Huaiyu He

Timing of the Jiufotang Formation (Jehol Group) in Liaoning, northeastern China, and its implications

The timing of the Jiufotang Formation remains speculative despite recent progress in the study of the Jehol Biota. In this paper we contribute to this topic with Ar-40/Ar-39 dating on K-feldspar (sanidine and orthoclase) from tuffs interbedded within the fossil-bearing shales of the Jiufotang Formation, from the upper part of the Jehol Group in Chaoyang, Liaoning, northeastern China. Ar-40/(39) Ar step heating analyses of K-feldspar and the SHRIMP U-Pb zircon data indicate that tuffs at the Shangheshou section erupted at 120.3 +/- 0.7 million years ago. This result confirms an Aptian age for the Jiufotang Formation that was mainly based on biostratigraphic evidence. It also places stringent controls on the age of the fossils from the formation, providing a minimum age (120 Ma) for the four-winged dinosaur, Microraptor, and the seed-eating bird, Jeholornis.

Stratigraphy and age of the Daohugou Bed in Ningcheng, Inner Mongolia

Recent fieldwork has extended the distribution of the Daohugou Bed deposits from the Daohugou Village to its several neighboring areas. The fossil-bearing Daohugou deposits uncomformably overlie complex bedrocks, and comprise three major parts. The red shales in the lower part were misidentified as belonging to the Tuchengzi Formation. Field excavation has indicated that the shales of upper part of the bed are the major fossil-bearing horizon. Due to strong tectonic activities, sediments were often folded with the sequences inverted in the region. Some newly recognized contacts between the Daohugou Bed and the volcanic rocks showed that the ignimbrite of the Tiaojishan Formation (159–164 Ma) underlies the Daohugou deposits, rather than overlying the latter as previously proposed. Thus, the age of the Daohugou deposits should be younger than the age of the ignimbrite, and thus it was incorrect to correlate the Daohugou Bed with the Middle Jurassic Jiulongshan Formation. Although biostratigraphic studies based on conchostracans and insects support a Middle Jurassic-early Late Jurassic age for the Daohugou deposits, vertebrate fossils such asLiaoxitriton, Jeholopterus and feathered maniraptorans show much resemblance to those of the Yixian Formation. In other words, despite the absence ofLycoptera, a typical fish of the Jehol Biota, the Daohugou vertebrate assemblage is closer to that of the Early Cretaceous Jehol Biota than to any other biota. We propose that the Daohugou fossil assemblage probably represents the earliest evolutionary stage of the Jehol Biota based on both vertebrate biostratigraphy and the sedimentological and volcanic features which suggest the Daohugou deposit belongs to the same cycle of volcanism and sedimentation as the Yixian Formation of the Jehol Group.

40Ar/39Ar dating of Lujiatun Bed (Jehol Group) in Liaoning, northeastern China

The Lujiatun bed of the Yixian Formation is famous for its extraordinary preservation of three-dimensional fossils and its implication for the most dramatic catastrophic mass mortality event in the Jehol Biota. The precise age of the fossil bearing deposits, however, remains to be established. Ar-40/Ar-39 step heating analyses on bulk K-feldspars from the fossil bearing tuff gave a weighted mean age of 123.2 +/- 1.0 Ma (2 sigma). This date suggests the Lujiatun bed was most likely deposited at about the same time as the Jianshangou bed of the lower Yixian Formation, representing a stage when the dinosaurs displayed the most significant radiation in the Early Cretaceous.

Geomagnetic field excursion recorded 17 ka at Tianchi Volcano, China: New 40Ar/39Ar age and significance

New 40Ar/39Ar dating of a comenditic lava atop Tianchi Volcano, China, indicates eruption at 17.1 ± 0.9 ka. The flow interior records a pair of transitional virtual geomagnetic poles and a low paleointensity of ~25 μT. Thus, it records a geomagnetic field excursion that is younger than the 41 ka Laschamp or 32 ka Auckland excursions. Implications are: (1) following a repose of several tens of kyr, Tianchi Volcano became highly active immediately following termination of the last glaciation maximum. The flare-up of silicic eruptions may reflect rapid deglaciation of the edifice. (2) A 17 ka age for the Tianchi excursion provides the first direct radioisotopic evidence that excursional behavior, which is imprecisely dated and less well documented magnetically at several other sites, is a global feature of geodynamo behavior. (3) During the Brunhes chron, 13 well-dated excursions cluster into two periods, including seven between 17 and 212 ka, and six between about 530 and 730 ka.

