Hongjoo Rhee

Micromechanical characterization of thermomechanically fatigued lead-free solder joints

Nanoindentation testing (NIT) was used to investigate micromechanical properties of (i) as-fabricated, (ii) thermomechanically fatigued (TMF), and (iii) TMF and crept lead-free solder joints. NIT also served to generate information for a database on lead-free solder joints. Sn–Ag-based solder materials used in this study included a binary eutectic alloy, one ternary alloy, and two quaternary alloys. TMF solder joints were thermally cycled for 0, 250, 500, 1000 cycles between −15 and 150 °C. Using NIT, mechanical properties such as hardness, elastic modulus, strength trends, creep behavior, and stress exponent for power-law creep were obtained on small (nominally, 100 μm thick) solder joints. Because the volume of material probed by the indenter during NIT is small and highly localized, the properties observed depended strongly on the particular joint microstructure of the indent location. Scanning electron microscopy (SEM) was used to image the nanoindents and monitor deformation and fracture events that resulted from the indenting.

Mechanical characterization of Sn‐3.5Ag solder joints at various temperatures

Deformation studies on eutectic Sn‐Ag solder (Sn‐3.5Ag in wt percent) joints were carried out at a range of temperatures using a rheometric solids analyzer (RSA‐III). Various performance parameters were evaluated with this equipment by subjecting geometrically realistic solder joints to shear loading at various temperatures (25, 75, 100, 125, and 150°C) with a nominal joint thickness of ∼100 μm and 1×1 mm solder joint area. Mechanical properties such as shear stress versus simple shear‐strain relationships, peak shear stress as a function of rate of simple shear‐strain and testing temperature, and creep parameters were evaluated to gain a better understanding of the parameters contributing to thermomechanical fatigue.

The effects of water and microstructure on the mechanical properties of bighorn sheep (Ovis canadensis) horn keratin

The function of the bighorn sheep horn prompted quantification of the various parametric effects important to the microstructure and mechanical property relationships of this horn. These parameters included analysis of the stress-state dependence with the horn keratin tested under tension and compression, the anisotropy of the material structure and mechanical behavior, the spatial location along the horn, and the wet-dry horn behavior. The mechanical properties of interest were the elastic moduli, yield strength, ultimate strength, failure strain and hardness. The results showed that water has a more significant effect on the mechanical behavior of ram horn more than the anisotropy, location along the horn and the type of loading state. All of these parametric effects showed that the horn microstructure and mechanical properties were similar to those of long-fiber composites. In the ambient dry condition (10 wt.% water), the longitudinal elastic modulus, yield strength and failure strain were measured to be 4.0 G Pa, 62 MPa and 4%, respectively, and the transverse elastic modulus, yield strength and failure strain were 2.9 GPa, 37 MPa and 2%, respectively. In the wet condition (35 wt.% water), horn behaves more like an isotropic material; the elastic modulus, yield strength and failure strain were determined to be 0.6G Pa, 10 MPa and 60%, respectively.

Compressive behavior of a turtle's shell: experiment, modeling, and simulation.

The turtles shell acts as a protective armor for the animal. By analyzing a turtle shell via finite element analysis, one can obtain the strength and stiffness attributes to help design man-made armor. As such, finite element analysis was performed on a Terrapene carolina box turtle shell. Experimental data from compression tests were generated to provide insight into the scute through-thickness behavior of the turtle shell. Three regimes can be classified in terms of constitutive modeling: linear elastic, perfectly inelastic, and densification regions, where hardening occurs. For each regime, we developed a model that comprises elasticity and densification theory for porous materials and obtained all the material parameters by correlating the model with experimental data. The different constitutive responses arise as the deformation proceeded through three distinctive layers of the turtle shell carapace. Overall, the phenomenological stress-strain behavior is similar to that of metallic foams.

