Stergios John Papadakis

Controlled placement of an individual carbon nanotube onto a microelectromechanical structure

We report on the precise placement of a single carbon nanotube (CNT) onto a microlectromechanial system (MEMS) structure. Using a hybrid atomic force microscope/scanning electron microscope (AFM/SEM) system, an individual multiwalled CNT was retrieved from a cartridge by the AFM tip, translated to a MEMS device, and then placed across a gap between an actuating and a stationary structure. Progress toward a resistance versus stress/strain measurement on a CNT will be discussed, including SEM images of a MEMS structure we have designed specifically for such a measurement.

Torsional Response and Stiffening of Individual Multiwalled Carbon Nanotubes

We report on the characterization of torsional oscillators which use multiwalled carbon nanotubes as the spring elements. Through atomic-force-microscope force-distance measurements we are able to apply torsional strains to the nanotubes and measure their torsional spring constants, and estimate their effective shear moduli. The data show that the nanotubes are stiffened by repeated flexing. We speculate that changes in the intershell mechanical coupling are responsible for the stiffening.

Fabrication of nanometer-scale mechanical devices incorporating individual multiwalled carbon nanotubes as torsional springs

We report on the fabrication of nanometer-scale mechanical devices incorporating multiwalled carbon nanotubes (MWNTs) as the torsional spring elements. We have employed electron beam lithography to pattern device elements directly onto individual MWNTs on a silicon dioxide substrate. The structures were suspended by etching the substrate and subsequent critical-point drying of the sample. We also briefly present characterization of the torsional properties of an individual MWNT. The techniques described are applicable to other nanometer-scale rod-like objects.

Simultaneous atomic force microscopy measurement of topography and contact resistance of metal films and carbon nanotubes

We present a quartz tuning-fork-based atomic force microscopy (AFM) setup that is capable of mapping the surface contact resistance while scanning topography. The tuning-fork setup allows us to use etched Pt/Ir tips, which have higher durability and better conductivity than probes used in earlier AFM conductance measurements. The performance of the method is demonstrated with contact resistance measurements of gold lines on silicon dioxide and carbon nanotubes on graphite.

Visualization and natural control systems for microscopy

This chapter presents these microscope systems, along with brief descriptions of the science experiments driving the development of each system. Beginning with a discussion of the philosophy that has driven the Nanoscale Science Research Group (NSRG) and the methods used, the chapter describes the lessons learned during system development, including both useful directions and blind alleys. The first lesson is to begin software development at least as soon as hardware development. The second lesson is to partner with experts in required technologies. The NSRG attempts to use the best available computer technology to develop effective systems for use by the physical science team, which then become cost-effective and can be deployed on widely available hardware as technology marches on. The chapter also describes techniques to enable telemicroscopy in the context of remote experiments and outreach.

Mechanics of nanotubes and nanotube‐based devices

We discuss the mechanical properties of carbon nanotubes and devices incorporating carbon nanotubes. We demonstrate novel measurement and force application techniques using an atomic force microscope coupled to a unique computing environment that simplifies manipulations. We report on results from measurements of the mechanical and electronic interactions between nanotubes and graphite surfaces. We also fabricate nanometer‐scale electromechanical devices which incorporate nanotubes as springs, and discover a remarkable stiffening behavior of the nanotubes.