Martin Leich

Efficient Yb laser fibers with low photodarkening by optimization of the core composition

We report on photodarkening (PD) investigations at Yb doped fibers with specific variation of the concentrations of the codopants aluminum and phosphorus, measured during cladding pumping at 915 nm. A core composition with equal content of Al and P is most promising to achieve Yb fibers with low PD, high laser efficiency and low numerical aperture of the laser core despite of high codoping. A laser output power of more than 100 W was demonstrated on such a fiber with a slope efficiency of 72%. The correlation of the PD loss with the NIR-excited cooperative luminescence encourages the supposition that cooperative energy transfer from excited Yb(3+) ions to the atomic defect precursors in the core glass enables the formation of color centers in the pump-induced PD process.

Highly efficient Yb-doped silica fibers prepared by powder sinter technology

We report on the characteristics of an active fiber with core material made by sintering of Yb-doped silica powders as an alternative to a conventional modified chemical vapor deposition (MCVD) technique. This material provides the possibility to design very large and homogenously rare-earth doped active fiber cores. We have determined a fiber background attenuation of 20 dB/km and measured a slope efficiency of 80%. These values are comparable to established fibers made by MCVD technology.

Photodarkening kinetics as a function of Yb concentration and the role of Al codoping

We investigated the photodarkening (PD) kinetics of two fiber series with variation of the Yb content for constant Al concentration or constant ratio of Al/Yb, respectively. The results show the outstanding importance of the absolute value of Al concentration also in the case of fibers with strongly reduced Yb content. An Al/Yb ratio of 5 to 6 is not sufficient to mitigate PD loss. Moreover, a model to describe PD loss and rate constant as functions of Yb concentration and excitation is suggested that links measurements of PD in single fibers of the same type (variation of Yb inversion) and in fiber series (constant Yb inversion).

Non-isothermal bleaching of photodarkened Yb-doped fibers.

We report on the thermal treatment of photodarkened Yb-doped fiber samples. The method of non-isothermal bleaching at different temperature ramp rates can be used to determine the thermal energy distribution of photodarkening induced color centers. A distributed activation energy with a mean value of about 1.3 eV and a FWHM of 0.5 eV was found. Spectral changes during thermal treatment were observed and could be interpreted, e.g. as an enhancement of the absorption cross section.

A highly efficient Yb-doped silica laser fiber prepared by gas phase doping technology

In this paper we report on an alternative technique for the preparation of ytterbium (Yb)-doped silica fibers and their characteristics compared to the conventional modified chemical vapor deposition (MCVD) process in combination with solution doping and powder sinter technology (REPUSIL). In the case of the technique applied here, the active core diameter in the preform can be significantly increased via the deposition of Yb and the most important codopant, aluminum (Al), in the gas phase through the high-temperature evaporation of the Yb chelate compound and Al chloride in the MCVD process. The prepared preform shows a homogenous distribution of the refractive index and dopant concentration. The background loss of the drawn fiber was measured to be 25 dB km−1 at 1200 nm. Efficient lasing up to 200 W, showing a slope efficiency of about 80%, was demonstrated, which is comparable to fibers made via MCVD/solution doping and the REPUSIL technique.

Influence of Tm- or Er-codoping on the photodarkening kinetics in Yb fibers

We investigated photodarkening (PD) parameters of Yb/Al-doped silica fibers as a function of the concentration of additional rare earth ions like Tm or Er. It was found that both Tm and Er cause a decrease in Yb inversion followed by a reduction of PD in the case of Er, whereas Tm-codoping with more than 10 mol-ppm can strongly accelerate the process and also increase the PD loss. However, contrary to [1], we conclude that the typical PD behavior of Yb/Al fibers is an intrinsic feature of this fiber type and not caused by trace impurities of Tm (< 1 mol-ppm) unintentionally incorporated by the raw materials during fiber preparation.

High power laser fiber fabricated through vapor phase doping of Ytterbium

We present the characteristics of an ytterbium-doped alumino-silicate fiber, fabricated through vapor phase doping of aluminum and ytterbium in the core, along with silica and in conjunction with the modified chemical vapor deposition process. The vapor phase doping of rare-earths provides the opportunity to fabricate large core active fibers with a uniform distribution of dopants. The fibers fabricated exhibited low OH− content, negligible center dip and good optical properties. Lasing performance was tested up to output power of 105 W, with a slope efficiency of 77% with respect to launched pump power. The linear variation of the laser power with a pump shows its potentiality for further power scaling.

Multi-kW single fiber laser based on an extra large mode area fiber design

The quality of Yb-doped fused bulk silica produced by sintering of Yb-doped fused silica granulates has improved greatly in the past five years [1 - 4]. In particular, the refractive index and doping level homogeneity of such materials are excellent and we achieved excellent background fiber attenuation of the active core material down to about 20 dB/km at 1200 nm. The improvement of the Yb-doped fused bulk silica has enabled the development of multi-kW fiber laser systems based on a single extra large multimode laser fiber (XLMA fiber). When a single active fiber is used in combination with the XLMA multimode fiber of 1200 μm diameter simple and robust high power fiber laser setups without complex fiber coupling and fiber combiner systems become possible. In this papper, we will discuss in detail the development of the core material based on Yb-doped bulk silica and the characterization of Yb-doped fibers with different core compositions. We will also report on the excellent performance of a 4 kW fiber laser based on a single XLMA-fiber and show the first experimental welding results of steel sheets achieved with such a laser.

Role of Ce in Yb/Al laser fibers: prevention of photodarkening and thermal effects.

We report on detailed investigations of ytterbium (Yb) and aluminum (Al) doped silica fiber and preform samples co-doped with cerium (Ce). The prevention of pump-induced photodarkening (PD) by temporary oxidation of Ce3+ to Ce4+ (or rather Ce3++) was proved by observed modifications in the ultraviolet (UV) spectra of transient absorption during near-infrared (NIR) pumping of thin preform slices. Only a small part of available Ce3+ ions (< 4%) was found to be involved in this process despite Yb inversions of up to 0.28. The modifications in the UV absorption spectra disappeared completely when the pump power was switched-off. From these observations we conclude that the recombination to Ce3+ takes place very fast thereby enabling these ions to capture liberated holes h+ perpetually during further pumping. We found a concentration ratio of Ce/Yb ≈0.5 to be sufficient to reduce PD loss to 10% in comparison to Ce-free fibers. Thus, the thermal load caused by absorption of PD color centers at pump (and laser) wavelength is expected to be also reduced. Unfortunately, new heat sources arise with the presence of Ce which cannot be explained by the absorption of Ce ions at the pump wavelength but must be attributed to the interaction with excited Yb ions. Fiber temperature increase of more than 200 K was observed if both, Yb2O3 and Ce2O3 concentration exceed 0.4 mol%.

Very large mode area ytterbium fiber amplifier with aluminum-doped pump cladding made by powder sinter technology

We demonstrate amplification experiments using a very large mode area Yb-doped double-clad fiber with 100 µm aluminum-cer codoped core and 440 µm pump cladding realized by high aluminum codoping. The material for core and pump cladding was fabricated by reactive powder sinter technology. A high numerical aperture (NA) of the pump cladding with NA = 0.21 and a low one of the core with NA = 0.084 could be realized. Using a 0.55 m short fiber sample as the main amplifier in a three-stage ns pulsed fiber master oscillator power amplifier system we achieved 3 ns, 2 mJ output pulses with 360 kW peak power limited by the available pump power. Stimulated Raman scattering effects and amplified spontaneous emission were successfully suppressed.