M. N. Mohammed

An Overview of Semisolid Processing of Aluminium Alloys

Semisolid metal processing (SSM) or thixoforming is a new technology that offers several advantages over liquid processing and solid processing. This process utilizes semisolid behavior as well as reduces macrosegregation, porosity, and forming forces during shaping process. A lot of research work has been carried out by various researchers in order to exploit the potential of this process to produce different products especially for automotive industry. This paper will summarise the rheological behavior of aluminium alloys in semisolid slurries, thixoformability of modified aluminium alloys, the effect of feedstock production method on mechanical properties, and the importance of developing low-cost raw materials for semisolid processing.

Semisolid Metal Processing Techniques for Nondendritic Feedstock Production

Semisolid metal (SSM) processing or thixoforming is widely known as a technology that involves the formation of metal alloys between solidus and liquidus temperatures. For the procedure to operate successfully, the microstructure of the starting material must consist of solid near-globular grains surrounded by a liquid matrix and a wide solidus-to-liquidus transition area. Currently, this process is industrially successful, generating a variety of products with high quality parts in various industrial sectors. Throughout the years since its inception, a number of technologies to produce the appropriate globular microstructure have been developed and applied worldwide. The main aim of this paper is to classify the presently available SSM technologies and present a comprehensive review of the potential mechanisms that lead to microstructural alterations during the preparation of feedstock materials for SSM processing.

Study on thixojoining process using partial remelting method

Cold-work tool steel is considered to be a nonweldable metal due to its high percentage content of carbon and alloy elements. The application of a new process of the semisolid joining of two dissimilar metals is proposed. AISI D2 cold-work tool steel was thixojoined to 304 stainless steel by using a partial remelting method. After thixojoining, microstructural examination including metallographic analysis, energy dispersive spectroscopy (EDS), and Vickers hardness tests was performed. From the results, metallographic analyses along the joint interface between semisolid AISI D2 and stainless steel showed a smooth transition from one to another and neither oxides nor microcracking was observed. Hardness values obtained from the points in the diffusion zone were much higher than those in the 304 stainless steel but lower than those in the AISI D2 tool steel. The study revealed that a new type of nonequilibrium diffusion interfacial structure was constructed at the interface of the two different types of steel. The current work successfully confirmed that avoidance of a dendritic microstructure in the semisolid joined zone and high bonding quality components can be achieved without the need for force or complex equipment when compared to conventional welding processes.

Microstructural evolution during DPRM process of semisolid ledeburitic D2 tool steel

Semisolid metal processing is a relatively new technology that offers several advantages over liquid processing and solid processing because of the unique behaviour and characteristic microstructure of metals in this state. With the aim of finding a minimum process chain for the manufacture of high-quality production at minimal cost for forming, the microstructural evolution of the ledeburitic AISI D2 tool steel in the semisolid state was studied experimentally. The potential of the direct partial remelting (DPRM) process for the production of AISI D2 with a uniform globular microstructure was revealed. The liquid fraction was determined using differential scanning calorimetry. The microstructures of the samples were investigated using an optical microscope and a scanning electron microscope equipped with an energy dispersive spectroscopy analyser, while X-ray phase analysis was performed to identify the phase evolution and the type of carbides. Mechanical characterisation was completed by hardness measurements. The typical microstructure after DPRM consists of metastable austenite which was located particularly in the globular grains (average grain size about 50 μm), while the remaining interspaces were filled by precipitated eutectic carbides on the grain boundaries and lamellar network.

Evolution of Globular Microstructures during Direct Partial Re-Melting Experiment of AISI D2 Tool Steel

Steel is a mostly challenging metal to semisolid process because of the high temperatures implicated and the prospective for surface oxidation. Slurry processing experiment was performed with AISI D2 cold work tool steel to identify the evolution of globular microstructures via Direct Partial Re-Melting Method (DPRM). Samples were heated in an argon atmosphere up to 1330°C which corresponded to about 38% of liquid fraction and held for 5 minutes. The typical microstructure after DPRM consists of globular grains (average grain size about 50μm) while the remaining interspaces were filled by precipitated eutectic carbides on the grain boundaries and lamellar network. Based on the requirements of thixoformability, the current work confirms the suitability of the AISI D2 cold work tool steel as a candidate material for semi-solid forming.

