. For phosphate bonded investment, the setting expansion after being mixed with its own mixing solution was 2.10%, which was larger than the other investments; the thermal expansion was −0.25% at 200 ^∘C, the compressive strength 14 and 5 MPa after heating. For titanium cast in phosphate bonded investment, the hardness on its top surface was 655 Hv, the tensile strength was 379 MPa, the elongation was 19.4%, and the surface roughness was 2.29 μ m. Athough the thermal expansion of phosphate bonded investment is small, the setting expansion is large enough to compensate for the shrinkage of titanium castings. As its thermal expansion at T ≥ 600∘C was constant and its heating-cooling cycle was almost reversible, these two properties can reduce the thermal shock and thus avoid cracking of the investment.

Hardness and microstructure of Ti-15Mo-5Zr-3Al alloy for dental casting.

Abstract Objective . The hardness and microstructures of Ti-15Mo-5Zr-3Al alloy castings were investigated for application to dental cast prostheses. Materials and methods. Cast specimens of Ti-15Mo-5Zr-3Al alloy, Ti-6Al-7Nb alloy and CP Ti were prepared using a centrifugal-type casting machine and a magnesia-based investment material. The hardness of the cross-sections of the cast specimens were measured. The microstructure of the castings was observed using an optical microscope and was then analyzed by X-ray diffractometry. Results and conclusions. The hardness of Ti-15Mo-5Zr-3Al alloy at the inner part of the castings was 361 Hv, while the hardnesses of Ti-6Al-7Nb alloy and CP Ti were 384 and 269 Hv, respectively. The thickness of the surface hardened layer for Ti-15Mo-5Zr-3Al alloy was thinner than those for Ti-6Al-7Nb alloy and CP Ti. The microstructure of the Ti-15Mo-5Zr-3Al alloy casting was confirmed to be β phase.

Dimensional changes in stone models simulating full crown preparations with adjacent teeth resulting from long-term immersion of medium-viscosity additiontype silicone rubber impressions in disinfectant solutions

If impression materials could be immersed in disinfectant solutions for a longer period, then this form of disinfection would be easier to incorporate into dental preparation procedures. This study investigated the dimensional changes in stone models resulting from immersion of medium-viscosity hydrophilic addition-type silicone rubber impression material in disinfectant solutions for 30 min and 24 h. Impressions of a master die designed to simulate a full crown preparation with adjacent teeth were immersed in 2% glutaraldehyde and 0.55% ortho-phthalaldehyde solutions. The dimensional changes in the mesiodistal and buccolingual dimensions in the stone models were then measured using a three-dimensional coordinate system. It was found that the dimensional changes in the stone models caused by immersion of the impression materials were less than 15 μm. Immersion in 2% glutaraldehyde or 0.55% ortho-phthalaldehyde for 24 h was as clinically acceptable for medium-viscosity hydrophilic addition-type silicone rubber impressions as immersion for 30 min.