Matt Clark

Spatially resolved acoustic spectroscopy for fast noncontact imaging of material microstructure

We have developed a noncontact and nondestructive technique that uses laser-generated and detected surface acoustic waves to rapidly determine the local acoustic velocity, in order to map the microstructure of multi-grained materials. Optical fringes excite surface waves at a fixed frequency, and the generation efficiency is determined by how closely the fringe spacing matches the acoustic wavelength in the excitation region. Images of titanium alloys are presented, acquired using the technique. Methods to improve the current lateral resolution of 0.8mm are discussed, and the ability to measure velocity change to an accuracy of one part in 3300 is experimentally demonstrated.

All-optical adaptive scanning acoustic microscope☆

We have constructed a fast laser-based surface acoustic wave (SAW) microscope, which may be thought of as a non-perturbing scanning acoustic microscope. The instrument is capable of rapid high resolution vector contrast imaging at several discrete frequencies, without any damage to the sample. Tailoring the generating optical distribution using computer-generated holograms allows us to both focus the acoustic waves (increasing their amplitude) and to spread the optical power over the sample surface (preventing damage). Accurate quantitative amplitude and phase (velocity) measurements and unique acoustic contrast mechanisms are possible with our instrument based on this technology due to the non-perturbing nature and the instrument geometries.However, the complexity of the optical generation profile leads to a strong dependence on material properties such as the SAW velocity and material anisotropy. We address these issues in this paper, and demonstrate how a spatial light modulator may be used to adapt the generating optical distribution to compensate for the material properties. This facilitates simpler alignment and velocity matching, and, combined with an acoustic wavefront sensor, will allow real-time adjustment of the generating source to enable imaging on anisotropic materials.

A direct-search method for the computer design of holograms

A new optimisation technique for the computer design of holograms has been developed. It has much in common with simulated annealing but requires less computational effort. Additionally the technique is not restricted to any particular holographic set up such as Fourier transform holograms. The method has been used to design phase holograms for laser machining at CO/sub 2/ wavelengths. To evaluate the technique these elements have been re-scaled for reconstruction at HeNe wavelengths. They have been reconstructed optically as well as digitally and the results from these exercises used.

Determination of crystallographic orientation of large grain metals with surface acoustic waves

A previously described laser ultrasonic technique known as spatially resolved acoustic spectroscopy (SRAS) can be used to image surface microstructure, using the local surface acoustic wave (SAW) velocity as a contrast mechanism. It is shown here that measuring the SAW velocity in multiple directions can be used to determine the crystallographic orientation of grains. The orientations are determined by fitting experimentally measured velocities to theoretical velocities. Using this technique the orientations of 12 nickel and 3 aluminum single crystal samples have been measured, and these are compared with x-ray Laue backreflection (LBR) measurements with good agreement. The root mean square difference between SRAS and LBR measurements in terms of an R-value is less than 4.1°. The influence of systematic errors in the SAW velocity determination due to instrument miscalibration, which affects the accurate determination of the planes, is discussed. SRAS has great potential for complementary measurements or even for replacing established orientation determination and imaging techniques.

Measurement of material nonlinearity using surface acoustic wave parametric interaction and laser ultrasonics

A dual frequency mixing technique has been developed for measuring velocity changes caused by material nonlinearity. The technique is based on the parametric interaction between two surface acoustic waves (SAWs): The low frequency pump SAW generated by a transducer and the high frequency probe SAW generated and detected using laser ultrasonics. The pump SAW stresses the material under the probe SAW. The stress (typically <5 MPa) is controlled by varying the timing between the pump and probe waves. The nonlinear interaction is measured as a phase modulation of the probe SAW and equated to a velocity change. The velocity-stress relationship is used as a measure of material nonlinearity. Experiments were conducted to observe the pump-probe interaction by changing the pump frequency and compare the nonlinear response of aluminum and fused silica. Experiments showed these two materials had opposite nonlinear responses, consistent with previously published data. The technique could be applied to life-time predictions of engineered components by measuring changes in nonlinear response caused by fatigue.

