Jae Seol Lee

Microstructure and Mechanical Properties of Mg-Al-Ca-Sm Alloys at High Temperature

The aims of this research are to investigate the effect of Sm addition in Mg-Al-Ca alloys on microstructure and mechanical properties. Sm addition to Mg-5Al-3Ca based alloys results in the change from dendritic to equiaxed grain morphorlogy and formation of Al-Sm rich itermetallic compounds at grain boundary and α-Mg matrix. And these Al-Sm rich intermetallic compounds were dispersed homogeously and stabilized at high temperature. And maximum yield and ultimate strength value was obtained at Mg-5Al-3Ca-2Sm alloys at elevated temperature because of homogeneous dispersion of stable Al-Sm rich intermetallic compound at high temperature.

Effect of Calcium on Solidification Behavior of Mg-Sn Based Alloys

The effect of Ca addition on microstructure change, precipitation behaviours and mechanical properties, in the present work, of Mg-Sn based alloys were investigated. With increasing of Ca additions, size of the Mg-Sn-Ca ternary phases (A-type) with fine needle shape was decreased and volume fraction of these phase were increased. As Ca was increase from 1 wt.%, 2 wt.%, size and volume fraction of Mg2Sn with coarse needle shape phase (B-type) was increased. However, in 3 wt.% Ca containing alloy, size of these Mg2Sn phase was smaller than that of 2 wt% Ca addition alloy and volume fraction of these phase was decreased.

Effects of Samarium on Microstructure and Mechanical Properties of Mg-Al-Ca Alloys

As samarium addition was increased, α- Mg matrix morphology was changed from dendritic to equiaxed grains and average value of grain size was decreased from 101.6㎛ to 39.3㎛. Samarium addition to Mg-5Al-3Ca based alloys resulted in the formation of Mg-Al-Sm thernary intermetallic compounds at grain boundarys and α-Mg matrix grains. In these alloys, two kinds of eutectic structure were observed; coarse irregular-shape structure at grain boundary and fine needle-shape structure in the α-Mg matrix grain. It is found that the yield strength and ultimate strength showed the maximum value of 109.1MPa and 139.3 at Mg-5Al-3Ca-2Sm alloy, respectively.

Superplastic Forming of AZ31 Mg Alloy Recycled by Solid-State Processing

Superplastic forming characteristics of AZ31 Mg alloy recycled by solid-state process were investigated. Cylindrical scraps and machined chips were recycled by hot extrusion and hot rolling in air. As a result of tensile test, elongation to failure of the specimens recycled from small and large cylindrical scraps was almost the same as that of the rolled specimen from a virgin ingot. On the other hand, the specimen from machined chips had much lower elongation at elevated temperatures. The oxygen concentration of the specimen recycled from machined chips showed about 60 times higher value compared with that of the other specimens. In superplastic forming tests, the specimen from small and large cylindrical scraps exhibited excellent formability similar to the rolled specimen from a virgin ingot. However, the specimen from machined chips showed poor formability. Thus, oxide contamination adversely affected the formability of recycled Mg alloy.

Microstructure and Mechanical Properties of Mg-Zn-Y Alloys Fabricated by Rapid Solidification and Spark Plasma Sintering Processes

Mg97Zn1Y2 alloy powders were prepared from gas atomization process, followed by consolidation using spark plasma sintering (SPS) process. The atomized Mg97Zn1Y2 alloy particles were entirely spherical in shape and dendrite microstructure. The compacts sintered by SPS process have values more than 99% of theoretical density. The compressive yield strength was decreased as sintering temperature increased. It is found that the compressive strength showed the maximum value of 303MPa at the sintered specimen under load of 250MPa at 350°C.

