Petr Sedlak

New automatic localization technique of acoustic emission signals in thin metal plates.

In acoustic emission (AE) measurement, the information of the arrival time is very important for event location, event identification and source mechanism analysis. Manual picks are time-consuming and sometimes subjective, especially in the case of large volumes of digital data. Various techniques have been presented in the literature and are routinely used in practice such as amplitude threshold, analysis of the long-term average/short-term average (LTA/STA), high-order statistics or artificial neural networks. A new automatic determination technique of the first arrival times of AE signals is presented for thin metal plates. Based on Akaikes information criterion, proposed algorithm of the first arrival detection uses a specific characteristic function, which is sensitive to change of frequency in contrast to others such as envelope of the signal. The approach is applied to data sets of three different tests. Reliable results show the potential of our approach.

Anomalous lattice softening of Ni2MnGa austenite due to magnetoelastic coupling

Elastic constants of the cubic Ni2MnGa austenite phase and corresponding mechanical damping were determined in the temperature range from 220 K to 400 K and magnetic field up to 2 T using ultrasound pulse-echo method and resonant ultrasound spectroscopy. The shear coefficient c′ increases from 3.6 GPa in the demagnetized state to 5.9 GPa at magnetic saturation, whereas the damping decreased nearly six times. The changes of other elastic constants, c11 and c44 with an applied field were less than 1%. In the ferromagnetic state, the c′ was proportional to the square of magnetization. Above the Curie point, the coefficient c′ and damping were field-independent. The anomalous shear softening is attributed to strong magnetoelastic coupling enhanced by low magnetic anisotropy.

Acoustic and electromagnetic emission as a tool for crack localization

The creation of cracks is accompanied by electric charge redistribution due to loosened chemical bounds. Electric charge on a crack wall creates dipole moments. Vibrations of crack walls produce time-dependent dipole moments and, consequently, electric and magnetic fields are generated. An electric signal is induced on metal electrodes. Simultaneously with the electromagnetic emission (EME) signal, an acoustic emission (AE) signal is generated, but due to the different velocities of propagation of both waves, the detection of the AE signal is delayed. This time delay presents the time of the wave propagation from the individual acoustic emission sensor to the crack. The defect can be located by means of these time intervals. This paper describes the localization using acoustic and electromagnetic emission signals for the two-dimensional case.

Linearized forward and inverse problems of the resonant ultrasound spectroscopy for the evaluation of thin surface layers

In this paper, linearized approximations of both the forward and the inverse problems of resonant ultrasound spectroscopy for the determination of mechanical properties of thin surface layers are presented. The linear relations between the frequency shifts induced by the deposition of the layer and the in-plane elastic coefficients of the layer are derived and inverted, the applicability range of the obtained linear model is discussed by a comparison with nonlinear models and finite element method (FEM), and an algorithm for the estimation of experimental errors in the inversely determined elastic coefficients is described. In the final part of the paper, the linearized inverse procedure is applied to evaluate elastic coefficients of a 310 nm thick diamond-like carbon layer deposited on a silicon substrate.

Physical Simulation of the Random Failure of Implanted Braided NiTi Stents

A problem of random clinical failures of the braided esophageal NiTi stents has been addressed by performing physical simulation experiments on helical NiTi springs loaded in cyclic tension in air, water, and simulated biological fluid. Strains and stresses involved in spring deformation were analyzed through simulation by FEM implemented SMA model. It was found that the fatigue life of NiTi springs is significantly lower in fluids than in the air pointing toward the corrosion fatigue mechanism. There is, however, a fatigue limit roughly corresponding to the onset of martensitic transformation in the wire, which is not common for corrosion fatigue. It is proposed that surface TiO2 oxide cracking plays major role in that. Once the oxide layer on the NiTi wire surface fractures, typically during the first mechanical cycle, cracks in the oxide layer periodically open and close during subsequent mechanical cycling. This leads to the localization of mechanical and corrosion attacks under the oxide cracked regions. Microcracks within the surface oxide layer crossing over into the NiTi matrix were indeed revealed by scanning electron microscopy of FIB sections of fatigued wires. A corrosion assisted mechanism for fatigue crack nucleation at the interface between the surface oxide and NiTi matrix is proposed based on the available evidence. The approach opens a space for a better assessment of the corrosion fatigue performance of superelastic NiTi and ultimately for estimation of the lifetime of implanted braided NiTi stents.