New age determination of the Cenozoic Lunpola basin, central Tibet

Knowing when the Tibetan Plateau reached its present elevation is important for understanding the uplift history of Tibet. Recently, Rowley & Currie (2006) suggested that central Tibet exceeded 4000 m from 35 Ma to the Pliocene using the oxygen-isotope composition of calcareous minerals in Lunpola basin sediments. However, they adopted a poor age assignment for the Dingqing Formation in the Lunpola basin based on previous microfossil studies. In this study, we present SIMS U–Pb zircon dates from a bentonite layer intercalated within the middle to lower Dingqing Formation. Twenty-six measurements yield a highly reliable U–Pb age of 23.5 ± 0.2 Ma (2σ, MSWD = 1.1), suggesting that the deposition age of the Dingqing Formation is late Oligocene to early Miocene, much older than the Miocene–Pliocene age used by Rowley & Currie (2006). This age robustly constrains the age of Cenozoic sedimentary strata in central Tibet, and hence provides an important basis for estimating the palaeoelevation in the high Tibet during the geological past.

Clockwise rotations recorded in redbeds from the Jinggu Basin of northwestern Indochina

Paleomagnetic data have been used to infer clockwise rotations and significant southward motion of the Indochina block during Cenozoic extrusion from the India-Asia collision zone. Because the Cenozoic of the Indochina block has been sparsely sampled to date and is key to determining the timing of this tectonic motion, we performed an extensive paleomagnetic study on Paleocene to Oligocene redbeds and middle Miocene sandy silts from the Jinggu Basin (23.5°N, 100.7°E), in northern Indochina. Paleomagnetic results from the redbeds pass fold tests, but they show exclusively normal polarity. There is controversy, however, on the age assignment to the lower part of the succession. If the age of the redbeds is indeed Paleogene, this indicates a prefolding remagnetization associated with Oligocene deformation of the Indochina block. If the age of the redbeds would be Late Cretaceous, their magnetization may be primary, and deposition could have taken place during the Cretaceous normal superchron. However, the abundance of secondary hematite in the redbeds in combination with the biostratigraphy, which indicates a Paleogene age for at least the upper two formations of the redbeds in the Jinggu Basin, implies a pervasive remagnetization. The middle Miocene sediments pass both the fold test and the reversals test and contain magnetite as well as hematite as carriers, suggesting a primary magnetization. Our large data set from the redbeds (>2000 paleomagnetic directions) demonstrates an ∼30°−35° clockwise rotation of the Jinggu Basin with respect to Eurasia, for both scenarios, i.e., when compared to a ca. 100 Ma pole (if the redbeds carry a primary natural remanent magnetization) or to a ca. 30 Ma pole (if the sequence is remagnetized). The middle Miocene results, however, indicate that the Jinggu Basin experienced no significant (2° ± 5.6°) rotation with respect to Eurasia. Since no major deformation has occurred within northern Indochina during Late Cretaceous to Eocene times, our results reflect a major clockwise rotation of the Indochina block during its Oligocene to early Miocene extrusion from the India-Asia collision zone.

Age and origin of charoitite, Malyy Murun massif, Siberia, Russia

Сharoitite consists of gem-quality mineral charoite and subordinate quartz, aegirine, K-feldspar, tinaksite, canasite, and some other minerals. This rock type is known only from one locality in the world associated with the Early Cretaceous (131.3 ± 2.4 Ma, K–Ar age) Malyy Murun syenite massif, Siberia, Russia. Although charoitite mineralogy is well known, there is disagreement whether it reflects metasomatic or magmatic activity. In order to understand when the charoitites formed we attempted to date it by 40Ar/39Ar incremental step-heating and laser ablation techniques. Our results show that the fibrous structure of water-bearing charoite does not retain radiogenic argon. Laser ablation 40Ar/39Ar for K-feldspar and tinaksite from the charoitite yielded several age clusters even from the same mineral grain. The oldest cluster of 134.1 ± 2.9 Ma for the K-feldspar agrees with the age of the Malyy Murun syenites. The youngest age of 113.3 ± 3.4 Ma for charoitite K-feldspar overlaps with the youngest of published K–Ar ages (112 ± 5 Ma) for one K-feldspar sample of the Malyy Murun syenite. Tinaksite is characterized by a similar spread of ages (from 133.0 ± 3 Ma to 115.7 ± 4.3 Ma) within a single grain. We suggest that charoitites originated due to the interaction of metasomatic agents derived from the Malyy Murun magma and country rocks. Timing of magma emplacement and charoitite crystallization is reflected by the older cluster of ages, whereas the younger ages are due to a secondary process.

