Joelle Aubin

Effect of Axial Agitator Configuration (Up-Pumping, Down-Pumping, Reverse Rotation) on Flow Patterns Generated in Stirred Vessels

Single phase turbulent flow in a tank stirred with two different axial impellers, a pitched blade turbine (PBT) and a Mixel TT (MTT), has been studied using Laser Doppler Velocimetry. The effect of the agitator configuration, i.e. up-pumping, down-pumping and reverse rotation, on the turbulent flow field, as well as power, circulation and pumping numbers has been investigated. An agitation index for each configuration was also determined. In the down-pumping mode, the impellers induced one circulation loop and the upper part of the tank was poorly mixed. When up-pumping, two circulation loops are formed, the second in the upper vessel. The PBT pumping upwards was observed to have a lower flow number and to consume more power than down-pumping, however, the agitation index and circulation efficiencies were notably higher. The MTT has been shown to circulate liquid more efficiently in the up-pumping configuration than in the other two modes. Only small effects of the MTT configuration on the power number, flow number and pumping effectiveness have been observed.

Blending of newtonian and shear-thinning fluids in a tank stirred with a helical screw agitator

Newtonian and non-Newtonian laminar fluid flow has been simulated using Computational Fluid Dynamics for a cylindrical vessel stirred by a helical screw agitator. Simulations have been performed for a vessel geometry with and without a draft tube. Simulated flow patterns in the vessel have been examined and compared with the experimental work of previous authors. The power number and the circulation number have been evaluated, and interpreted in a similar manner to other works. The PO.Re constant, A, has been determined to be 295 for the geometry with the draft tube and 150 for that without the draft tube. These results are in the same range as previously reported values. The Metzner and Otto constant, k, has been evaluated to be 16.23 which is in excellent agreement with experimental results reported in the literature.

On the combined effects of surface tension force calculation and interface advection on spurious currents within Volume of Fluid and Level Set frameworks

This paper deals with the comparison of Eulerian methods to take into account the capillary contribution in the vicinity of a fluid-fluid interface. Eulerian methods are well-known to produce additional vorticity close to the interface that leads to non-physical spurious currents. Numerical equilibrium between pressure gradient and capillary force for the static bubble test case within a VOF framework has been reached in 35] with the height-function technique 14,35]. However, once the bubble is translated in a uniform flow, spurious currents are maintained by slight errors induced by translation schemes. In this work, two main points are investigated: the ability of Volume of Fluid and Level Set methods to accurately calculate the curvature, and the magnitude of spurious currents due to errors in the calculation of the curvature after advection in both translating and rotating flows. The spurious currents source term is expressed from the vorticity equation and used to discuss and compare the methods. Simulations of gas-liquid Taylor flow at low capillary number show that the flow structure and the bubble velocity can be significantly affected by spurious currents.

Key role of temperature monitoring in interpretation of microwave effect on transesterification and esterification reactions for biodiesel production

Microwave effects have been quantified, comparing activation energies and pre-exponential factors to those obtained in a conventionally-heated reactor for biodiesel production from waste cooking oils via transesterification and esterification reactions. Several publications report an enhancement of biodiesel production using microwaves, however recent reviews highlight poor temperature measurements in microwave reactors give misleading reaction performances. Operating conditions have therefore been carefully chosen to investigate non-thermal microwave effects alone. Temperature is monitored by an optical fiber sensor, which is more accurate than infrared sensors. For the transesterification reaction, the activation energy is 37.1kJ/mol (20.1-54.2kJ/mol) in the microwave-heated reactor compared with 31.6kJ/mol (14.6-48.7kJ/mol) in the conventionally-heated reactor. For the esterification reaction, the activation energy is 45.4kJ/mol (31.8-58.9kJ/mol) for the microwave-heated reactor compared with 56.1kJ/mol (55.7-56.4kJ/mol) for conventionally-heated reactor. The results confirm the absence of non-thermal microwave effects for homogenous-catalyzed reactions.

Flow Generated by Radial Flow Impellers: PIV Measurements and CFD Simulations

Particle image velocimetry (PIV) and computational fluid dynamics (CFD) have been used to investigate the single phase and gas-liquid flow generated by a Scaba SRGT turbine. The key details of the trailing vortices, the turbulent flow around the impeller blades and the accumulation of gas have been studied by using PIV measurements and CFD simulations. Both the experimental and numerical results show that the flow and the trailing vortices are not altered significantly upon gassing. The simulated results are generally in good agreement with the experimental findings. The CFD simulations also show that only small low-pressure regions exist behind the blades of the Scaba turbine compared with the very large low-pressure zones formed by the Rushton turbine. These results enable better understanding of the improved performance of the Scaba turbine for gas-liquid dispersions compared with the Rushton turbine.

Intensification of waste cooking oil transformation by transesterification and esterification reactions in oscillatory baffled and microstructured reactors for biodiesel production

Abstract The transformation of waste cooking oils for fatty acid methyl ester production is investigated in two intensified technologies: microstructured Corning® and oscillatory baffled NiTech® reactors, compared to a reference batch reactor to quantify the process intensification provided by each technology. Both reactors achieve high conversions in shorter times. For transesterification, 96 wt.% of esters are obtained in 1.4 min at 97°C in the Corning® reactor and 92.1 wt.% of esters in 6 min at 44°C in the NiTech® reactor, compared with 94.8 wt.% of esters in 10 min at 60°C in the batch reactor. For esterification, 92% conversion is obtained in 2.5 min in the Corning® reactor at 75°C compared with 20–30 min in the batch reactor at 60°C, and at 40°C, 96.8% conversion is achieved in 13.3 min in the NiTech® reactor, compared with 30 min in the batch reactor. The advantage of the Corning® reactor is that it can operate at higher pressures (1–20 bar) and temperatures (100°C), thereby providing faster kinetics than the NiTech® reactor. However, oils with a high free fatty acid level (73%) cause the Corning® reactor channels to be blocked. A wider range of operating conditions could be obtained in NiTech® with a pressure-resistant material.