Somjeet Biswas

Influence of initial texture on the microstructural instabilities during compression of commercial α-Titanium at 25 °C to 400 °C

Cylindrical specimens of textured commercial pure α-titanium plate, cut with the cylinder axis along the rolling direction for one set of experiments and in the long transverse direction for the other set, were compressed at strain rates in the range of 0.001 to 100 s~’ and temperatures in the range of 25 °C to 400 °C. At strain rates ≥ 1 s−1 ’, both sets of specimens exhibited adiabatic shear bands, but the intensity of shear bands was found to be higher in the rolling direction specimens than in the long transverse direction specimens. At strain rates ⪯0.1s−1 the material deformed in a microstructurally inhomogeneous fashion. For the rolling direction specimens, cracking was observed at 100 °C and at strain rates ⪯0.1 s−1. This is attributed to dynamic strain aging. Such cracking was not observed in the long transverse specimens. The differences in the intensity of adiabatic shear bands and that of dynamic strain aging between the two sets of test specimens are attributed to the strong crystallographic texture present in these plates.

Relationship Between the 3D Porosity and β-Phase Distributions and the Mechanical Properties of a High Pressure Die Cast AZ91 Mg Alloy

Currently, most magnesium lightweight components are fabricated by casting as this process is cost effective and allows forming parts with complex geometries and weak textures. However, cast microstructures are known to be heterogeneous and contain unpredictable porosity distributions, which give rise to a large variability in the mechanical properties. This work constitutes an attempt to correlate the microstructure and the mechanical behavior of a high pressure die cast (HPDC) Mg AZ91 alloy, aimed at facilitating process optimization. We have built a stairway-shaped die to fabricate alloy sections with different thicknesses and, thus, with a range of microstructures. The grain size distributions and the content of β-phase (Mg17Al12) were characterized by optical and electron microscopy techniques as well as by electron backscatter diffraction (EBSD). The bulk porosity distribution was measured by 3D computed X-ray microtomography. It was found that the through-thickness microhardness distribution is mostly related to the local area fraction of the β-phase and to the local area fraction of the pores. We correlate the tensile yield strength to the average pore size and the fracture strength and elongation to the bulk porosity volume fraction. We propose that this empirical approach might be extended to the estimation of mechanical properties in other HPDC Mg alloys.

Microstructure and Texture Evolution in Interstitial-Free (IF) Steel Processed by Multi-Axial Forging

In this study, severe plastic deformation (SPD) of Ti-bearing interstitial-free steel was carried out by multi-axial forging (MAF) technique. The grain refinement achieved was comparable to that by other SPD techniques. A considerable heterogeneity was observed in the microstructure and texture. Texture of multi-axially forged steels has been evaluated and reported for the first time. The material exhibited a six-fold increase in the yield strength after four cycles of MAF.

Ultra-fine Grain Materials by Severe Plastic Deformation: Application to Steels

Severe plastic deformation techniques are known to produce grain sizes up to submicron level. This leads to conventional Hall-Petch strengthening of the as-processed materials. In addition, the microstructures of severe plastic deformation processed materials are characterized by relatively lower dislocation density compared to the conventionally processed materials subjected to the same amount of strain. These two aspects taken together lead to many important attributes. Some examples are ultra-high yield and fracture strengths, superplastic formability at lower temperatures and higher strain rates, superior wear resistance, improved high cycle fatigue life. Since these processes are associated with large amount of strain, depending on the strain path, characteristic crystallographic textures develop. In the present paper, a detailed account of underlying mechanisms during SPD has been discussed and processing-microstructure-texture-property relationship has been presented with reference to a few varieties of steels that have been investigated till date.

