Jim Crowley

Calibrating the middle and late Permian palynostratigraphy of Australia to the geologic time-scale via U–Pb zircon CA-IDTIMS dating

ABSTRACT The advent of chemical abrasion-isotope dilution thermal ionisation mass spectrometry (CA-IDTIMS) has revolutionised U–Pb dating of zircon, and the enhanced precision of eruption ages determined on volcanic layers within basin successions permits an improved calibration of biostratigraphic schemes to the numerical time-scale. The Guadalupian and Lopingian (Permian) successions in the Sydney, Gunnedah, Bowen and Canning basins are mostly non-marine and include numerous airfall tuff units, many of which contain zircon. The eastern Australian palynostratigraphic scheme provides the basis for much of the local correlation, but the present calibration of this scheme against the numerical time-scale depends on a correlation to Western Australia, using rare ammonoids and conodonts in that succession to link to the standard global marine biostratigraphic scheme. High-precision U–Pb zircon dating of tuff layers via CA-IDTIMS allows this tenuous correlation to be circumvented—the resulting direct calibration of the palynostratigraphy to the numerical time-scale highlights significant inaccuracies in the previous indirect correlation. The new data show: the top of the Praecolpatites sinuosus Zone (APP3.2) lies in the early Roadian, not the middle Kungurian; the top of the Microbaculispora villosa Zone (APP3.3) lies in the middle Roadian, not the early Roadian; the top of the Dulhuntyispora granulata Zone (APP4.1) lies in the Wordian, not in the latest Roadian; the top of the Didecitriletes ericianus Zone (APP4.2) lies in the first half of the Wuchiapingian, not the latest Wordian; the Dulhuntyispora dulhuntyi Zone (APP4.3) is exceptionally short and lies within the Wuchiapingian, not the early Capitanian; and the top of the Dulhuntyispora parvithola Zone (APP5) lies at or near the Permo-Triassic boundary, not in the latest Wuchiapingian.

U–Pb Geochronology and Palynology from Lopingian (Upper Permian) Coal Measure Strata of the Galilee Basin, Queensland, Australia

ABSTRACT This study presents the first chemical abrasion-isotope dilution thermal ionisation mass spectrometry (CA-IDTIMS) U–Pb zircon ages from tuffs in Lopingian (upper Permian) strata of the Galilee Basin, Queensland and reassigns the B coal-seam to the ‘Burngrove Formation equivalent.’ Five Lopingian tuffs were dated: four from the CRD Montani-1 drill hole including three from the ‘Fair Hill Formation equivalent’ (255.13 ± 0.09, 254.41 ± 0.07 and 254.32 ± 0.10 Ma) and one from the ‘Burngrove Formation equivalent’ (252.81 ± 0.07 Ma, approximately the age of the Yarrabee Tuff in the adjacent Bowen Basin); and a single tuff from the Black Alley Shale in the GSQ Tambo-1-1A drill hole (254.09 ± 0.06 Ma). In the Galilee Basin, all three units are constituents of the Betts Creek Group, here formally elevated in nomenclatural status from the Betts Creek beds. On the western margin of the basin, the group thins, and the ‘J and K’ seams (formerly known as the Crossmore and Glenaras sequences, respectively) in the GSQ Muttaburra-1 drill hole have been interpreted through palynology as Cisuralian–early Guadalupian (spore-pollen assemblage APP3.2). This corroborates the exclusion of the ‘J and K’ seams from the overlying Lopingian Betts Creek Group (spore-pollen assemblage APP5), and the underlying lower to mid-Cisuralian Aramac Coal Measures (spore-pollen assemblage APP2.2), which represent the uppermost unit of the Joe Joe Group. It is proposed that the ‘J and K’ seams are restricted to a depocentre in the Hulton–Rand structure. The recognition of these strata containing APP3.2 spore-pollen assemblages suggests that the mid-Permian hiatus is locally reduced to 12–13 My from 30 Ma (where the ‘J and K’ seams are absent). The results of the radiometric dating and palynological analysis in the Galilee Basin support the proposed, albeit informal stratigraphy, that is given in terms of equivalents of formational units in the Bowen Basin and on the intervening Springsure Shelf.

