María Parra-Borderías

EURECA - A European-Japanese micro-calorimeter array

The EURECA (EURopean-JapanEse Calorimeter Array) project aims to demonstrate the science performance and technological readiness of an imaging X-ray spectrometer based on a micro-calorimeter array for application in future X-ray astronomy missions, like Constellation-X and XEUS. The prototype instrument consists of a 5 × 5 pixel array of TES-based micro-calorimeters read out by by two SQUID-amplifier channels using frequency-domain-multiplexing (FDM). The SQUID-amplifiers are linearized by digital base-band feedback. The detector array is cooled in a cryogenfree cryostat consisting of a pulse tube cooler and a two stage ADR. A European-Japanese consortium designs, fabricates, and tests this prototype instrument. This paper describes the instrument concept, and shows the design and status of the various sub-units, like the TES detector array, LC-filters, SQUID-amplifiers, AC-bias sources, digital electronics, etc. Initial tests of the system at the PTB beam line of the BESSY synchrotron showed stable performance and an X-ray energy resolution of 1.58 eV at 250 eV and 2.5 eV @ 5.9 keV for the read-out of one TES-pixel only. Next step is deployment of FDM to read-out the full array. Full performance demonstration is expected mid 2009.

Size and dimensionality effects in superconducting Mo thin films

Molybdenum is a low Tc, type I superconductor whose fundamental properties are poorly known. Its importance as an essential constituent of new high performance radiation detectors, the so-called transition edge sensors (TESs) calls for better characterization of this superconductor, especially in thin film form. Here we report on a study of the basic superconducting features of Mo thin films as a function of their thickness. The resistivity is found to rise and the critical temperature decreases on decreasing film thickness, as expected. More relevant, the critical fields along and perpendicular to the film plane are markedly different, thickness dependent and much larger than the thermodynamic critical field of Mo bulk. These results are consistent with a picture of type II 2D superconducting films, and allow estimates of the fundamental superconducting lengths of Mo. The role of morphology in determining the 2D and type II character of the otherwise type I molybdenum is discussed. The possible consequences of this behaviour on the performance of radiation detectors are also addressed.

Effects of Stress and Morphology on the Resistivity and Critical Temperature of Room-Temperature-Sputtered Mo Thin Films

We report on the structural and electrical characterization of Mo thin films deposited at room temperature by RF magnetron sputtering. The effect of RF power on the morphology and residual stress of the films is analyzed. The films are under compressive stress and consist of densely packed columns with a lateral size on the order of 20 nm. The stress, critical temperature, and resistivity of the films are found to rise when increasing the ejected ion energy during the sputtering process. The changes in critical temperature and resistivity are discussed in terms of the observed morphology and stress changes.

Mo-Based Proximity Bilayers for TES: Microstructure and Properties

We report on the fabrication and characterization of Mo films, Mo/Au and Mo/Cu bilayers for Transition Edge Sensors (TES). The fabrication conditions (at room temperature) have been varied to achieve layers with the required properties for TES applications. The dependence of their functional properties (i.e. electrical resistivity and superconducting critical temperature) on microstructure (grain size, stress) is investigated.

Transition Edge Sensors (TES) Using a Low-G Spider-Web-Like SiN Supporting Structure

We fabricated and characterized a low thermal conductance (G) transition edge sensor (TES). The device is based on a superconducting Ti/Au bilayer deposited on a suspended SiN membrane. The critical temperature of the device is 155 mK. The low thermal conductance is realized by using narrow SiN ring-like supporting structures. All measurements were performed having the device in a light-tight box, which to a great extent eliminates the loading of the background radiation. We measured the current-voltage (IV) characteristics of the device in different bath temperatures and determine the thermal conductance (G) to be equal to 1.66 pW/K. This value corresponds to a noise equivalent power (NEP) of 1×10-18 W/√Hz. The current noise and complex impedance are also measured at different bias points at 25 mK bath temperature. The measured electrical (dark) NEP is 2×10-18 W/√Hz, which is about a factor of 2 higher than what is expected from the thermal conductance that comes out of the IV curves analysis. We also measured the complex impedance of the same device at several bias points. Fitting a simple first order thermal-electrical model to the measured data, we find an effective time constant of about 62 μs and a thermal capacity of 3 fJ/K.

