Vinícius Felipe Wandscher

Preliminary results of the survival and fracture load of roots restored with intracanal posts: weakened vs nonweakened roots.

PURPOSE To evaluate the fracture load and survival rate of weakened and non-weakened roots restored with different intracanal posts. METHODS Eighty teeth (16 mm) were prepared to a length of 10 mm with a custom drill. Fifty roots were weakened with a tapered diamond drill, and 30 roots were not. The specimens were embedded with acrylic resin up to 3 mm from the coronal aspect, and the periodontal ligament was simulated. The 50 weakened roots were restored with (n=10) CPC-gold (cast post and core made of gold alloy), CPC-Ni (cast post and core made of Ni-Cr alloy), FP (glass fiber posts), FP-W (glass fiber posts with a wider coronal diameter), and FP-CR (fiber posts relined with composite resin). The 30 nonweakened roots were restored with (n=10) CPC-gold, CPC-Ni, and FP. All of the posts were adhesively cemented. All of the specimens were mechanically cycled (37°C, 45°, 130 N, 2.2 Hz, and 1.5 million pulses) and evaluated after every 5 × 10(4) cycles to evaluate the presence of cracks as a primary outcome (event). The specimens that survived cycling were subjected to a fracture load test (load application on the palatal aspect at a 45° inclination). Failure mode was classified as favorable (above the simulated bone level) and catastrophic (below the simulated bone level). Survival rates were estimated using the Kaplan-Meier method. Fracture load data were analyzed using the Kruskal-Wallis test (α=0.05) for weakened roots, one-way analysis of variance, and Tukey test (p<0.05) for non-weakened roots, and Student t-test (p<0.05) compared nonweakened vs weakened roots for the same post system. RESULTS For the preliminary survival results, FP-W showed a higher survival rate when compared with CPC (gold/Ni). For the fracture load (N), the statistical analysis (p<0.0001) presented differences among the weakened groups: CPC-gold (541.4) = CPC-Ni (642.6) > FP (282.2) = FP-W (274.1) = FP-RC (216.6). No differences were observed for the groups that were nonweakened (majority of favorable failures): CPC-gold (459.3) = CPC-Ni (422.0) = FP (347.9). Weakened roots restored with CPC-gold promoted high values of load fracture and unfavorable failure rates. CONCLUSION Cast post and cores or fiber posts can be used for restoring nonweakened roots. However, for weakened roots, a fiber post with a wider cervical emerging diameter appears to be a better alternative when compared with cast post and cores.

Fatigue surviving, fracture resistance, shear stress and finite element analysis of glass fiber posts with different diameters

This study evaluated the shear stress presented in glass fiber posts with parallel fiber (0°) and different coronal diameters under fatigue, fracture resistance and FEA. 160 glass-fiber posts (N=160) with eight different coronal diameters were used (DT=double tapered, number of the post=coronal diameter and W=Wider - fiber post with coronal diameter wider than the conventional): DT1.4; DT1.8W; DT1.6; DT2W; DT1.8; DT2.2W; DT2; DT2.2. Eighty posts were submitted to mechanical cycling (3×10(6) cycles; inclination: 45°; load: 50N; frequency: 4Hz; temperature: 37°C) to assess the surviving under intermittent loading and other eighty posts were submitted to fracture resistance testing (resistance [N] and shear-stress [MPa] values were obtained). The eight posts types were 3D modeled (Rhinoceros 4.0) and the shear-stress (MPa) evaluated using FEA (Ansys 13.0). One-way ANOVA showed statistically differences to fracture resistance (DT2.2W and DT2.2 showed higher values) and shear stress values (DT1.4 showed lower values). Only the DT1.4 fiber posts failed after mechanical cycling. FEA showed similar values of shear stress between the groups and these values were similar to those obtained by shear stress testing. The failure analysis showed that 95% of specimens failed by shear. Posts with parallel fiber (0°) may suffer fractures when an oblique shear load is applied on the structure; except the thinner group, greater coronal diameters promoted the same shear stresses.

