Thomas Trottenberg

Experimental determination of the charge on dust particles forming Coulomb lattices

Abstract Large dust grains ( r p =10 μ m) are found to form hexagonal Coulomb lattices with an interparticle distance of R p =880 μ m in the sheath of an argon rf discharge. The charge on the particle is measured from its resonant response to an external periodic force. The charge is found to be -200000 e .

Measurement of the electric charge on particulates forming Coulomb crystals in the sheath of a radiofrequency plasma

Monodisperse electrically charged particulates (9.4 mu m diameter) are trapped in the sheath of an argon RF parallel plate discharge. The particulates form Coulomb crystals consisting of horizontal hexagonal layers. A method for the determination of the charge on the particles is demonstrated that uses the response to a modulation of the electrode bias. Charges about three to five thousand elementary units are measured. The commonly applied orbital motion limited (OML) charging model leads to charges higher than the measured values. The strong coupling system is compared to the one component plasma (OCP model) and to a model with Yukawa potentials.

Dust confinement and dust-acoustic waves in weakly magnetized anodic plasmas

Experiments on dust-acoustic waves (DAW) in a magnetized anodic plasma are presented for the regime of low collisionality. The dust trapping and the self-excited and synchronized DAW dynamics are studied. Based on Langmuir and emissive probe measurements the dust confinement is found to be well described with respect to size, stability, and position of the dust cloud by an effective potential well formed by ion drag and Coulomb forces. Moreover, the measurements indicate the necessity for a kinetic model for the wave dispersion. By means of singular value decomposition the local wavelengths and growth rates of the waves are measured systematically. It is found that the measured mean wave number is well described by kinetic theory, while the theoretical growth rates overestimate the experiments. A novel observation for the DAW is a systematic variation of the wavelength inside the dust cloud.

A calorimetric probe for plasma diagnostics

A calorimetric probe for plasma diagnostics is presented, which allows measurements of the power taken by a test substrate. The substrate can be biased and used as an electric probe in order to obtain information about the composition of the total heating power. A new calibration technique for calorimetric probes, which uses monoenergetic electrons at low pressure, has been developed for an improved accuracy. The use of the probe is exemplified with an experiment where both energetic neutral atoms and ions heat the test substrate.

Dynamics of small dust clouds trapped in a magnetized anodic plasma

Small dust clouds, which are confined in an anodic plasma, are studied with respect to their structure and their response to modulation of the anode bias. The dust cloud is displaced from the center of the discharge by a process similar to the void mechanism in radio-frequency discharges under microgravity. The top layers of the dust cloud are in a crystalline state and the cloud performs a slow rotation about the magnetic field direction. For modulation frequencies below 15Hz, a sloshing and stretching motion in the confining potential well is found. Spontaneously excited dust density waves are observed when the dust cloud exceeds a minimum size. The waves are characterized by sickle-shaped wave fronts. No standing waves were found. The wave dispersion shows an influence of the boundedness of the system in terms of a frequency cutoff.

Effect of surface treatments on the properties and morphological change of dental zirconia

STATEMENT OF PROBLEM Creating a rough surface for bonding with airborne-particle abrasion with alumina may damage the surface of zirconia. Other treatment methods for creating a bonding surface without causing damage require investigation. PURPOSE The purpose of this in vitro study was to find ways of treating the zirconia surface without causing flaws, debris, pits, microcracks, or tetragonal to monoclinic phase transformation. MATERIAL AND METHODS Yttria-stabilized tetragonal zirconia polycrystal (Y-TZP) ceramic surfaces were treated with gas plasma, argon-ion bombardment, 150-μm abrasive zirconia particles, and abrasive 150-μm alumina particles; untreated surfaces were used as the control group. X-ray diffraction (XRD) and confocal Raman spectroscopy were used to study the phase transformation. The roughness of specimens was measured with a confocal 3D laser scanning microscope. Modification of surface topography was analyzed with field emission scanning electron microscopy (FESEM), and the flexural strength was measured with a universal testing machine. Statistical analyses were performed with 1-way ANOVA, followed by comparison of means with the Tukey honest significant difference test. The standard deviation was calculated with descriptive statistics. RESULTS The sintered Y-TZP ceramic used in this study showed 2 phases, tetragonal and cubic. Specimens abraded with 150-μm alumina particles showed a higher monoclinic volume fraction (VmXRD=8.68%) and roughness (Ra=0.91μm) than specimens abraded with 150-μm zirconia particles (VmXRD=1.22%, Ra=0.08μm). One-way ANOVA indicated a significance difference in roughness among groups (P<.01). No phase transformation was observed in specimens treated with argon-ion bombardment or plasma. According to the Raman results, the volume fraction of the monoclinic phase for the specimens treated with airborne-particle abrasion depended on the distance from the ceramic surfaces and decreased with the increase in this distance. A slightly higher flexural strength was observed for untreated specimens (1009 MPa), followed by specimens treated with gas plasma (1000 MPa) and those airborne-particle abraded with 150-μm zirconia particles (967 MPa). The flexural strength of other specimens was lower (940 MPa for specimens abraded with 150-μm alumina particles and 916 MPa for specimens subjected to argon-ion bombardment). One-way ANOVA analysis indicated no significant difference in flexural strengths among all groups (P>.2). FESEM measurements showed that airborne-particle abrading Y-TZP surfaces with 150-μm alumina particles caused more damage to this area than the other methods. CONCLUSIONS Y-TZP ceramic surfaces treated with zirconia particles, argon-ion bombardment, and gas plasma were damaged less in comparison with surfaces abraded with alumina particles.

