Stephanie Deboeuf

Flows of suspensions of particles in yield stress fluids

We study the rheological behavior of suspensions of noncolloidal spheres in yield stress fluids (concentrated emulsions). These are good model systems for understanding, e.g., the rheology of fresh concrete or debris flows, and more generally, the behavior of particles dispersed in any nonlinear material. We use magnetic resonance imaging techniques to investigate the flows of these yield stress suspensions in a concentric-cylinder Couette geometry. We extend the theoretical approach of Chateau et al. [J. Rheol. 52, 489–506 (2008)], valid for isotropic suspensions, to describe suspensions in simple shear flows, in which an anisotropic spatial distribution of particles is induced by flow. Theory and experiments show that the suspensions can be modeled by a Herschel–Bulkley behavior of same index as their interstitial fluid. We characterize the increase of their consistency and their yield stress with the particle volume fraction ϕ in the 0%–50% range. We observe a good agreement between the experimental variations of the consistency with ϕ and the theoretical prediction. This shows that the average apparent viscosity of the sheared interstitial material is correctly estimated and taken into account. We also observe shear-induced migration with similar properties as in a Newtonian fluid, which we predict theoretically, suggesting that particle normal stresses are proportional to the shear stress. However, the yield stress at flow stoppage increases much less than predicted. We also show that new features emerge in the rheology of the yield stress fluid when adding particles. We predict and observe the emergence of a nonzero normal stress difference at the yielding transition. We observe that the yield stress at flow start can differ from the yield stress at flow stoppage, and depends on flow history. It is likely a signature of a shear-dependent microstructure, due to the nonlinear behavior of the interstitial fluid, which makes these materials different from suspensions in Newtonian media. This is confirmed by direct characterization of shear-rate-dependent pair distribution functions using X-ray microtomography. This last observation explains why the theory predictions for the consistency can be correct while failing to model the yield stress at flow stoppage: a unique microstructure was indeed assumed as a first approximation. More sophisticated theories accounting for a shear-dependent microstructure are thus needed.We study the rheological behavior of suspensions of noncolloidal spheres in yield stress fluids (concentrated emulsions). These are good model systems for understanding, e.g., the rheology of fresh concrete or debris flows, and more generally, the behavior of particles dispersed in any nonlinear material. We use magnetic resonance imaging techniques to investigate the flows of these yield stress suspensions in a concentric-cylinder Couette geometry. We extend the theoretical approach of Chateau et al. [J. Rheol. 52, 489–506 (2008)], valid for isotropic suspensions, to describe suspensions in simple shear flows, in which an anisotropic spatial distribution of particles is induced by flow. Theory and experiments show that the suspensions can be modeled by a Herschel–Bulkley behavior of same index as their interstitial fluid. We characterize the increase of their consistency and their yield stress with the particle volume fraction ϕ in the 0%–50% range. We observe a good agreement between the experimental v...

Flow Rule, Self-Channelization, and Levees in Unconfined Granular Flows

Unconfined granular flows along an inclined plane are investigated experimentally. During a long transient, the flow gets confined by quasistatic banks but still spreads laterally towards a well-defined asymptotic state following a nontrivial process. Far enough from the banks a scaling for the depth averaged velocity is obtained, which extends the one obtained for homogeneous steady flows. Close to jamming it exhibits a crossover towards a nonlocal rheology. We show that the levees, commonly observed along the sides of the deposit upon interruption of the flow, disappear for long flow durations. We demonstrate that the morphology of the deposit builds up during the flow, in the form of an underlying static layer, which can be deduced from surface velocity profiles, by imposing the same flow rule everywhere in the flow.

Dynamics of grain ejection by sphere impact on a granular bed

The dynamics of grain ejection consecutive to a sphere impacting a granular material is investigated experimentally and the variations of the characteristics of grain ejection with the control parameters are quantitatively studied. The time evolution of the corona formed by the ejected grains is reported, mainly in terms of its diameter and height, and favorably compared with a simple ballistic model. A key characteristic of the granular corona is that the angle formed by its edge with the horizontal granular surface remains constant during the ejection process, which again can be reproduced by the ballistic model. The number and the kinetic energy of the ejected grains are evaluated and allow for the calculation of an effective restitution coefficient characterizing the complex collision process between the impacting sphere and the fine granular target. The effective restitution coefficient is found to be constant when varying the control parameters.

