Marjan Sedighi Gilani

Hygric properties of Norway spruce and sycamore after incubation with two white rot fungi

Abstract In this study, changes in the hygroscopic properties of two main wood species for violin making, Norway spruce and sycamore, after treatment with Physisporinus vitreus and Xylaria longipes were investigated. Swelling and moisture sorption capacity of wood at the growth ring scale were visually and quantitatively assessed by thermal neutron radiography analysis. It was demonstrated that the fungal treatment improved the dimensional stability of both Norway spruce and sycamore, but also increased their moisture adsorption capacity. Dynamic vapor sorption tests and measurements of the changes in dimensions of the specimens in the laboratory were in good agreement with the results of neutron radiography analysis. The main difference between the moisture sorption of the untreated controls and treated wood was observed at high relative humidity, e.g., above 75%. The contradictory behavior of the increased hygroscopicity and reduced swelling was explained by selective degradation of the chemical components and condensation of the moisture content gained in the capillary voids that developed in the cell walls during fungal decay.

Investigation of Water Uptake in Porous Asphalt Concrete Using Neutron Radiography

Porous asphalt (PA), a highly porous hydrophobic composite material, is subjected to water uptake and the process is documented with neutron radiography (NR). While the un-aged laboratory-prepared PA specimens do not show any water uptake, we observe uptake in aged PA even though the bitumen binder is a hydrophobic material. The moisture content distribution plots derived from the NR images clearly identify regions in the aged specimens where water uptake is active. Two-dimensional degree of saturation (DoS) distribution images, which are obtained by combining micro-computer tomography and NR images, identify those pores where saturated flow is certainly active. However, to clearly distinguish between saturated and unsaturated flows in the remaining wet pores, the DoS distribution images are read together with the three-dimensional PA microstructure obtained by micro-CT. It is observed that uptake begins mainly as unsaturated film/corner flow at large well-defined pores. As this uptaken water travels further into the material, the flow transforms into a combination of saturated flow and unsaturated film/corner flow. Saturated flow is seen to be mostly active in the small pores within the mastic. From the observed succession of unsaturated and saturated flows in an aged PA specimen, it can be concluded that years of environmental and mechanical loading has resulted in the stripping of binder from the aggregate surfaces and has consequently exposed patches of hydrophilic aggregate to water, which enables the capillary uptake of water. We also simulate an absolute permeability experiment and observe that relatively less tortuous and more connected paths play an important role in determining the preferential path of the uptaken water.

Synchrotron X-ray micro-tomography imaging and analysis of wood degraded by Physisporinus vitreus and Xylaria longipes.

Incubation of Norway spruce with Physisporinus vitreus and sycamore with Xylaria longipes results in reduction in density of these wood species that are traditionally used for the top and bottom plate of a violin, which follows by enhanced acoustic properties. We used Synchrotron X-ray micro-tomography, to study the three-dimensional structure of wood at the micro-scale level and the alterations of the density distribution after incubation with two white-rot fungi. Micro-tomography data from wood treated at different incubation periods are analyzed and compared with untreated (control) specimens to determine the wood density map and changes at the cell-wall level. Differences between the density of early- and latewood, xylem ray and around bordered pits in both Norway spruce and sycamore are studied. Three-dimensional hyphal networks of the P.vitreus and Xylaria longipes hyphae are visualized inside the cell lumina and their significance on the density of the early- and latewood cells after different incubation periods are discussed. The study illustrates the utility of X-ray micro-tomography for both qualitative and quantitative studies of a wide variety of biological systems and due to its high sensitivity, small structural changes can be quantified.

Dynamics of microcrack propagation in hardwood during heat treatment investigated by synchrotron-based X-ray tomographic microscopy

The process of crack propagation in wood during pyrolysis is strongly linked to heterogeneities in its hierarchical porous structure. Fundamental understanding of this process is necessary for the analysis of the behavior of wood structural elements during fire exposure. Synchrotron-based X-ray tomographic microscopy combined with a recently developed laser-based furnace at the TOMCAT beamline of the Swiss Light Source provides a unique opportunity to study the heat-induced propagation of microcracks in hardwood in situ with high spatial and temporal resolutions. In this study, attention was focused on the 3D microstructure of beech and the interconnectivity between morphology and cracking patterns. It is shown that thermal cracks initiate mainly along the ray cells in hardwood and in the junction of seasonal growth layers. There is a clear indication of increased total porosity of the wood due to charring.

A hygrothermo-mechanical model for wood: part A. Poroelastic formulation and validation with neutron imaging

Abstract The correct prediction of the behavior of wood components undergoing environmental loading or industrial process requires that the hygrothermal and mechanical (HTM) behavior of wood is considered in a coupled manner. A fully coupled poromechanical approach is proposed and validated with neutron imaging measurements of moist wood specimens exposed to high temperature. This paper demonstrates that a coupled HTM approach adequately captures the variations of temperature, moisture content, and dimensions that result in a moist wood sample exposed to one-side heating.

Transport of Polar and Nonpolar Liquids in Softwood Imaged by Neutron Radiography

The influence of the moisture capacity of cell walls on liquid transport in wood is studied using neutron imaging in combination with precision weighing. The time-dependent and spatial distribution of two liquids, one polar, water, and one nonpolar, decane, is documented during liquid uptake in the three orthotropic directions for samples of three softwood species: spruce and fir heartwood, and pine sapwood. Polar and nonpolar liquid uptake versus time is compared, the spatial distribution of the liquids within the samples is discussed, and the liquid volume and swelling profiles along the height of the samples are described in details. Water uptake is shown to be slower than decane uptake, due to water being adsorbed by the cells walls. Decane, due to its very low contact angle and high wettability compared to water, does not face much resistance from wood cellular features.

Influence of incubation time on the vibration and mechanic properties of mycowood

Abstract The goal of the current study was to investigate the physical and mechanical properties of mycowood as a high quality tone-wood, obtained from Norway spruce by treatment of the white rot fungus Physisporinus vitreus as a function of the treatment time. In focus was the stiffness to weight ratio, which is often considered a main criterion for tone-wood selection. The vibro-mechanical properties were tested by non-destructive methods. The change of color and density were also measured after 4–12 months of fungal incubation. Density decreased up to 5% after 12 months of fungal treatment. Sound velocity was measured in small size specimens by means of the free-free vibration approach, while in large specimens the air-coupled ultrasound method was applied. The two techniques gave similar results and indicated that the sound velocity decreased in mycowood. Internal damping was increased in mycowood to a higher extent than the reduction in the specific modulus of elasticity (E/ρ) and thus the sound velocity in the material. The sound velocity was decreasing with increasing incubation times and scattering of data with this regard was larger in the transversal than in the longitudinal direction. The sound radiation coefficient and the characteristic impedance were enhanced in mycowood and its color was more brownish and richer in tone.

Combined Experimental and Numerical Investigation of Vibro-Mechanical Properties of Varnished Wood for Stringed Instruments

The obvious purpose of varnishing a stringed instrument is the protection against wear and relative humidity changes as well as enhancing its aesthetic appearance. Besides, it is known that varnishing changes the acoustic properties of the wood [1]. Unlike studies on the chemical compositions of old varnishes, in searching for the “secret” of well-known historical instruments [2], the vibro-mechanical properties of varnished wood have been less studied. Nevertheless, the vibrational and mechanical properties of wood are influenced after varnishing [3]. Vibrational experiments show that varnishing changes the specific stiffness and internal damping of wood. Therefore, varnishing also influences acoustic properties that are commonly used to evaluate the sound quality of an instrument such as speed of sound, characteristic impedance, sound radiation coefficient and emission ratio.