Microstructure and Formability of Different-Speeds Rolled AZ31 Mg Sheet

The aims of this study ares to investigate the microstructure evolution of AZ31 Mg alloys with normal rolling and different speeds rolling during hot rolling affects microstructure, texture and mechanical properties of AZ31 Mg alloy. In the microstructures of as-rolled both samples, twins are clearly apparent, small and recrystallized grains are visible along some grain boundary and twinned regions. The tensile strength and yield strength of DSR sample were slightly higher than that of NR sample. Also, in the case of the NR sample, tensile strength indicated different values to the rolling directions. From this result, NR sample compared to DSR sample strongly indicated to the plastic anisotropy tendency. Therefore, it is noted that DSR sample could be presented to the good formability, comparing to the NR sample. DSR samples deformed at 473K and 523K could be perfectly formed, indicating the potential application of the DSR process to improve formability of the Mg alloys at warm temperatures.

Microstructure and Mechanical Properties of Mg-Al-Ca Alloys with Yttrium Addition

The aims of this study are to investigate the effect of Y (yttrium) addition in the Mg-Al- Ca alloys on microstructure and mechanical properties. In additions, the alloys were solution treated in order to achieve a better understanding of the precipitation mechanisms. The as-cast microstructure of Mg-5Al-3Ca alloy and Mg-5Al-3Ca-xY alloys contains dendritic α-Mg matrix and eutectic intermetallic compound at grain boundary. The hardness values of Mg-Al-Ca alloy with Y additions were slightly increased than that of Mg-Al-Ca with no Y addition. It is because of reduction of α-Mg phase and presence of (Mg,Al)2Ca and Al-Y rich intermetallic phase at grain boundary and α-Mg matrix grains. Also, hardness value of yttrium (Y) containing alloys was increased with increasing Y contents. Compared to Mg-5Al-3Ca alloy, maximum strength and yield strength of the alloys with Y additions have slightly increased with increasing Y additions in the case of as-cast samples.

Characterization of Mg-Al Sheet Clad Materials Fabricated by Hot Rolling

AZ31 Mg / 5083 Al clad sheet was fabricated by the hot rolling method and its mechanical properties were investigated in this study. The tensile strength and yield strength of Mg- Al clad samples were slightly higher than that of AZ31 Mg sample, resulting in high strength 5083 Al alloy. Also, in the case of the AZ31 Mg sample, tensile strength indicated different values to the rolling directions. The thickness of interface layers between magnesium and aluminum materials increased with increasing rolling temperature. The thickness of interface layer was about 1.2 μm and 1.6 μm, respectively. The difference of thickness on the interface layer with variation of rolling temperature was attributed to promote the diffusion between magnesium and aluminum materials. The Vickers hardness of Mg-Al interface layer was around 125 Hv. The interface layer composed of hard inter-metallic phases which may act a increment of Vickers hardness depending upon its thickness.

DEVELOPMENT OF HIGH STRENGTH Mg-Cu-Zn ULTRAFINE EUTECTIC COMPOSITES WITH ENHANCED PLASTICITY

Mg-Cu-Zn ultrafine eutectic composites with different length scale heterogeneity, consisting of micrometer size dendrites and/or ultrafine scale bimodal eutectics, exhibit high yield strength as well as good plasticity at room temperature compression. Among these alloys, micron-scale α-Mg dendrites reinforced ultrafine eutectic composites exhibit high yield strength of 310 ~ 420 MPa and large plasticity of 7 ~ 12%. Meanwhile, a Mg72Cu5Zn23 alloy comprising a bimodal eutectic structure without the micron-scale α-Mg dendrites shows the optimized mechanical properties the highest yield strength of 455 MPa combined with a considerable plastic strain of ~5%.

Microstructure and Texture Evolution of Cross Rolled AZ31 Mg Sheet

The aims of this study are to investigate the microstructure evolution of AZ31 Mg alloys with normal rolling and cross rolling as the large strain hot rolling affects microstructure, texture and mechanical properties of AZ31 Mg alloys. In the microstructures of as-rolled both samples, twins are clearly apparent, small and recrystallized grains are visible along some grain boundary and twinned regions. The Lankford values of large strain cross rolled sample obviously demonstrate the higher average r-value and lower planar anisotropy value. The press formability of cross rolled Mg alloy might be improved due to control of texture and grain size by severe deformation.