Janvier Mukiza

Crystal structure of bis(μ2-S-(Z)-3-(hydroxido(phenyl)methylene)-1,1- diphenyl thioureaa-κO,S,S)hexacarbonyl dirhenium(I), C60H52N4O8Re2S2

Abstract C60H52N4O8Re2S2, monoclinic, P21/c (no. 14), a = 24.2146(6) Å, b = 8.9277(2) Å, c = 31.2847(7) Å, β = 118.864(2)°, V = 5923.1 Å3, Z = 4, Rgt(F) = 0.0360, wRref(F2) = 0.0786, T = 200 K.

Crystal structure of trans-((2-aminophenolato-κO)-(2-hydroxyphenylimido- κ2N,O)-bromido-bis(triphenylphosphane)-rhenium(V)) bromide – acetonitrile – water (1:2:1), C52H49Br2N4O3P2Re

Abstract C52H49Br2N4O3P2Re, triclinic, P1̄ (no. 2), a = 13.5222(9) Å, b = 14.1956(9) Å, c = 14.3102(9) Å, α = 92.096(3)°, β = 114.726(2)°, γ = 96.966(2)°, V = 2456.0 Å3, Z = 2, Rgt(F) = 0.0221, wRref(F2) = 0.0501, T = 200 K.

Crystal structure of (µ2-acetato-κ2O,O’)-(µ2-chlorido)-(µ2-oxido)- bis(dichlorido-triphenylphosphane-rhenium(IV)), C38H33Cl5O3P2Re2

Abstract C38H33Cl5O3P2Re2, orthorhombic, Pbca (no. 61), a = 18.9747(6) Å, b = 17.6316(5) Å, c = 22.3528(6) Å, V = 7478.2 Å3, Z = 8, Rgt(F) = 0.0278, wRref(F2) = 0.0649, T = 200 K.

Crystal structure of (μ2-acetato-κ2O,O’)-(μ2-bromido)-(μ2-oxido)-tetrabromido- triphenylphosphane-κP-triphenylphosphaneoxide-κOdirhenium( IV)), C38H33Br5O4P2Re2

Abstract C38H33Br5O4P2Re2, triclinic, P1̄ (no. 2), a = 10.7759(5) Å, b = 13.4635(6) Å, c = 14.7580(7) Å, α = 93.642(2)°, β = 108.372(2)°, γ = 91.303(2)°, V = 2025.8 Å3, Z = 2, Rgt(F) = 0.0207, wRref(F2) = 0.0492, T = 200 K.

Crystal structure of fac-κO,S-(Z)-1,1-diethyl-3-(hydroxido(phenyl)methylene) thiourea-(κS'(Z)-1,1-diethyl-3-(hydroxido(phenyl)methylene)- thiourea)- tricarbonyl rhenium(I), C27H31N4O5ReS2

Abstract C27H31N4O5ReS2, monoclinic, P21/n (no. 14), a = 10.8449(3) Å, b = 14.0018(3) Å, c = 19.9573(5) Å, β = 100.825(1)°, V = 2976.6 Å3, Z = 4, Rgt(F) = 0.0151, wRref(F2) = 0.0351, T = 200 K.

Crystal structure of tricarbonyl-chlorido-(N-(pyridin-2-yl)-N-((4-tertbutyl) benzoyl)pyridine-2-amine)rhenium(I), C24H21ClN3O4Re

Abstract C24H21ClN3O4Re, monoclinic, C2/c (no. 15), a = 22.178(1) Å, b = 12.4411(5) Å, c = 17.1519(7) Å, β = 90.270(2)°, V = 4732.5 Å3, Z = 8, Rgt(F) = 0.0179, wRref(F2) = 0.0376, T = 200 K.

Crystal structure of a second polymorph of tetraphenylphosphonium perrhenate(VII), at 200 K, C24H20O4PRe

Abstract C24H20O4PRe, tetragonal, I4̅ (no. 82), a = 12.2013(3) Å, c = 7.1016(2) Å, V = 1057.2 Å3, Z = 2, Rgt(F) = 0.0170, wRref(F2) = 0.0416, T = 200 K.

Crystal structure of chlorido-tricarbonyl-bis(2-pyridylmethanone-N,N′)-rhenium(I), C14H8ClN2O4Re

Abstract C14H8ClN2O4Re, triclinic, P1̅ (no. 2), a = 7.5566(3) Å, b = 8.3079(3) Å, c = 12.0017(6) Å, α = 83.583(1)°, β = 88.746(2)°, γ = 76.915(1)°, V = 729.3 Å3, Z = 2, Rgt(F) = 0.0277, wRref(F2) = 0.0801, T = 200 K.

Crystal structure of ammonium 5-aminoorotat monohydrate, C5H10N4O5

C5H10N4O5, orthorhombic, Pbca (no. 61), a = 7.1324(4) Å, b = 15.0481(8) Å, c = 15.285(1) Å, V = 1640.5 Å, Z = 8, Rgt(F) = 0.0339, wRref(F ) = 0.0982, T = 200 K.

Crystal structure of bis(4,5-diaza-fluoren-9-one-κ2N,N) dioxo-μ2- oxodirhenium(V)- acetonitrile (1:2), C26H18Cl4N6O5Re2

C26H18Cl4N6O5Re2, monoclinic, P21/c (no. 14), a = 10.0110(4) Å, b = 14.1829(6) Å, c = 10.7113(4) Å, % = 96.265(2)°, V = 1511.8 Å, Z = 2, R(F) = 0.0230, wRref(F ) = 0.0542, T = 200 K.