John Kaufman

Impact of nitrogen doping of niobium superconducting cavities on the sensitivity of surface resistance to trapped magnetic flux

Future particle accelerators such as the SLAC “Linac Coherent Light Source-II” (LCLS-II) and the proposed Cornell Energy Recovery Linac require hundreds of superconducting radio-frequency (SRF) niobium cavities operating in continuous wave mode. In order to achieve economic feasibility of projects such as these, the cavities must achieve a very high intrinsic quality factor (Q0) to keep cryogenic losses within feasible limits. To reach these high Q0s in the case of LCLS-II, nitrogen-doping of niobium cavities has been selected as the cavity preparation technique. When dealing with Q0s greater than 1 × 1010, the effects of ambient magnetic field on Q0 become significant. Here, we show that the sensitivity to RF losses from trapped magnetic field in a cavitys walls is strongly dependent on the cavity preparation. Specifically, standard electropolished and 120 °C baked cavities show a sensitivity of residual resistance from trapped magnetic flux of ∼0.6 and ∼0.8 nΩ/mG trapped, respectively, while nitrogen...

Advanced Vertical Electro-Polishing studies at Cornell with Faraday

Cornell’s SRF group and Faraday Technology, Inc. have started collaborations on two phase-II SBIR projects. Both projects are aiming for the development of advanced Vertical Electro-Polishing (VEP) for Nb SRF cavities, such as HF free or acid free VEP protocols. These could be eco-friendlier alternatives for the standard, HF-based EP electrolyte used, and could bring new breakthrough performance for Nb SRF cavities. Here we give a status update and report first results from these two projects.

Vertical Electropolishing Studies at Cornell with KEK and Marui

Cornells SRF group has been developing Vertical Electro-Polishing (VEP) which was applied on 1.3GHz Niobium SRF cavities as the primary surface treatment. The process was done in the vertical direction, the upper and the lower half cell had removal difference. Cavity need to be flipped over during the process to compensate this. Cornell has started collaboration with KEK and Marui Galvanizing Co. Ltd. (Marui) in 2014. The first step of collaboration focused on the demonstration of Marui’s original VEP cathode named “i-cathode Ninja®” at Cornell, which was developed to make more uniform VEP removal. The results of VEP using Ninja cathode at Cornell will be presented in this paper.

Surface Analysis and Material Property Studies of Nb3Sn on Niobium for Use in SRF Cavities

Studies of superconducting Nb3Sn cavities and samples at Cornell University and Argonne National Lab have shown that current state-of-the-art Nb3Sn cavities are limited by material properties and imperfections. In particular, the presence of regions within the Nb3Sn layer that are deficient in tin are suspected to be the cause of the lower than expected peak accelerating gradient. In this paper we present results from a material study of the Nb3Sn layer fabricated using the vapour deposition method, with data collected using AFM, SEM, TEM, EDX, and XRD methods as well as with pulsed RF testing.

