Mateusz Smietana

Detection of bacteria using bacteriophages as recognition elements immobilized on long-period fiber gratings

The paper presents for the first time a study of long-period gratings (LPGs) applied for label-free detection of specific bacteria using physically adsorbed bacteriophages. For the purposes of the experiment a number of highly sensitive LPGs working at the turning point of phase matching curve was fabricated in SMF28 fiber using UV exposure. We show that the device allows for real-time monitoring of phenomena taking place on the sensors surface, including phage-bacteria interactions. For the applied conditions a resonance wavelength shift of ~1.3 nm induced by bacteria binding was observed.

Increasing sensitivity of arc-induced long-period gratings—pushing the fabrication technique toward its limits

This paper presents an investigation of the sensing properties of long-period gratings (LPGs) written with the electric-arc technique in commonly used standard germanium-doped Corning SMF28 and boron co-doped Fibercore PS1250/1500 fibers. In order to increase the sensitivity of the LPGs, we studied and established for each fiber the writing parameters allowing for the coupling of the highest possible order of cladding modes at a resonance wavelength around λ = 1550 nm. The sensitivity of the LPGs to refractive index, to temperature and to hydrostatic pressure was investigated. The experimental results were supported by extensive numerical simulations. Thanks to the well-established and precisely controlled arc-writing process, we were able to reduce the minimum period of the gratings down to 345 and 221 µm, respectively, for LPGs based on the SMF28 and PS1250/1500 fibers. To the best of our knowledge, these are the shortest periods ever achieved for these fibers using the arc-manufacturing technique. The pressure sensitivities of 13 and 220 pm bar−1 are the highest ever measured for LPGs written in the SMF28 and PS1250/1500 fibers, respectively. Moreover, a reduction in the diameters of the SMF28 fiber induced by the arc was found, which significantly affected the distribution of resonances generated by the coupled cladding modes.

Label-free sensitivity of long-period gratings enhanced by atomic layer deposited TiO 2 nano-overlays

In this paper, we discuss an impact of thin titanium dioxide (TiO(2)) coatings on refractive index (RI) sensitivity and biofunctionalization of long-period gratings (LPGs). The TiO(2) overlays on the LPG surfaces have been obtained using atomic layer deposition (ALD) method. This method allows for a deposition of conformal, thickness-controlled, with well-defined optical properties, and high-RI thin films which are highly desired for optical fiber sensors. It has been found that for LPGs working at a dispersion turning point of higher order cladding modes only tens of nanometers of TiO(2) overlay thickness allow to obtain cladding mode transition effect, and thus significant improvement of RI sensitivity. When the TiO(2) overlay thickness reaches 70 nm, it is possible to obtain RI sensitivity exceeding 6200 nm/RIU in RI range where label-free sensors operate. Moreover, LPGs with TiO(2)-enhanced RI sensitivity have shown improved sensitivity to bacteria endotoxin (E. coli B lipopolysaccharide) detection, when TiO(2) surface is functionalized with endotoxin binding protein (adhesin) of T4 bacteriophage.

Refractive index sensing of fiber optic long-period grating structures coated with a plasma deposited diamond-like carbon thin film

Long-period grating (LPG) structures including cascaded LPGs on step index fibers and photonic crystal fibers were coated with thin films of diamond-like carbon (DLC) using plasma deposition techniques. Improvements in the coating procedures increased sensitivity to external refractive index variations indicating significant improvements in sensing capability of the hybrid structures. DLC films in the range of tens of nanometers significantly increased sensitivity of all the structures tested.

Tuned Pressure Sensitivity of Dual Resonant Long-Period Gratings Written in Boron Co-Doped Optical Fiber

This paper presents a pressure sensor based on a long-period grating (LPG) written in boron co-doped photosensitive fiber and operating at the phase-matching turning point. It is shown that the pressure sensitivity can be tuned by varying the UV exposure time during the LPG fabrication process as well as by varying ambient temperature during pressure measurements. The achieved pressure sensitivity in certain pressure range can reach over 1 nm·bar- 1, and is at least four times higher than for previously presented gratings working away from the double-resonance regime. In terms of an intensity-based measurement, the sensitivity at the turning point can reach 0.212 dB ·bar - 1.