New U–Pb Constraints Identify the End-Guadalupian and Possibly End-Lopingian Extinction Events Conceivably Preserved in the Passive Margin of North America: Implication for Regional Tectonics

The discovery and dating of a volcanic ash bed within the upper Phosphoria Formation in SE Idaho, USA, is reported. The ash occurs 11 m below the top of the phosphatic Meade Peak Member and yielded a 206 Pb/ 238 U date of 260.57 ± 0.07 / 0.14 / 0.31 Ma, i.e. latest Capitanian, Guadalupian. The stratigraphic position of this ash near the top of the Meade Peak phosphatic Member of Phosphoria Formation indicates plausible completeness of the sedimentation within the Guadalupian–Lopingian and probably at the Permo-Triassic (P-T) transitions. The new radiometric age reveals that the regional biostratigraphy and palaeontology of Phosphoria and Park City formations requires serious reconsideration, particularly in cool water conodonts, bryozoans and brachiopods. The new age proposes that the Guadalupian–Lopingian boundary (GLB) coincides with the Meade Peak – Rex contact and consequently with the end-Guadalupian extinction event. The lack of a major unconformity at the P-T transition suggests that the effects of the Sonoma orogeny were not as extensive as has been assumed.

Early Ordovician CA-IDTIMS U–Pb zircon dating and conodont biostratigraphy, Canning Basin, Western Australia

ABSTRACT A continuously cored section of more than 300 m through the Nambeet Formation and the basal part of the conformably overlying Willara Formation in the Olympic 1 petroleum well, drilled in the Canning Basin of northern Western Australia, yields valuable information that increases by more than 40% the number of precise isotopic ages available to constrain the Ordovician Period. New CA-IDTIMS U–Pb zircon ages for seven bentonite layers in the Olympic 1 core are integrated into a new conodont biostratigraphic framework for the Early Ordovician comprising four biozones recognised in this well. The weighted mean U–Pb dates range from 479.37 ± 0.16 Ma within the late Tremadocian Paroistodus proteus conodont Biozone, to 470.18 ± 0.13 Ma near the boundary between the Floian and Dapingian stages within the Jumudontus gananda conodont Biozone. The intervening Prioniodus oepiki–Serratognathus bilobatus conodont Biozone (early Floian) and succeeding Oepikodus communis conodont Biozone (middle Floian) are similarly well constrained by isotopic dates centred on ca 477 Ma for the early Floian and by three ages of 473–471 Ma for the middle Floian. The seven new isotopic dates significantly increase the precision of dating for the Early Ordovician, where previously only two ages with limited or imprecise biostratigraphic control were known globally.

Recalibrating Australian Triassic Palynostratigraphy to the International Geologic Timescale Using High Resolution CA-IDTIMS Dating

The Triassic is an important interval for Australian petroleum exploration, with Middle to Upper Triassic Mungaroo Formation reservoirs in the Northern Carnarvon Basin, and recent Lower Triassic discoveries in the Roebuck Basin. The chronostratigraphic understanding of Triassic petroleum systems is underpinned by biostratigraphic dating using palynological zonations. The numerical ages of these zones are usually assigned through inference and interpolation, often via tenuous correlations to the international geologic timescale using scattered marine biota, (primarily foraminifera, and rare ammonites, conodonts and/or dinoflagellates). In contrast, we tie Australian biozones to the timescale through Chemical Abrasion-Isotope Dilution Thermal Ionisation Mass Spectrometry (CA-IDTIMS) dating of interbedded volcanic tuffs. Such ashfalls are reasonably common in Australian basins, and can provide high-precision CA-IDTIMS ages if they contain magmatic zircons. We recently recalibrated Australian middle and late Permian palynozones using this approach and preliminary results suggest that Triassic biozone ages are likewise in need of considerable revision. We have targeted Triassic tuffs across Queensland, (Tarong beds, Brisbane Tuff, Moolayember Formation, Rewan Group), New South Wales (Garie Formation, Coal Cliff Sandstone, Milligan Road Formation), and Tasmania (upper Triassic coal measures) to provide numerical ages for palynozones. Additional dates in New Zealand (Murihiku Supergroup) and Timor-Leste (Wailuli Formation) will allow international correlation of dinocyst and spore-pollen zones. Numerical constraints for Triassic biozone boundaries facilitate correlation of Australian biozones with the international geologic timescale. This can impact burial history models used in petroleum exploration anywhere these biozones are used, often far beyond the basins from which the samples were collected.