Modeling of mechanical response of NiTi shape memory alloy subjected to combined thermal and non-proportional mechanical loading: a case study on helical spring actuator:

Textured polycrystals of NiTi-based shape memory alloys (SMA) exhibit pronounced anisotropic properties which significantly influence their response to mechanical and thermal loading. In this work, a constitutive model tailored for non-proportional multi-axial loading of NiTi SMA exhibiting two-stage phase transformation via R-phase is enhanced so that the anisotropy of martensitic structure is captured. Numerical simulations of the mechanical response of a NiTi SMA helical spring subjected to thermal cycling at a constant applied force are performed and compared with experimental data. Quantitative correspondence between experiments and simulations demonstrates the predictive potential of the model. Simulations also provide detailed information on the evolution of distributions of phase fractions and stress within a cross-section of the wire forming the spring. Because the loading is non-proportional, the evolution is rather complex and intriguing.

Nyquist Relation and Its Validity for Piezoelectric Ceramics Considering Temperature

In this paper, we focused on validity of the Nyquist relation for piezoelectric ceramics in temperatures 303 K–393 K. The electrical impedance and noise spectral density were measured and compared for every 10 K in frequency range 100 kHz–1 MHz. The measurements were made in thermal stable condition and under equilibrium conditions in the case of noise measurement.

Simulations of Self-Expanding Braided Stent Using Macroscopic Model of NiTi Shape Memory Alloys Covering R-Phase

Self-expanding stents or stentgrafts made from Nitinol superelastic alloy are widely used for a less invasive treatment of disease-induced localized flow constriction in the cardiovascular system. The therapy is based on insertion of a stent into a blood vessel to maintain the inner diameter of the vessel; it provides highly effective results at minimal cost and with reduced hospital stays. However, since stent is an external mechanical healing tool implemented into human body for quite a long time, information on the mechanical performance of it is of fundamental importance with respect to patient’s safety and comfort. Advantageously, computational structural analysis can provide valuable information on the response of the product in an environment where in vivo experimentation is extremely expensive or impossible. With this motivation, a numerical model of a particular braided self-expanding stent was developed. As a reasonable approximation substantially reducing computational demands, the stent was considered to be composed of a set of helical springs with specific constrains reflecting geometry of the structure. An advanced constitutive model for NiTi-based shape memory alloys including R-phase transition was employed in analysis. Comparison to measurements shows a very good match between the numerical solution and experimental results. Relation between diameter of the stent and uniform radial pressure on its surface is estimated. Information about internal phase and stress state of the material during compression loading provided by the model is used to estimate fatigue properties of the stent during cyclic loading.

Sensitivity of the resonant ultrasound spectroscopy to weak gradients of elastic properties

The applicability of resonant ultrasound spectroscopy on materials with weak spatial gradients in elastic coefficients and density is analyzed. It is shown that such gradients do not affect measurably the resonant spectrum but have a significant impact on the modal shapes. A numerical inverse procedure is proposed to explore the possibility of reconstructing the gradients from experimentally obtained modal shapes. This procedure is tested on synthetic data and applied to determine the gradient of the shear modulus in a continuously graded silicon nitride ceramic material. The results are in a good agreement with the gradient calculated for the examined material theoretically as well as with the results of other experimental methods.

Noise in Piezoceramics

Thermal noise and polarisation noise are the main sources of voltage or current fluctuations in piezoceramic samples which are used as acoustic emission sensors. Signal to noise ratio plays important role. Noise is related to energy dissipation and due to that conductivity is proportional to imaginary part of susceptibility and to the frequency. The measured noise spectral density is 1/f type, but it is not related to the mobility fluctuations in this case, because no DC current or voltage was applied on the sample. Physical quantity SU/RS shows that in all frequency range SU/RS is a constant in the first approximation and it is very near to 4kT. There is no source of 1/f fluctuations caused by mobility fluctuations.