Qilai Zhou

Rapid Fabrication of Li2TiO3 Pebbles via Microwave-Induced Combustion Process and 3D Printing

Li2TiO3 has been recognized as one of the most promising tritium breeding materials for D-T fusion reactor blanket. In this study, ultra-fine Li2TiO3 powder was prepared rapidly by microwave-induced solution combustion synthesis (MSCS) using nitrates of lithium and titanate as raw materials, citric acid as fuel. The as-synthesized Li2TiO3 powder exhibits an average crystalline size as small as 20 nm with uniform distribution. Computer-assisted 3D printing technology was employed to fabricate Li2TiO3 ceramic breeding pebbles. This computer-assisted process is precise, efficient and controllable, which offers an alternative for the mass production of Li2TiO3 pebbles. The pebbles exhibit good sphericity, relatively small grain size, preferable sinterability and crushing load strength.Copyright

Effect of Lath Width and Dislocation Density on Resistance to Irradiation of Warmly Deformed SCRAM Steel

The martensitic lath width (0.83 ± 0.45μm ∼ 0.48 ± 0.14 μm) and dislocation density (1.3 ± 0.3 × 1015 m−2 ∼ 6.4 ± 1.6 ×1015 m−2) change of Super-clean Reduced Activation Martensitic (SCRAM) steel caused by warm deformation on Gleeble-3500 thermo-simulation machine have been examined. The irradiation-induced helium bubbles and hardening were observed in all the specimens after helium implantation to 1e + 17/cm2 at 723 K. The helium bubbles became smaller and more numerous while the distribution was more homogeneous when the lath width decrease and dislocation density increase. The nano-indentation hardness indicated that the sample, the martensitic lath width is 0.83 ± 0.45μm and the dislocation density is 1.3 ± 0.3 × 1015 m−2, exhibited the maximum nano-indentation variation (ΔH) and the ΔH decreased with the lath width decreasing and dislocation density increasing. The hardening occurred in all helium implanted samples can mainly be ascribed to helium bubbles.Copyright