Measurement of the force on microparticles in a beam of energetic ions and neutral atoms

The force on microparticles in an energetic ion beam is investigated experimentally. Hollow glass microspheres are injected into the vertically upward directed beam and their trajectories are recorded with a charge-coupled device camera. The net force on the particles is determined by means of the measured vertical acceleration. The resulting beam pressures are compared with Faraday cup measurements of the ion current density and calorimetric measurements of the beam power density. Due to the neutral gas background, the beam consists, besides the ions, of energetic neutral atoms produced by charge-exchange collisions. It is found that the measured composition of the drag force by an ion and a neutral atom component agrees with a beam model that takes charge-exchange collisions into account. Special attention is paid to the momentum contribution from sputtered atoms, which is shown to be negligible in this experiment, but should become measurable in case of materials with high sputtering yields.

An experiment for the investigation of forces on microparticles in ion beams

A novel experiment for the study of forces on microparticles in ion beams is presented. A broad beam ion source provides a vertically upward directed beam wherein 100 microm hollow glass spheres are injected. The particles are illuminated by a diode laser and recorded with a charge-coupled device camera. From the trajectories the acceleration and the net force on the particles are determined. Information on energetic neutral atoms is achieved, which is not accessible by electrostatic methods.

Resonance cones in a dusty magnetized plasma

A new diagnostic method for magnetized dusty plasmas, the excitation of lower hybrid resonance cones, is investigated experimentally. The resonance cone is excited with a small antenna, and the angular distribution of the wave field with respect to the magnetic field shows a resonant enhancement, which shifts according to the free electron density. It is demonstrated that dust reduces the free electron density in agreement with Langmuir probe results. Wave damping by scattering effects is found negligible.

Effect of surface modifications on the bond strength of zirconia ceramic with resin cement resin

OBJECTIVES Purpose of this in vitro study was to evaluate the effect of surface modifications on the tensile bond strength between zirconia ceramic and resin. METHODS Zirconia ceramic surfaces were treated with 150-μm abrasive alumina particles, 150-μm abrasive zirconia particles, argon-ion bombardment, gas plasma, and piranha solution (H2SO4:H2O2=3:1). In addition, slip casting surfaces were examined. Untreated surfaces were used as the control group. Tensile bond strengths (TBS) were measured after water storage for 3 days or 150 days with additional 37,500 thermal cycling for artificial aging. Statistical analyses were performed with 1-way and 3-way ANOVA, followed by comparison of means with the Tukey HSD test. RESULTS After storage in distilled water for three days at 37 °C, the highest mean tensile bond strengths (TBS) were observed for zirconia ceramic surfaces abraded with 150-μm abrasive alumina particles (TBS(AAP)=37.3 MPa, TBS(CAAP)=40.4 MPa), and 150-μm abrasive zirconia particles (TBS(AZP)=34.8 MPa, TBS(CAZP)=35.8 MPa). Also a high TBS was observed for specimens treated with argon-ion bombardment (TBS(BAI)=37.8 MPa). After 150 days of storage, specimens abraded with 150-μm abrasive alumina particles and 150-μm abrasive zirconia particles revealed high TBS (TBS(AAP)=37.6 MPa, TBS(CAAP)=33.0 MPa, TBS(AZP)=22.1 MPa and TBS(CAZP)=22.8 MPa). A high TBS was observed also for specimens prepared with slip casting (TBS(SC)=30.0 MPa). A decrease of TBS was observed for control specimens (TBS(UNT)=12.5 MPa, TBS(CUNT)=9.0 MPa), specimens treated with argon-ion bombardment (TBS(BAI)=10.3 MPa) and gas plasma (TBS(GP)=11.0 MPa). A decrease of TBS was observed also for specimens treated with piranha solution (TBS(PS)=3.9 MPa, TBS(CPS)=4.1 MPa). A significant difference in TBS after three days storage was observed for specimens treated with different methods (p<0.001). Thermal cycling significantly reduced TBS for all groups (p<0.001) excluding groups: AAP(p>0.05), CAAP(p>0.05) and SC(p>0.05). However, the failure patterns of debonded specimens prepared with 150-μm abrasive zirconia particles were 96.7% cohesive. CONCLUSION Treatment of zirconia ceramic surfaces with abrasive zirconia particles is a promising method to increase the tensile bond strength without significant damage of the ceramic surface itself. An alternative promising method is slip casting.