Semi-Solid Joining of D2 Cold-Work Tool Steel

Cold-work tool steel is considered to be a non-weldable metal due to its high percentage content of carbon and alloying elements. To address this problem the application of a new process of semisolid joining using a direct partial remelting method was developedto achieve a spherical join structure between two parts of AISI D2 cold-work tool steel. Since the surface oxidation of this metalis very high, the control of the atmosphere during joining had to be considered. Samples were heated in an argon atmosphere at two different temperatures of 1250°C and 1275°C for 10 minutes. Metallographic analyses along the joint interface showed that an increase in temperature promoted the final joining properties and also that at a liquid fraction of 15% joining was not fully practicable. However, a20% liquid fraction can produce a very good joint and microstructure as compared to the other experimental liquid fraction. Metallographic analyses along the joint interface showed a smooth transition from one to the other and neither oxides nor microcracking was observed. The current work confirmed that avoidance of a dendritic microstructure in the semisolid joined zone and high bonding quality components can be achieved without the need for force or complex equipment when compared to conventional welding processes.

Effects of Cu on the Microstructures and Tensile Properties of Thixoformed Al-Si Alloys

In this study, the effects of copper content on the microstructures and tensile properties of thixoformed Al-5Si-xCu-0.5Fe (x =1.0, 2.0 and 3.0 wt. %) were investigated. For this study, three different alloys having various amounts of copper were prepared using cooling slope casting before thixoforming. The semi-solid liquid range for the alloys were estimated using the diffrential scanning calorimetry (DSC) analysis. The samples were thixoformed at 40% liquid fraction. Some of these samples were treated with a T6 aging process. The thixoformed and thixoformed T6 samples were then characterized by optical microscopy, scanning electron microscope (SEM) and energy dispersive X-ray (EDX) as well as tensile tests. The different phases formed in the thixoformed and thixoformed T6 samples were throughly investigated.The results indicate that as copper content increases, the tensile strength also increases, which might due to precipitation hardening. The thixoformed T6 alloys attained an ultimate tensile strength (UTS) as high as 303 MPa when Cu content is 3 wt%.

A Study of Microstructure Properties of AISI D2 Tool Steel in Partial Re-Melting Method

Due to the growing demand for cold-work tool steel in various industrial applications, it is crucial to improve the fabrication technique, because complex shapes involve an extensive and costly workshop effort. Hence, a one-step net-shaping process, such as the semi-solid forming, could offer great benefits. With the aim of finding a minimum process chain for the manufacturing of a high-quality production, the microstructural evolution of the ledeburitic AISI D2 tool steel in the semi-solid-state was studied experimentally via the Direct Partial Re-Melting Method (DPRM). Samples were heated in an argon atmosphere up to 1255°C, which corresponded to about 16% of liquid fraction, and held for 0 minute. The microstructural observation after DPRM showed that the equiaxed austenite grains are observable within a small liquid matrix. The microstructure also contains primary, non-dissolved carbides with a new, precipitated eutectic.

The interface morphology of thixo-joined cold work tool steel

Cold-work tool steel is considered to be a nonweldable metal due to its high percentage content of carbon and alloying elements. The application of a new process of the semi-solid joining of two parts of AISI D2 cold-work tool steel is proposed using a partial remelting method. Samples were heated in an argon atmosphere up to 1275°C which corresponded to about 20% of liquid fraction and held for 10 minutes. Metallographic analyses along the joint interface showed a smooth transition from one to the other and neither oxides nor micro-cracking was observed. The current work successfully confirmed that avoidance of a dendritic microstructure in the semi-solid joined zone and high bonding quality components can be achieved without the need for force or complex equipment when compared to conventional welding processes.