Comparative study of long-period gratings written in a boron co-doped fiber by an electric arc and UV irradiation

The paper presents for the first time a comparative study of long-period gratings (LPGs) written by point-by-point UV irradiation and by electrical arc discharges. These gratings were inscribed in a highly photosensitive boron co-doped fiber that can be considered as a suitable platform for LPG writing using either technology. The experimental transmission data for the manufactured LPG devices fit well when compared to the simulations we carried out in parallel. As a result of each of these writing processes, we were able to obtain a remarkably good quality of grating. Two reasons could explain the observed small differences between the spectra: a slight mismatch of the period of the gratings and an unintentional tapering of the fiber during the arc-based processes. We also found that the UV irradiation at λ = 248 nm can cause clearly visible damage to the fibers surface. As a result of the UV writing, a coupling to the asymmetrical cladding modes can take place. Moreover, the gratings written using the two technologies show a very similar refractive index and temperature-sensing properties. The only differences between them can come from a physical deformation of the fiber induced by the electric arc discharges.

Refractive-Index Sensing With Inline Core-Cladding Intermodal Interferometer Based on Silicon Nitride Nano-Coated Photonic Crystal Fiber

This paper presents a modification of the refractive-index (RI) response of an intermodal interferometer based on photonic crystal fiber (PCF) using a thin plasma-deposited silicon nitride (SiNx) overlay with a high refractive index. We show that the film overlay can effectively change the distribution of the cladding modes and thus tune the RI sensitivity of the interferometer. Thanks to the nano-coating we were able to increase the RI sensitivity eightfold in the range required for biosensors (nD ~ 1.33). Due to the extreme hardness of SiNx films and their excellent adhesion to the fiber surface, we believe that after the film deposition the device will still maintain its advantages, i.e., lack of degradation over time or with temperature.

Temperature sensitivity of silicon nitride nanocoated long-period gratings working in various surrounding media

This paper presents the temperature sensing properties of a silicon nitride (SiNx) nanocoated long-period grating (LPG). A high-temperature, radio-frequency plasma-enhanced chemical-vapor-deposited SiNx nanocoating was applied to tune the external refractive index (RI) sensitivity of LPGs written with UV and electric arc techniques in boron co-doped and standard germanium doped fibers, respectively. The technique allows for deposition of good quality, hard and wear-resistant nanofilms as are required for optical sensors. Thanks to the high-RI SiNx nanocoating, which is less than 90 nm thick, it is possible to reduce RI sensitivity over a wide range (from nD = 1.333 to 1.479), simultaneously decreasing its cross-sensitivity to temperature. For the presented nanocoated LPGs, the temperature effect on resonance wavelength is linear and slightly dependent on the thermo-optic coefficient of the surrounding liquid. The other advantage of the nanocoating is that it makes the resonance clearly visible in the whole investigated external RI range. To the best of our knowledge, this work presents for the first time a nanocoating able to simultaneously tune the RI sensitivity and enable temperature measurements in high-RI liquids applied to LPGs.

Pressure sensing in high-refractive-index liquids using long-period gratings nanocoated with silicon nitride.

The paper presents a novel pressure sensor based on a silicon nitride (SiNx) nanocoated long-period grating (LPG). The high-temperature, radio-frequency plasma-enhanced chemical-vapor-deposited (RF PECVD) SiNx nanocoating was applied to tune the sensitivity of the LPG to the external refractive index. The technique allows for deposition of good quality, hard and wear-resistant nanofilms as required for optical sensors. Thanks to the SiNx nanocoating it is possible to overcome a limitation of working in the external-refractive-index range, which for a bare fiber cannot be close to that of the cladding. The nanocoated LPG-based sensing structure we developed is functional in high-refractive-index liquids (nd > 1.46) such as oil or gasoline, with pressure sensitivity as high as when water is used as a working liquid. The nanocoating developed for this experiment not only has the highest refractive index ever achieved in LPGs (n > 2.2 at λ = 1,550 nm), but is also the thinnest (<100 nm) able to tune the external-refractive-index sensitivity of the gratings. To the best of our knowledge, this is the first time a nanocoating has been applied on LPGs that is able to simultaneously tune the refractive-index sensitivity and to enable measurements of other parameters.

Combined Plasma-Based Fiber Etching and Diamond-Like Carbon Nanooverlay Deposition for Enhancing Sensitivity of Long-Period Gratings

This paper presents an application of reactive ion etching followed by diamond-like carbon nanooverlay deposition using radio frequency plasma-enhanced chemical vapor deposition method for effective tuning of the refractive index (RI) sensitivity of long-period gratings (LPGs). Both etching and deposition take place within one process. Combination of both plasma-based processes allows for well-controlled tuning of the LPG sensorial response up to its operation at both dispersion turning point of higher order cladding modes and mode transition regime. As a result of the processing, the RI sensitivity has been enhanced up to over 12 000 nm/RIU per single resonance in narrow RI range (1.3344-1.3355 RIU) and over 2000 nm/RIU in broader RI range (1.34-1.356 RIU). Experimental results have been supported by numerical analyses that show capabilities for further significant improvement of both RI sensitivity and range of RI measured with the enhanced sensitivity.