Influence of periodontal ligament simulation on bond strength and fracture resistance of roots restored with fiber posts

Objective Considering that periodontal ligament simulation may influence the stress distribution over teeth restored with intraradicular retainers, this study aimed to assess the combined effect of mechanical cycling and periodontal ligament simulation on both the bond strength between fiber posts and root dentin and the fracture resistance of teeth restored using glass fiber posts. Material and Methods Ninety roots were randomly distributed into 3 groups (n=10) (C-MC: control; P-MC: polyether; AS-MC: addition silicone) to test bond strength and 6 groups (n=10) (C: control; P: polyether; AS: addition silicone, without mechanical cycling, and C-MC, P-MC and AS-MC with mechanical cycling) to test fracture strength, according to the material used to simulate the periodontal ligament. For the bond strength test, fiber posts were cemented, cores were built, mechanical cycling was applied (2×106 cycles, 88 N, 2.2 Hz, and 45º incline), and the teeth cut into 3 slices (2 mm), which were then subjected to the push-out test at 1 mm/min. For the fracture strength test, fiber posts were cemented, cores were built, and half of the groups received mechanical cycling, followed by the compressive strength (45° to the long axis and 1 mm/min) performed on all groups. Results Periodontal ligament simulation did not affect the bond strength (p=0.244) between post and dentin. Simulation of periodontal ligament (p=0.153) and application of mechanical cycling (p=0.97) did not affect fracture resistance. Conclusions The materials used to simulate the periodontal ligament did not affect fracture or bond strength, therefore periodontal ligament simulation using the tested materials could be considered optional in the conditions of the study.

Mechanical behavior of yttria-stabilized tetragonal zirconia polycrystalline ceramic after different zirconia surface treatments

This study investigated the effects of different zirconia surface conditioning methods on the biaxial flexure strength, surface characteristics and fractographic analysis of a Y-TZP ceramic. Disc-shaped specimens were manufactured according to ISO 6872-2008 for biaxial flexure strength testing, and then randomly assigned into seven groups (n=30). Control (CTRL): without treatment; Tribochemical silica coating (TBS): specimens were sandblasted with silica-coated aluminum oxide particles (CoJet-Sand) for 10s; Silica nanofilm (SNF): specimens were silica coated with a 5nm SiO2 nanofilm; and four protocols of low-fusing porcelain glaze (GLZ): etching with 10% hydrofluoric acid gel (HF) for 1min (GLZ1), 5min (GLZ5), 10min (GLZ10) and 15min (GLZ15). Phase transformation, roughness, micro-morphological, flexural analysis tests, and fractographic analyses were performed. X-ray diffraction (XRD) analysis showed that the TBS promoted the highest m-phase content (20.35). However, for the GLZ groups, XRD analysis was not sensitive enough to obtain an accurate reading for phase transformation. The GLZ group had the highest roughness values. The TBS group had the highest characteristic strength (1291.38MPa), followed by SNF (999.26MPa). These results suggest that (TBS) and (SNF) treatments did not reduce the mechanical properties, while (GLZ) led to a degradation in the mechanical properties.

Fiber-matrix integrity, micromorphology and flexural strength of glass fiber posts: Evaluation of the impact of rotary instruments.

Several rotary instruments have been daily employed on clinic to promote cut aiming to adjust the length of fiber posts to the radicular conduct, but there is no information on the literature about the effects of the different rotary instruments and its impact on the micromorphology of surface and mechanical properties of the glass fiber post. This study aimed the impact of rotary instruments upon fiber-matrix integrity, micromorphology and flexural-strength of glass-fiber posts (GFP). GFP (N=110) were divided into 5 groups: Ctrl: as-received posts, DBc: coarse diamond-bur, DBff: extra-fine diamond-bur, CB: carbide-bur, DD: diamond-disc. Cutting procedures were performed under abundant irrigation. Posts exposed to rotary instruments were then subjected to 2-point inclined loading test (compression 45°) (n=10/group) and 3-point flexural-strength test (n=10/group). Fiber-matrix integrity and micromorphology at the cut surface were analyzed using a SEM (n=2/group). Cutting procedures did not significantly affect the 2-point (51.7±4.3-56.7±5.1 MPa) (p=0.0233) and 3-point flexural-strength (671.5±35.3-709.1±33.1 MPa) (p=0.0968) of the posts (One-way ANOVA and Tukey׳s test). Fiber detachment was observed only at the end point of the cut at the margins of the post. Cut surfaces of the CB group were smoother than those of the other groups. After 3-point flexural strength test, fiber-matrix separation was evident at the tensile side of the post. Rotary instruments tested with simultaneous water-cooling did not affect the resistance of the tested fiber posts but caused disintegration of the fibers from the matrix at the end of the cut, located at the margins.