Fast, all-optical Rayleigh wave microscope: Imaging on isotropic and anisotropic materials

A fast, non-contact Rayleigh wave scanning microscope is demonstrated, which is capable of scan rates of up to a maximum of 1000 measurements/s with typical speeds of up to 250 measurements/s on real samples. The system uses a mode-locked, Q-switched Nd:YAG laser operating at a mode-locked frequency of 82 MHz and a Q-switch frequency of 1 kHz. The Q-switch frequency determines the upper limit of the scanning rate. The generating laser illumination is delivered and controlled by a computer-generated hologram (CGH). The generating laser produces around 30 pulses at 82 MHz and additional harmonics at 164 and 246 MHz and above. The microscope can operate at these harmonics provided the spatial bandwidth of the optics and the temporal bandwidth of the electronics are suitable. The ultrasound is detected with a specialized knife-edge detector. The microscope has been developed for imaging on isotropic materials. Despite this, the system can be used on anisotropic materials, but imaging and interpreting images can be difficult. The anisotropy and grain structure of the material can distort the Rayleigh wavefront, leading to signal loss. A model has been developed to simulate polycrystalline-anisotropic materials; this is discussed along with possible solutions that would overcome the problems associated with anisotropy. Rayleigh wave amplitude images are demonstrated on silicon nitride at 82 and 164 MHz and on polycrystalline aluminium at 82 MHz.

Frequency control in laser ultrasound with computer generated holography

In laser ultrasonics a laser is used to excite ultrasonic waves. The intensity profile of the laser on the sample can be used to control the frequency of the ultrasound generated. In this letter we show how the frequency content of Rayleigh (surface acoustic) waves generated with an 82 MHz mode-locked laser can be controlled using computer generated holograms (CGHs). To demonstrate the effectiveness of the frequency control the CGHs used were defocused to generate new illumination profiles. The agreement between the actual and predicted amplitudes for these profiles is striking. Using this technique, the intensity output from the CGHs may be considered as a tunable Rayleigh wave source.

Cheap optical transducers (CHOTs) for narrowband ultrasonic applications

We have developed an innovative ultrasonic transducer system (CHOT) which is optically excited by means of lasers. It can be used both for generation and detection of narrowband ultrasound and provides non-contact (or even remote), couplant-free generation and/or detection. It has also the advantage of being inexpensive to manufacture and the simplicity of its concept makes it ideal for industrial applications. In this study we present results where CHOTs have been used both for excitation and detection of surface acoustic waves. An initial theoretical model is also presented which describes the principle of operation.

Diffractive acoustic elements for laser ultrasonics

Laser ultrasonics is an effective means of generating surface acoustic waves (SAWs). We have shown in previous publications how computer-generated holograms (CGHs) can be used to project optical distributions onto the sample surface. These can be used to control both the frequency content and the spatial distribution of the resulting ultrasound field. In this paper the concept is extended further to produce distributions which themselves act as diffractive acoustic elements (DAEs) for SAWs. It is demonstrated how frequency suppression, multiple foci, and frequency selective focusing of Rayleigh waves may be achieved with these elements. Agreement between the distributions predicted from the designs and those actually measured is excellent.

Spatially resolved acoustic spectroscopy for rapid imaging of material microstructure and grain orientation

Measuring the grain structure of aerospace materials is very important to understand their mechanical properties and in-service performance. Spatially resolved acoustic spectroscopy is an acoustic technique utilizing surface acoustic waves to map the grain structure of a material. When combined with measurements in multiple acoustic propagation directions, the grain orientation can be obtained by fitting the velocity surface to a model. The new instrument presented here can take thousands of acoustic velocity measurements per second. The spatial and velocity resolution can be adjusted by simple modification to the system; this is discussed in detail by comparison of theoretical expectations with experimental data.