Roles of imposed cyclic strain amplitude and cyclic strain rate on the stress relaxation behaviour of pre‐strained eutectic Sn‐3.5Ag solder joints

Purpose – To understand the roles of service‐related parameters, such as imposed cyclic strain amplitude and cyclic strain rate, on the stress relaxation behaviour of eutectic Sn‐Ag solder joints.Design/methodology/approach – Cyclic shear straining with associated stress relaxation at the shear strain extremes imposed was carried out on pre‐strained eutectic Sn‐Ag solder joints with various cyclic shear straining conditions. Results from such experiments were compared with previously reported findings from monotonic shear straining and stress relaxation tests.Findings – At higher testing temperatures with a larger cyclic strain amplitude, stress states realized at the subsequent cycle are comparable with, or even gradually increase on, those experienced at the previous cycle, especially after few cycles. The maximum shear stress obtained at each cycle and residual stress during stress relaxation are strongly affected by cyclic strain rate. Stress relaxation during subsequent cycles of straining was found ...

Geometric Effects on Stress Wave Propagation

The present study, through finite element simulations, shows the geometric effects of a bioinspired solid on pressure and impulse mitigation for an elastic, plastic, and viscoelastic material. Because of the bioinspired geometries, stress wave mitigation became apparent in a nonintuitive manner such that potential real-world applications in human protective gear designs are realizable. In nature, there are several toroidal designs that are employed for mitigating stress waves; examples include the hyoid bone on the back of a woodpeckers jaw that extends around the skull to its nose and a rams horn. This study evaluates four different geometries with the same length and same initial cross-sectional diameter at the impact location in three-dimensional finite element analyses. The geometries in increasing complexity were the following: (1) a round cylinder, (2) a round cylinder that was tapered to a point, (3) a round cylinder that was spiraled in a two dimensional plane, and (4) a round cylinder that was tapered and spiraled in a two-dimensional plane. The results show that the tapered spiral geometry mitigated the greatest amount of pressure and impulse (approximately 98% mitigation) when compared to the cylinder regardless of material type (elastic, plastic, and viscoelastic) and regardless of input pressure signature. The specimen taper effectively mitigated the stress wave as a result of uniaxial deformational processes and an induced shear that arose from its geometry. Due to the decreasing cross-sectional area arising from the taper, the local uniaxial and shear stresses increased along the specimen length. The spiral induced even greater shear stresses that help mitigate the stress wave and also induced transverse displacements at the tip such that minimal wave reflections occurred. This phenomenon arose although only longitudinal waves were introduced as the initial boundary condition (BC). In nature, when shearing occurs within or between materials (friction), dissipation usually results helping the mitigation of the stress wave and is illustrated in this study with the taper and spiral geometries. The combined taper and spiral optimized stress wave mitigation in terms of the pressure and impulse; thus providing insight into the rams horn design and woodpecker hyoid designs found in nature.

Strain Rate and Stress-State Dependence of Gray Cast Iron

An investigation of the mechanical strain rate, inelastic behavior, and microstructural evolution under deformation for an as-cast pearlitic gray cast iron (GCI) is presented. A complex network of graphite, pearlite, steadite, and particle inclusions was stereologically quantified using standard techniques to identify the potential constituents that define the structure–property relationships, with the primary focus being strain rate sensitivity (SRS) of the stress–strain behavior. Volume fractions for pearlite, graphite, steadite, and particles were determined as 74%, 16%, 9%, and 1%, respectively. Secondary dendrite arm spacing (SDAS) was quantified as 22.50 lm 6 6.07 lm. Graphite flake lengths and widths were averaged as 199 lm 6 175 lm and 4.9 lm 6 2.3 lm, respectively. Particle inclusions comprised of manganese and sulfur with an average size of 13.5 lm 6 9.9 lm. The experimental data showed that as the strain rate increased from 10 3 to 10 s , the averaged strength increased 15–20%. As the stress state changed from torsion to tension to compression at a strain of 0.003 mm/mm, the stress asymmetry increased 470% and 670% for strain rates of 10 3 and 10 s , respectively. As the strain increased, the stress asymmetry differences increased further. Coalescence of cracks emanating from the graphite flake tips exacerbated the stress asymmetry differences. An internal state variable (ISV) plasticity-damage model that separately accounts for damage nucleation, growth, and coalescence was calibrated and used to give insight into the damage and work hardening relationship. [DOI: 10.1115/1.4035616]

