K. Prasad Rao

The formation and control of Laves phase in superalloy 718 welds

Weld heat input/cooling rate (affected by welding process, parameters, technique, tooling, etc.) was found to influence the microstructural characteristics and segregational features in alloy 718 welds, with low heat inputs proving beneficial. Laves phase formed in the interdendritic regions of the weld metals as a result of segregation. The morphology and composition of Laves phase depended strongly on heat input/cooling rate and influenced its response to subsequent homogenization post-weld heat treatment. The various factors affecting the formation and control of Laves phase in alloy 718 welds are highlighted.

Weld microstructure refinement in a 1441 grade aluminium-lithium alloy

Clad 2 mm thick sheets of Russian 1441 grade Al-Li alloys were welded using a gas tungsten arc welding process (GTAW). Comparisons were made between the weld beads obtained under (i) continuous current (CC), (ii) pulsed current (PC), and (iii) arc oscillation (AO) conditions for their macro- and microstructural details. In the case of CC GTAW, sound welds could be produced only under a narrow range of welding parameters. Centre line cracks, which occurred in CC GTAW welds under certain conditions, were halted by switching to PC or AO conditions while the welding was in progress. Microstructural refinement was significant in the case of PC and AO GTA welding.

Control of Laves phase in Inconel 718 GTA welds with current pulsing

AbstractThe presence of Nb rich Laves phase in Inconel 718 weld fusion zones is known to be detrimental to weld mechanical properties. In the present study, an attempt was made to control the formation of Laves phase in alloy 718 gas tungsten arc welds using pulsed current. Welds were produced in 2 mm thick sheets of the alloy with constant current and pulsed current and were subjected to post-weld solution treatment at 980°C followed by aging. Detailed microstructural studies and tensile tests at 650°C were conducted. The results show that the use of current pulsing (i) refines the fusion zone microstructure, (ii) reduces the amount of Laves phase and exerts a favourable influence on its morphology and (iii) improves the response of the fusion zone to post-weld heat treatment and weld tensile properties.Abstract The presence of Nb rich Laves phase in Inconel 718 weld fusion zones is known to be detrimental to weld mechanical properties. In the present study, an attempt was made to control the formation of Laves phase in alloy 718 gas tungsten arc welds using pulsed current. Welds were produced in 2 mm thick sheets of the alloy with constant current and pulsed current and were subjected to post-weld solution treatment at 980°C followed by aging. Detailed microstructural studies and tensile tests at 650°C were conducted. The results show that the use of current pulsing (i) refines the fusion zone microstructure, (ii) reduces the amount of Laves phase and exerts a favourable influence on its morphology and (iii) improves the response of the fusion zone to post-weld heat treatment and weld tensile properties.

Microstructure and Mechanical Properties of Friction Stir Lap Welded Aluminum Alloy AA2014

F riction stir lap welds were produced in 3 mm thick Alclad sheets of Al alloy 2014-T4 using two difierent tools (with triangular and threaded taper cylindrical pins). The efiects of tool geometry on weld microstructure, lap-shear performance and failure mode were investigated. The pin proflle was found to signiflcantly in∞uence the hook geometry, which in turn strongly in∞uenced the joint strength and the failure mode. Welds produced in alloy 2014-T4 Alclad sheets by using triangular and threaded taper cylindrical tools exhibited an average lap-shear failure load of 16.5 and 19.5 kN, respectively, while the average failure load for standard riveted joints was only 3.4 kN. Welds produced in alloy 2014-T6 Alclad sheets and in alloy 2014-T4 bare sheets (i:e:, no Alclad) were comparatively evaluated with those produced in alloy 2014-T4 Alclad sheets. While the welds made (with threaded taper cylindrical tool) in T6 and T4 conditions showed very similar lap-shear failure loads, the joint e‐ciency of the welds made in T6 condition (43%) was considerably lower (because of the higher base material strength) than those made in T4 condition (51%). The Alclad layers were found to present no special problems in friction stir lap welding. Welds made with triangular tool in alloy 2014-T4 Alclad and bare sheets showed very similar lap-shear failure loads. The present work provides some useful insights into the use of friction stir welding for joining Al alloys in lap conflguration.