Low-noise transition edge sensor (TES) for SAFARI instrument on SPICA

Transition edge sensor (TES) is the selected detector for the SAFARI FIR imaging spectrometer (focal plane arrays covering a wavelength range from 30 to 210 μm) on the Japanese SPICA telescope. Since the telescope is cooled to <7 K, the instrument sensitivity is limited by the detector noise. Therefore among all the requirements, a crucial one is the sensitivity, which should reach an NEP (Noise Equivalent Power) as low as 3E-19 W/Hz^0.5 for a base temperature of >50 mK. Also the time constant should be below 8 ms. We fabricated and characterized low thermal conductance transition edge sensors (TES) for SAFARI instrument on SPICA. The device is based on a superconducting Ti/Au bilayer deposited on suspended SiN membrane. The critical temperature of the device is 155 mK. The low thermal conductance is realized by using narrow SiN ring-like supporting structures. All measurements were performed having the device in a light-tight box, which to a great extent eliminates the loading of the background radiation. We measured the current-voltage (IV) characteristics of the device in different bath temperatures and determine the thermal conductance (G) to be equal to 1.66 pW/K. This value corresponds to a noise equivalent power (NEP) of 1E-18 W/√Hz. The current noise and complex impedance is also measured at different bias points at 25 mK bath temperature. The measured electrical (dark) NEP is 2E-18 W/√Hz, which is about a factor of 2 higher than what we expect from the thermal conductance that comes out of the IV curves. Despite using a light-tight box, the photon noise might still be the source of this excess noise. We also measured the complex impedance of the same device at several bias points. Fitting a simple first order thermal-electrical model to the measured data, we find an effective time constant of about 65 μs and a thermal capacity of 3-4 fJ/K in the middle of the transition

Characterization of a Mo/Au Thermometer for ATHENA

The first dark characterization of a thermometer fabricated with our Mo/Au bilayers to be used as a transition edge sensor is presented. High-quality, stress-free Mo layers, whose thickness is used to tune the critical temperature (<i>T</i>_C) down to 100 mK, are deposited by sputtering at room temperature (<i>RT</i>) on Si₃N₄ bulk and membranes, and protected from degradation with a 15-nm sputtered Au layer. An extra layer of high-quality Au is deposited by ex situ e-beam to ensure low residual resistance. The thermometer is patterned on a membrane using standard photolithographic techniques and wet etching processes, and is contacted through Mo paths, displaying a sharp superconducting transition (α ≈ 600). Results show a good coupling between Mo and Au layers and excellent <i>T</i>_C reproducibility, allowing to accurately correlate <i>d</i>_Mo and <i>T</i>_C. Since <i>d</i>_Au is bigger than ξ_M for all analyzed samples, bilayer residual resistance can be modified without affecting <i>T</i>_C . Finally, first current to voltage measurements at different temperatures are measured and analyzed, obtaining the corresponding characterization parameters.

Thermal stability of Mo/Au bilayers for TES applications

Mo/Au bilayers are among the most suitable materials to be used as transition-edge sensors (TES) in cryogenic microcalorimeters and bolometers, developed, among other fields, for space missions. For this purpose the thermal stability of TES at temperatures below 150 °C is a critical issue. We report on the dependence of functional properties (superconducting critical temperature, residual resistance and α) as well as on microstructure, chemical composition and interface quality for optimized high quality Mo/Au bilayers on annealing temperature and time. Data show that the functional properties of the bilayers remain stable at T < 150 °C, but changes in microstructure, interface quality and functional properties were observed for layers heated at T ≥ 200 °C. Microstructural and chemical composition data suggest that the measured changes in residual resistance ratio (RRR) and TC at T ≥ 200 °C are mainly due to an increase in the average Au grain size and to Au migration along the Mo grain boundaries at the Au/Mo interface. A way to stabilize the functional properties of the Mo/Au bilayers against temperature enhancements is proposed.

Negative magnetization in NdFexGa1-xO3 studied by XMCD

Negative Magnetization (NM) in NdFe0.8Ga0.2O3 is reported, both by magnetization, ac-susceptibility and x-ray Magnetic Circular Dichroism measurements. The mechanism of NM in NdFe0.8Ga0.2O3 is the blocking of the weak-ferromagnetic domain walls and the polarization of the paramagnetic Nd sublattice by that of Fe at low temperatures.