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Synthetic Communications | 2012

Facile Synthesis of Functionalized Bis(arylethynyl)benzene Derivatives via Sila–Sonogashira Reaction

Zhang-Lin Zhou; Lihua Zhao; Sean Zhang; Kent D. Vincent; Si-Ty Lam; Dick Henze

Abstract This article describes a facile synthesis of a new series of symmetrical bis(arylethynyl)benzene derivatives via a one-pot coupling reaction between trialkylsilyl protected arylalkynyes and aryldihalides bearing both electron-withdrawing (EW) and electron-donating groups (ED) in the presence of PdCl2(PPh3)2(5%) / CuI/tetrabutylammonium fluoride / triethylamine / tetrahydrofuran (sila–Sonogashira reaction) at room temperature. GRAPHICAL ABSTRACT


Archive | 1990

Colorimeter and calibration system

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Archive | 1991

Variable wavelength light filter and sensor system

Kent D. Vincent


Archive | 1998

Print method and apparatus for re-writable medium

Kent D. Vincent


Archive | 1991

Substrate advance measurement system using cross-correlation of light sensor array signals

John P. Ertel; William D. Holland; Kent D. Vincent; Rueiming Jamp; Richard R. Baldwin


Archive | 1987

Color imager utilizing novel trichromatic beamsplitter and photosensor

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Archive | 1990

Heater assembly for printers

Kent D. Vincent; John P. Ertel


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Heated transfer line for capillary tubing

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Archive | 1989

Color combiner and separator and implementations

Kent D. Vincent; Hans D. Neumann


Archive | 1989

Device to assure paper flatness and pen-to-paper spacing during printing

Kent D. Vincent; John P. Ertel

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