Microstructure and mechanical properties of Inconel 718 electron beam welds

Abstract Bead on plate, full penetration electron beam welds were produced in 2 mm thickness sheets of Inconel 718 in the solution treated condition. Welds were subjected to an aging treatment with and without post-weld solution treatment. Weld microstructures, high temperature tensile properties and stress rupture properties were evaluated. The as welded fusion zone showed a considerable amount of interdendritic niobium segregation and brittle intermetallic Laves phase. The tensile and stress rupture properties of the welds after post-weld aging treatment were found to be inferior in relation to the base metal. Post-weld solution treatment at 980°C was found to result in partial dissolution of Laves phase, some reduction in niobium segregation and the formation of δ phase needles around the Laves particles. The use of 980°C solution treatment was found to improve the weld properties to some extent, although not to the level of the base metal. The reasons for this behaviour are discussed, correlating microstructures, fracture features and mechanical properties.

Microstructure and mechanical properties of Sc modified Al–Cu alloy (AA2219) electron beam welds

Abstract Al alloy AA2219 is a high strength alloy belonging to the 2000 series Al alloys widely used for aerospace application. One of the drawbacks of most of the high strength Al alloys is that they suffer from poor weldability. However AA2219 is an exception due to the presence of more Cu that helps in healing cracks by providing extra eutectics. Although AA2219 has excellent weldability the strength of a welded joint is only 35–45% of the base metal. The loss of strength is due to the dissolution of the strengthening precipitates during melting. Therefore, there is a need to improve the fusion zone strength of AA2219 welds. In this study an attempt was made experimentally to use electron beam welding and modify the base metal chemistry with addition of Sc and Zr in order to improve the mechanical properties of the AA2219 weld joints. Fine equiaxed microstructure was obtained in the fusion zone of electron beam welds with improved mechanical properties. Eutectic was found to be distributed discontinuously which resulted in improved yield strength, tensile strength and ductility compared to welds made without Sc and Zr.

Observation of high permittivity in Ho substituted BaZr0.1Ti0.9O3 ceramics

The authors observed an extremely high permittivity (∼35000 at TC) in barium zirconate titanate (BaZr0.1Ti0.9O3) ceramics with holmium substitution (1–5mol%) in Ba site. Careful microstructural investigation and energy dispersive spectroscopy analysis of the 1–2mol% of Ho substituted ceramics showed the enrichment of a Ho-phase along the grain boundaries with a composition close to the Ho2Ti2O7 pyrochlore. The formation of Ho rich phase resulted in the Maxwell-Wagner polarization mechanism, which leads to this unusually high permittivity. Ceramics with 3mol% or higher Ho content showed lesser permittivity values compared to 1–2mol%, probably due to the increase in pyrochlore phase. These high dielectric constant ceramics are useful in nanoscale devices.

Microstructures and Mechanical Properties of Friction Stir Spot Welded Aluminum Alloy AA2014

Friction stir spot welding (FSSW) is a relatively recent development, which can provide a superior alternative to resistance spot welding and riveting for fabrication of aluminum sheet metal structures. In the current work, FSSW experiments were conducted in 3-mm thick sheets of aluminum alloy 2014 in T4 and T6 conditions, with and without Alclad layers. The effects of tool geometry and welding process parameters on joint formation were investigated. A good correlation between process parameters, bond width, hook height, joint strength, and fracture mode was observed. The presence of Alclad layers and the base metal temper condition were found to have no major effect on joint formation and joint strength. Friction stir spot welds produced under optimum conditions were found to be superior to riveted joints in lap-shear and cross-tension tests. The prospects of FSSW in aluminum sheet metal fabrication are discussed.

Laves Phase Control in Inconel 718 Weldments

The detrimental laves formation in fusion zone during welding of Inconel 718 is controlled with compound current pulsing technique along with helium shielding gas. Also solid solution filler wire is used to minimize the niobium segregation. Welds were produced in 2mm thick sheets by GTA welding process and subjected to the characterization techniques. The results show, refined fusion zone microstructure, reduced amount of laves phase, minimum niobium segregation and softer fusion zone in the as welded condition.

Improvement of mechanical properties of gas tungsten arc and electron beam welded AA2219 (Al–6 wt-%Cu) alloy

Abstract Despite its excellent weldability characteristics, AA2219 suffers from poor fusion zone strength under the as welded condition. In the present work, it is attempted to increase the mechanical properties of the as welded fusion zone of this alloy by increasing the weld cooling rates and multipass welding. The cooling rate was increased with the use of high intense heat source, namely electron beam in a pulsed current mode. Multipass gas tungsten arc welding was carried out using direct current straight polarity. These techniques resulted in a significant improvement in fusion zone hardness and tensile properties, which is attributed to reduced copper segregation and natural aging as well as aging caused by heat of multipass welding.