Study of Texture Evolution of Pure Magnesium during ECAE using EBSD

Commercially Pure Magnesium initially hot rolled and having a basal texture was deformed by Equal Channel Angular Extrusion (ECAE). ECAE was carried out upto 8 passes in a 90° die following routes A and Bc through a processing sequence involving two temperatures, namely 523 and 473 K. Texture and microstructure formed were studied using electron back scatter diffraction (EBSD) technique. In addition to significant reduction in grain size, strong <0002> fiber texture inclined at an angle ~ 45o from the extrusion axis formed in the material. Texture was also analyzed by orientation distribution function (ODF) and compared vis-à-vis shear texture. A significant amount of dynamic recrystallization occurred during ECAE, which apparently did not influence texture.

Grain Growth in ECAE Processed Pure Magnesium

Grain growth kinetics was studied for commercially pure magnesium subjected to equal channel angular extrusion (ECAE). The specimens were ECAE processed upto 4 passes at 523 K following all the three important routes, namely A, 13, and C. Texture and microstructures of the samples were studied using Electron Back Scattered Diffraction (EBSD) technique in a Field Emission Gun Scanning Electron Microscope (FEG-SEM). It was observed that the grain size significantly reduces after ECAE. ECAE process produces a slightly rotated B and C-2 fiber. Static annealing leads to normal grain growth with unimodal distribution of grains through out the temperature range. Average activation energy for grain growth in the temperature range studied is found to be less than the activation energy for lattice diffusion and grain boundary diffusion of magnesium. No significant change in texture during isochronal annealing for 1 hour i.e., the predominant deformation texture remains same.

Texture and Grain Boundary Character Distribution during Equal Channel Angular Extrusion of some Two-Phase Copper Alloys

In the present work, a thorough investigation of evolution of microstructure and texture has been carried out to elucidate the evolution of texture and grain boundary character distribution (GBCD) during Equal Channel Angular Extrusion (ECAE) of some model two-phase materials, namely Cu-0.3Cr and Cu-40Zn. Texture of Cu-0.3Cr alloy is similar to that reported for pure copper. On the other hand, in Cu-40Zn alloy, texture evolution in α and β (B2) phases are interdependent. In Cu-0.3Cr alloy, there is a considerable decreases in volume fraction of low angle boundaries (LAGBs), only a slight increase in CSL boundaries, but increase in high angle grain boundaries (HAGBs) from 1 pass to 4 passes for both the routes. In the case of Cu-40Zn alloy, there is an appreciable increase in CSL volume fraction.

Corrosion Behavior of Ultra Fine Grain Pure Magnesium for Automotive Applications

The contemporary challenge in automotive industry is weight reduction. Compared to conventional automotive materials, commercially pure magnesium is having enhanced strength-to-mass ratio and low density, which confers to optimal requirement for automotive applications. Amongst various other reasons such as low hardness, low corrosion resistance also prevents it from entering mass production .severe plastic deformation by equal channel angular extrusion (ECAE) is regarded as one of the prominent method to increase the mechanical properties of magnesium. However, the investigation in corrosion resistance of extruded magnesium in automotive environment is not discussed in depth. This paper discusses the microstructure and corrosion characteristics of commercially pure magnesium which has been extruded by ECAE at 473k through the routes a and bc up to eight passes and their three surfaces (extrusion direction, normal direction & transverse direction) in detail. The corrosion experiment has been performed using conventional electrochemical techniques such as open-circuit potential measurements and potentiodynamic polarization method in 3.5 wt% Nacl solution environment. The surface morphology of the magnesium billet was examined in detail using scanning electron microscopy (SEM) and the hardness was measured using micro Vickers hardness tester.

Evolution of Crystallographic Texture During Equal Channel Angular Extrusion (ECAE) of (α+β) Brass

Equal channel angular extrusion is now a well know process to generate ultra-fine grain microstructure in bulk materials. Since the material undergoes a large deformation, the process is also associated with evolution of characteristic texture. Most of the studies carried out on this subject aim at studying single phase materials. However, such a study is very relevant for two-phase materials owing to the possible enhancement of super-plastic properties. In the present work, a thorough investigation of evolution of microstructure and texture has been carried out to elucidate the deformation mechanisms and subsequent texture evolution in a model two-phase material, namely (α + β) brass. A detailed analysis of texture evolution in both α and β (B2) phases will be presented.