Performance of the Cornell ERL Main Linac Prototype Cryomodule

Cornell has designed, fabricated, and completed initial cool down test of a high current (100 mA) CW SRF main linac prototype cryomodule for the Cornell ERL. This paper will report on the design and performance of this very high Q0 CW cryomodule including design issues and mitigation strategies. INTRODUCTION Cornell University has proposed to build Energy Recovery Linac (ERL) as drivers for hard x-ray sources because of their ability to produce electron bunches with small, flexible cross sections and short lengths at high repetition rates. The proposed Cornell ERL is designed to operate in CW at 1.3GHz, 2ps bunch length, 100mA average current in each of the accelerating and decelerating beams, normalized emittance of 0.3mmmrad, and energy ranging from 5GeV down to 10MeV, at which point the spent beam is directed to a beam stop [1, 2]. The design of main linac prototype cryomodule (MLC) for Cornell ERL had been completed in 2012. The fabrication and testing of MLC components (cavity, high power input coupler, HOM dampers, tuners, etc.,) and assembly of MLC cold mass had been completed in 2014. MLC installation and cooldown preparations began in this summer. We will describe about MLC and initial cool down results in this proceeding. MLC GENERAL LAYOUT The general layout of an ERL main linac cryomodule (MLC) is shown in Fig. 1. It is 9.8 m long and houses six 1.3 GHz 7-cell superconducting cavities with Individual HOM absorbers and one magnet/BPM section. Each cavity has a single coaxial RF input coupler which transfers power from an RF power source to the beam loaded cavity. The specification values of 7-cell cavities are Qo of 2.0e10 at 16.2MV/m, 1.8K. Due to the high beam current combined with the short bunch operation, a careful control and efficient damping of higher order modes (HOMs) is essential. So HOMs are installed next to each cavity. To minimize ambient magnetic field of high-Q 7-cell cavities, MLC has three layers of magnetic shielding; 1) Vacuum Vessel (carbon steel), 2) 80/40 K magnetic shield enclosing the cold mass, and 3) 2 K magnetic shield enclosing individual cavities. All components within the cryomodule are suspended from the Helium Gas Return Pipe (HGRP). This large diameter (280mm) titanium pipe will return the gaseous helium boiled off the cavity vessel to the liquefier and act as a central support girder. The HGRP will be supported by 3 support post. The middle one is fixed; the other side posts are not and will slide by 7-9mm respectively during the cooldown from room temperature to cold. 7-CELL CAVITIES FOR MLC Vertical Test Results All 7-cell cavities for MLC were fabricated in house. Three of six cavities were stiffened cavity and the other three were un-stiffened cavity. Cavity surface preparation recipe consists of bulk Buffered Chemical Polishing (BCP, 140um), degassing (650degC*4days), frequency and field flatness tuning, light BCP (10um), low temperature baking (120degC*48hrs), and HF rinse [3]. Figure 2 shows best Q(E)curve of MLC 7-cell cavities during vertical test (VT) at 1.8K. All 7-cell cavities had surpassed the specification values of Qo=2.0e10 at 16.2MV/m, 1.8K. In fact, average Qo=(3.0±0.3)*1e10 had been achieved during VT at 16.2MV/m, 1.8K. All VT was limited by administrative limit, no radiation or no quench were detected during VT. ____________________________________________ * Work is supported by NSF Grants NSF DMR-0807731 and NSF #ff97@cornell.edu PHY-1002467 Figure 1: Cornell ERL Main Linac Prototype Cryomodule Proceedings of SRF2015, Whistler, BC, Canada FRAA04 SRF Technology Cavity E06-Elliptical performance ISBN 978-3-95450-178-6 1437 C op yr ig ht

Niobium Impurity-Doping Studies at Cornell and CM Cool-Down Dynamic Effect on Q0

As part of a multi-laboratory research initiative on high Q0 niobium cavities for LCLS-II and other future CW SRF accelerators, Cornell has conducted an extensive research program during the last two years on impurity-doping of niobium cavities and related material characterization. Here we give an overview of these activities, and present results from single-cell studies, from vertical performance testing of nitrogen-doped nine-cell cavities, and from cryomodule testing of nitrogen-doped nine-cell cavities. We show that 2K quality factors at 16 MV/m well above the nominal LCLS-II specification of 2.7 × 10 can be reached reliably by nitrogen doping of the RF penetration layer. We demonstrate that the nitrogen furnace pressure is not a critical parameter in the doping process. We show that higher nitrogen doping levels generally result in reduced quench fields, with substantial variations in the quench field between cavities treated similarly. We propose that this can be explained by the reduced lower critical field Hc1 in N-doped cavities and the typical variation in the occurrence of defects on a cavity surface. We report on the results from five cryomodule tests of nitrogen-doped 9-cell cavities, and show that fast cooldown with helium mass flow rates above 2 g/s is reliable in expelling ambient magnetic fields, and that no significant change in performance occurs when a nitrogen-doped cavity is installed in a cryomodule with auxiliary components.