Mathias Röllig

Detection of shallow voids in concrete structures with impulse thermography and radar

Abstract New thermography systems enable the application of active investigation techniques, i.e. the observation of the cooling down process after heating the surface of a structure under investigation. Defects like voids in concrete having a different thermal diffusivity in comparison to the bulk material are visualised by different surface temperatures. The differences between temperature transient curves above sound regions and above inhomogeneities are expected to include information about the defect parameters. Experimental investigations with impulse thermography and radar on a concrete test specimen containing voids were analysed. Radar was used to determine the depth of the voids. The influence of size and depth of the voids on the temperature transient curves was studied for different heating times. The transient curves were also fitted with a simple semi-empirical model.

Transient thermography for structural investigation of concrete and composites in the near surface region

The cooling down process of building structures after heating up with an external radiation source was analysed to detect voids inside and below the surface of a concrete test specimen containing voids with different sizes at various depth or covered with carbon fibre reinforcing laminates. These experimental investigations were compared to the results of simulations performed with a finite difference program.

Near-UV laser interaction with contaminants and pigments on parchment: laser cleaning diagnostics by SE-microscopy, VIS-, and IR-spectroscopy

Abstract Potentials and limitations of the near-UV pulsed laser cleaning of parchment (wavelength 308 nm, pulse duration 17 ns) are demonstrated by the application of scanning electron microscopy (SEM), colour metrics and diffuse reflectance infrared Fourier transform spectroscopy (DRIFT) at model contamination/pigment/parchment systems. Pigment-binder systems stable and unstable against near-UV laser treatment could be identified. A chemical degradation threshold fluence of a goat parchment model substrate was determined which practically coincided with its ablation threshold fluence. This indicates that the fluence range of destructionless laser cleaning at 308 nm is almost not impaired by chemical modfications below the ablation limit. Nevertheless, spectroscopic diagnostics are necessary to guarantee destructionless cleaning for practical cases where the chemical conversion threshold fluence deviates from the ablation threshold to lower values.

Integration of active thermography into the assessment of cultural heritage buildings

Applications of infrared thermography in civil engineering are not limited to the identification of heat losses in building envelopes. Active infrared thermography methods enable structural investigations of building elements with one-sided access up to a depth of about 10 cm. Masonry and especially historical masonry has a very heterogeneous structure containing several different materials (brick, stone, mortar, plaster, wood, metal, etc.) with various thermal properties. As many classes of damage originate from defects that are close to the surface, active thermography is in general very well suited to assessing different test problems in cultural heritage buildings. In this paper, the physical background, equipment, environmental influences and material properties are discussed. Several application results are presented. It is shown how active thermography can be integrated into a holistic approach for the assessment of historical structures.

Detection and Characterization of Defects in Isotropic and Anisotropic Structures Using Lockin Thermography

Lockin thermography is a well-suited method for the characterization of structures made of both metal and fiber reinforced plastic. In most cases, only phase images are analyzed, although the amplitude images might contain useful information as well. Thus, systematic studies of lockin thermography are presented, assessing amplitude and phase images for the detection and quantification of defects in isotropic (steel) and anisotropic (carbon fiber reinforced plastic) materials. Characterized defects are flat bottom holes with different diameters and various remaining wall thicknesses as well as crossed notches at different depths. The excitation frequency was varied while keeping the number of analyzed excitation periods nearly constant for each material. The data analysis was focused on the detectability of the defects both in the amplitude and phase images, including the determination of the signal-to-noise ratio and of the spatial resolution. As a result, the limits of defect detectability and spatial resolution are given for each material.

Comparison of quantitative defect characterization using pulse-phase and lock-in thermography

Using optical excitation sources for active thermography enables a contactless, remote, and non-destructive testing of materials and structures. Currently, two kinds of temporal excitation techniques have been established: pulse or flash excitation, using mostly flash lamps; and periodic or lock-in excitation, using halogen lamps, LED, or laser arrays. From the experimental point of view, both techniques have their advantages and disadvantages. Concerning the comparison of the testing results of both techniques, only very few studies have been performed in the past. In this contribution, the phase values obtained at flat bottom holes in steel and CFRP and the spatial resolution measured at crossed notches in steel using flash and lock-in excitation are compared quantitatively.

Investigating historic masonry structures with a combination of active thermography and 3D laser scanner

Methods for the combination (i. e. comparison and overlay) and data fusion (i. e. integration of all data in one data set, replacement of data) of active thermography and 3D laser scanner (light section method) have been developed. Systematic investigations for quantification of damage in historic structures are presented using both techniques. A case study shows that reproducible investigations at regular time intervals are very well suited for structural monitoring.

In Situ Investigations of Mechanochemical One-Pot Syntheses

We present an in situ triple coupling of synchrotron X-ray diffraction with Raman spectroscopy, and thermography to study milling reactions in real time. This combination of methods allows a correlation of the structural evolution with temperature information. The temperature information is crucial for understanding both the thermodynamics and reaction kinetics. The reaction mechanisms of three prototypical mechanochemical syntheses, a cocrystal formation, a C-C bond formation (Knoevenagel condensation), and the formation of a manganese-phosphonate, were elucidated. Trends in the temperature development during milling are identified. The heat of reaction and latent heat of crystallization of the product contribute to the overall temperature increase. A decrease in temperature occurs via release of, for example, water as a by-product. Solid and liquid intermediates are detected. The influence of the mechanical impact could be separated from temperature effects caused by the reaction.

Development and Application of Active Thermography for Monitoring of Deterioration Processes of Historic Structures

As shown recently, the quantification of damage in historic masonry structures is possible by using active thermography. In this paper, a case study is presented concerning systematic studies of the determination of damage size and prognosis of damage increase inside a sandstone column by using different approaches of active thermography. Various heating sources as well as impulse and periodic heating have been compared. Reproducible investigations in regular time intervals for structural monitoring are possible.

Thermographic Investigation of Delaminated Plaster on Concrete

Active thermography is sensitive to inhomogeneities at and below the surface of objects investigated. Thus, it should be useful for detecting plaster delaminations on concrete. In this paper, the results of field and laboratory investigations into plaster-covered concrete were compared. For evaluating the bonding state of the plaster it is not sufficient to study only the thermal contrasts at the surface of the investigated objects. The experimental results suggest that the overall thermal behaviour has to be considered.