High‐precision U‐Pb geochronology of the Jurassic Yanliao Biota from Jianchang (western Liaoning Province, China): Age constraints on the rise of feathered dinosaurs and eutherian mammals

The Yanliao Biota of northeastern China comprises the oldest feathered dinosaurs, transitional pterosaurs, as well as the earliest eutherian mammals, multituberculate mammals, and new euharamiyidan species that are key elements of the Mesozoic biotic record. Recent discovery of the Yanliao Biota in the Daxishan section near the town of Linglongta, Jianchang County in western Liaoning Province have greatly enhanced our knowledge of the transition from dinosaurs to birds, primitive to derived pterosaurs, and the early evolution of mammals. Nevertheless, fundamental questions regarding the correlation of fossil-bearing strata, rates of dinosaur and mammalian evolution, and their relationship to environmental change in deep time remain unresolved due to the paucity of precise and accurate temporal constraints. These limitations underscore the importance of placing the rich fossil record of Jianchang within a high-resolution chronostratigraphic framework that has thus far been hampered by the relatively low precision of in situ radioisotopic dating techniques. Here we present high-precision U-Pb zircon geochronology by the chemical abrasion isotope dilution thermal ionization mass spectrometry (CA-ID-TIMS) from three interstratified ash beds previously dated by secondary-ion mass spectrometry (SIMS) technique. The results constrain the key fossil horizons of the Daxishan section to an interval spanning 160.89 to 160.25 Ma with 2σ analytical uncertainties that range from ±46 to ±69 kyr. These data place the Yanliao Biota from Jianchang in the Oxfordian Stage of the Late Jurassic, and mark the Daxishan section as the site of Earths oldest precisely dated feathered dinosaurs and eutherian mammals.

40Ar/39Ar age of the onset of high-Ti phase of the Emeishan volcanism strengthens the link with the end-Guadalupian mass extinction

ABSTRACT Precise time constraints of the main extrusive phase of the Emeishan large igneous province (ELIP) remain unresolved because basalts commonly do not contain suitable minerals for U–Pb dating, whereas previous 40Ar/39Ar studies on basalts yielded tectonothermal overprint ages. The timing for the ELIP was deduced from indirect dating of minor intrusions of ultramafic/mafic and felsic compositions by geochronological methods and geological correlations. The extrusive part of the ELIP consists of an older low-Ti and younger high-Ti basalt phases. We have found fresh samples of plagioclase-phyric rocks at the lower Qiaojia extrusive section (the Yunnan province of China), which belong to the ELIP unit of the high-Ti basalt series. 40Ar/39Ar dating on plagioclase from two samples conducted at two different laboratories using different age standards yielded statistically indistinguishable results with the weighted mean age of 260.1 ± 1.2 Ma for five individual measurements. This provides the direct constraints on the onset of the ELIP high-Ti basalt extrusive phase. The obtained age is within the error or slightly older than the age of the Guadalupian–Lopingian boundary and felsic ignimbrite capping the ELIP lava succession (both dated at 259.1 ± 0.5 Ma). Our new data are strengthening the short duration of the, at least, high-Ti phase of the ELIP volcanism and its temporal link with the end-Guadalupian mass extinction. Estimation of the total duration of the ELIP volcanism awaits finding of suitable for dating low-Ti basalts.

Ultra-violet laser probe measurement of40Ar/39Ar age profile in phlogopite

Ultra-Violet Laser Ablation Microprobe (UVLAMP) extraction technique enables the direct investigation of Ar-Ar age profile in crystals, and yields more information on rates and durations of geological process than conventional single time snapshots. Phlogopite flakes from lamprophyre at Pishan dyke in western Kunlun were dated by using an UV laser (λ = 213 nm) microprobe with spot analyses. The results show good agreement with those from the conventional40Ar/39Ar step heating experiments. This indicates that the Ar isotopes are distributed homogenously in the phlogopite and the UVLAMP can be a powerful tool in the study of thermal history.