On laser welding of thin steel sheets

Abstract This paper presents a process–structure–property relationship study of laser welds as a continuous consolidation method for joining thin monophased steel foils, thereby providing a more effective, less costly method to construct automotive catalytic converters. A body centred cubic (bcc) iron–chromium–aluminium alloy doped with Mischmetal was utilised in this study. Both pulsed and continuous wave modes were used to establish the limit welding diagrams for lap joint configuration. Actual laser welding parameters were selected using several testing conditions. The laser welds behaved substantially different from the base material under creep and high temperature oxidation. The difference was mainly attributed to the changes in grain morphology, precipitation of aluminium nitrides and carbides, and relocalisation of the reactive elements during liquid metal flow upon keyhole formation, solidification and cooling.

Quantitative Analysis of Tissue Damage Evolution in Porcine Liver With Interrupted Mechanical Testing Under Tension, Compression, and Shear

In this study, the damage evolution of liver tissue was quantified at the microstructural level under tensile, compression, and shear loading conditions using an interrupted mechanical testing method. To capture the internal microstructural changes in response to global deformation, the tissue samples were loaded to different strain levels and chemically fixed to permanently preserve the deformed tissue geometry. Tissue microstructural alterations were analyzed to quantify the accumulated damages, with damage-related parameters such as number density, area fraction, mean area, and mean nearest neighbor distance (NND). All three loading states showed a unique pattern of damage evolution, in which the damages were found to increase in number and size, but decrease in NND as strain level increased. To validate the observed damage features as true tissue microstructural damages, more samples were loaded to the above-mentioned strain levels and then unloaded back to their reference state, followed by fixation. The most major damage-relevant features at higher strain levels remained after the release of the external loading, indicating the occurrence of permanent inelastic deformation. This study provides a foundation for future structure-based constitutive material modeling that can capture and predict the stress-state dependent damage evolution in liver tissue.

Structure, property, and function of sheepshead ( Archosargus probatocephalus ) teeth

OBJECTIVES This paper studies A. probatocephalus teeth and investigates the mechanical properties and chemical composition of the enameloid and dentin. DESIGN Nanoindentation tests with a max load of 1000 μN and X-ray Energy Dispersive Spectroscopy (EDS) were performed along the diameter of the polished sample. Microstructural analysis of the dentin tubules was performed from SEM images. RESULTS From nanoindentation testing, the dentin of the sheepshead teeth has a nanoindentation hardness of 0.89 ± 0.21 (mean ± S.D.) GPa and a reduced Youngs modulus of 23.29 ± 5.30 GPa. The enameloid of A. probatocephalus has a hardness of 4.36 ± 0.44 GPa and a mean reduced Youngs modulus of 98.14 ± 6.91 GPa. Additionally, nanoindentation tests showed that the enameloids hardness and modulus increased closer to the surface of the tooth. X-ray Energy Dispersive Spectroscopy (EDS) data further suggests that the gradient may be a result of the wt% fluoride within the enameloid, where an increase in fluoride results in an increase in reduced Youngs modulus and hardness. CONCLUSION The microstructural characterization of the number density and area of the dentin tubules were used to address the porosity effect in the dentin to achieve the experimentally validated microhardness. The mechanical properties of the sheepshead teeth were also compared with previous nanoindentation tests from other aquatic species. The sheepshead teeth exhibit a greater reduced Youngs modulus and hardness compared to shark and piranha teeth.