J. M. M. M. de Almeida

Fiber optic hydrogen sensor based on an etched Bragg grating coated with palladium.

A study of a sensor for hydrogen (H2) detection based on fiber Bragg gratings coated with palladium (Pd) with self-temperature compensation is presented. The cladding around the gratings was reduced down to 50 μm diameter by a chemical etching process. One of the gratings was left uncoated, and the other was coated with 150 nm of Pd. It was observed that palladium hydride has unstable behavior in environments with high humidity level. A simple solution to overcome this problem based on a Teflon tape is presented. The sensing device studied was able to respond to H2 concentrations in the range 0%-1% v/v at room temperature and atmospheric pressure, achieving sensitivities larger than 20 pm/% v/v. Considering H2 concentrations in nitrogen up to 1%, the performance of the sensing head was characterized for different thicknesses of Pd coating ranging from 50 to 200 nm.

Study of corrosion using long period fiber gratings coated with iron exposed to salty water

A study of long period fiber gratings (LPFG) over coated with iron (Fe) and subjected to oxidation in water with different sodium chloride (NaCl) concentrations is presented. The formation of iron oxides and hydroxides was monitored in real time by following the features of the LPFG attenuation band. Preliminary results show that Fe coated LPFGs can be used as sensors for early warning of corrosion in offshore and in coastal projects where metal structures made of iron alloys are in contact with sea or brackish water.

Low temperature oxidation in air of iron thin films monitored with long period fiber gratings

In this work an investigation of long period fiber gratings (LPFGs) over coated with iron (Fe) thin layers with different thicknesses and subjected to oxidation in air atmosphere under controlled temperature is presented. The formation of iron oxides was monitored in real time by following the optical features of the LPFG attenuation band. The morphology of the oxide layer was further analyzed by scanning electron microscope (SEM). Preliminary results show that iron coated LPFGs can be used as sensors for early warning of corrosion in projects where metal structures made of iron alloys are in contact with atmospheric air.

New developments on fibre optic colorimetrie sensors for dissolved CO 2 in aquatic environments

The detection of dissolved carbon dioxide (dCO2) is made possible through a colorimetric effect that occurs in a sensitive membrane. The reaction with dCO2 changes the pH of the membrane causing a small difference in its colour which results in a characteristic absorbance spectrum band near 435 nm. A sensing platform based on this effect was developed and tested in gaseous and in aqueous environments. It is a combination of a bundle of large core fibre optics (with diameters above 200 μm) with light emission diodes (LEDs) in the visible range of the spectrum, a silicon photodetector and a polymer membrane sensitive to CO2. A variation in the absorption of 3 / %VV was obtained in the range from 0 to 1.6 % of gaseous CO2 with an estimated response time below 60 seconds.

Improved long period fibre gratings sensing devices coated with thin films

Long period fibre gratings (LPFG) have found an increasing interest due to the easy fabrication in any kind of fibre through the induced electric arc technique with low cost and flexibility. They have been used in applications such as gain-flattening and band-rejection, and for sensing strain, temperature and chemical and biological parameters. The sensitivity of LPFG increases when the fibre is coated with certain thin films. In this short review it is presented the recent developments and applications of these kind of sensors.

Optical fiber sensor for early warning of corrosion of metal structures

Long period fiber gratings (LPFGs) were over coated with iron (Fe) and subjected to oxidation in air and in solutions of water containing different sodium chloride (NaCl) concentrations. The formation of iron oxides and hydroxides was monitored in real time by following the features of the gratings attenuation band. Preliminary results show that Fe coated LPFGs can be used as sensors for early warning of corrosion in offshore and in coastal projects where metal structures made of iron alloys are in contact with sea or brackish water.