Memory of the Unjamming Transition during Cyclic Tiltings of a Granular Pile

Discrete numerical simulations are performed to study the evolution of the microstructure and the response of a granular packing during successive loading-unloading cycles, consisting of quasistatic rotations in the gravity field between opposite inclination angles. We show that internal variables--e.g., stress and fabric of the pile--exhibit hysteresis during these cycles due to the exploration of different metastable configurations. Interestingly, the hysteretic behavior of the pile strongly depends on the maximal inclination of the cycles, giving evidence of the irreversible modifications of the pile state occurring close to the unjamming transition. More specifically, we show that for cycles with maximal inclination larger than the repose angle, the weak-contact network carries the memory of the unjamming transition. These results demonstrate the relevance of a two-phase description--strong- and weak-contact networks--for a granular system, as soon as it has approached the unjamming transition.

Comparative Study of Crumpling and Folding of Thin Sheets

Crumpling and folding of paper are at first sight very different ways of confining thin sheets in a small volume: the former one is random and stochastic whereas the latest one is regular and deterministic. Nevertheless, certain similarities exist. Crumpling is surprisingly inefficient: a typical crumpled paper ball in a waste-bin consists of as much as 80% air. Similarly, if one folds a sheet of paper repeatedly in two, the necessary force becomes so large that it is impossible to fold it more than six or seven times. Here we show that the stiffness that builds up in the two processes is of the same nature, and therefore simple folding models allow us to capture also the main features of crumpling. An original geometrical approach shows that crumpling is hierarchical, just as the repeated folding. For both processes the number of layers increases with the degree of compaction. We find that for both processes the crumpling force increases as a power law with the number of folded layers, and that the dimensionality of the compaction process (crumpling or folding) controls the exponent of the scaling law between the force and the compaction ratio.

Jamming transition of a granular pile below the angle of repose

Abstract.We experimentally study the relaxation towards mechanical equilibrium following the surface avalanche of a granular pile and discuss it in the general context of glassy materials and jamming transition. Two coexisting dynamics are observed in the surface layer: a short time exponential decay related to rapid isolated grains displacements, and intermittent reactivation bursts consisting in spatially correlated moves. The competition of both dynamics results in long-lived intermittent transients, the total duration of which can last more than a thousand of seconds. The typical time-scales, and the two-time relaxation function of these transients are measured. Analyzing the response of the surface layer to localized perturbations provides new evidence for spatial correlations. We further analyse the relaxation function in a probabilistic framework, which allows to discuss different possible scalings according to the choice of specific hypothesis. Following some considerations on the observed time-scales, we finally discuss the similarities with aging systems which are suggested by our description of the observed dynamics.

Measuring order in the isotropic packing of elastic rods

The packing of elastic bodies has emerged as a paradigm for the study of macroscopic disordered systems. However, progress is hampered by the lack of controlled experiments. Here we consider a model experiment for the isotropic two-dimensional confinement of a rod by a central force. We seek to measure how ordered is a folded configuration and we identify two key quantities. A geometrical characterization is given by the number of superposed layers in the configuration. Using temporal modulations of the confining force, we probe the mechanical properties of the configuration and we define and measure its effective susceptibility. These two quantities may be used to build a statistical framework for packed elastic systems.

Imaging non-Brownian particle suspensions with X-ray tomography: Application to the microstructure of Newtonian and viscoplastic suspensions

A key element in the understanding of the rheological behavior of suspensions is their microstructure. Indeed, the spatial distribution of particles is known to depend on flow history in suspensions, which has an impact on their macroscopic properties. These micro-macrocouplings appeal for the development of experimental tools allowing for the rheological characterization of a suspension and the imaging of particles. In this paper, we present the technique we developed to image in three dimensions the microstructure of suspensions of non-Brownian particles, using X-ray computed tomography and subvoxel identification of particle centers. We also give examples of the information we can get in the case of Newtonian and viscoplastic suspensions, referring to Newtonian and viscoplastic suspending fluid. We compute three dimensional pair distribution functions and show that it is possible to get a nearly isotropic microstructure after mixing. Under shear, this microstructure becomes anisotropic in the shear pla...