Retentive Strength of Y-TZP Crowns: Comparison of Different Silica Coating Methods on the Intaglio Surfaces

OBJECTIVE To evaluate the effect of different methods of silica deposition on the intaglio surface of yttrium oxide stabilized zirconia polycrystal (Y-TZP) crowns on the retentive strength of the crowns. METHODS One hundred simplified full-crown preparations produced from fiber-reinforced polymer material were scanned, and 100 Y-TZP crowns with occlusal retentions were milled. Crown/preparation assemblies were randomly allocated into five groups (n=20) according to the treatment of the intaglio surfaces: TBS = tribochemical silica coating via air-abrasion with 30-μm silica-coated alumina particles; GHF1 = application of thin glaze layer + hydrofluoric acid (HF) etching for 1 minute; GHF5 = glaze application + HF for 5 minutes; GHF15 = glaze application + HF for 15 minutes; NANO = silica nanofilm deposition (5 nm) via magnetron sputtering. All groups received a silane application. The surfaces of the preparations (polymer) were conditioned with 10% HF for 30 seconds and silanized. The crowns were cemented with resin cement, thermocycled (12,000 cycles; 5°C/55°C), stored for 60 days, and subjected to a retentive strength test (0.5 mm/min until failure). The retention data (MPa) were analyzed using one-way analysis of variance, Tukey tests, and Weibull analysis. Failures were classified as 50C (above 50% of cement in the crown) and 50S (above 50% of cement on the substrate). RESULTS The TBS (5.6±1.7 MPa) and NANO groups (5.5±1 MPa) had higher retentive strength than the other groups (p<0.0001) and had the highest values of characteristic strength. There was no difference in Weibull modulus, except for the GHF1 group (lower values). The TBS and GHF15 groups, respectively, had 60% and 70% of their failures classified as 50C, while most of the other groups had 50S failures. CONCLUSION Tribochemical silica coating and silica nanofilm deposition on the inner surface of zirconia crowns promoted a higher retentive strength.

Color stability of ceramic laminate veneers cemented with light-polymerizing and dual-polymerizing luting agent: A split-mouth randomized clinical trial

Statement of problem The color stability of luting agents influences the esthetics of ceramic laminate veneers. Clinical studies that have evaluated the color changes of veneers cemented to enamel with light‐ and dual‐polymerizing resin cement are lacking. Purpose The purpose of this split‐mouth randomized clinical trial was to evaluate the color change and marginal discoloration of dual‐ and light‐polymerizing cement used for cementation of ceramic laminate veneers. Material and methods In 10 participants, 0.3‐mm‐thick ceramic laminate veneers were cemented on the buccal surface of the second premolars without tooth preparation. A randomized application of light‐polymerized cement was used on one side and a dual‐polymerized cement on the contralateral side. The operator and participants were blinded to the activation mode. Color was evaluated by a blinded evaluator with a spectrophotometer at 24 hours and at 2, 6, 12, and 24 months after cementation. The CIELab (&Dgr;E*ab) and CIEDE2000 (&Dgr;E*00) formulas were used to quantify color alteration, and &Dgr;a*, &Dgr;b*, and &Dgr;L* were calculated between the first and subsequent measurements. US Public Health Service guidelines were used to evaluate the marginal discoloration. Results Wilcoxon tests did not show a statistical difference in &Dgr;E*ab and &Dgr;E*00 between the groups (P>.05). At 24 months, the median &Dgr;E*ab was 2.31 (interquartile ranges [IQR]: 3.34) for the light‐polymerizing mode and 1.57 (IQR: 0.41) for the dual‐polymerizing mode, while the median &Dgr;E*00 was 1.65 for the light‐polymerizing mode (IQR: 2.34) and 1.18 for the dual‐polymerizing mode (IQR: 0.25). The thresholds for clinically acceptable color changes &Dgr;E*ab>3.46 and &Dgr;E*00>2.25 were found for both curing modes. Marginal discoloration was observed from the 2‐year assessment. Conclusions The color stability of ceramic laminate veneers was similar for both of the polymerizing modes for all evaluated periods. Marginal discoloration increased over a 2‐year period for both the light‐ and the dual‐polymerizing modes.

Translucency of IPS e.max and cubic zirconia monolithic crowns

Statement of problem. Although several monolithic zirconia ceramics have recently been introduced, the need for improved optical properties remains. The newest cubic‐zirconia has been claimed to have optimal translucency characteristics for esthetic restorations. Purpose. This in vitro study evaluated the optical properties of novel cubic ultratranslucent (UT) and supertranslucent (ST) zirconia by comparing them with lithium disilicate (L‐DIS) glass‐ceramic for the manufacture of monolithic computer‐aided design and computer‐aided manufacturing (CAD‐CAM) molar crowns. Material and methods. The UT and ST multilayered zirconia and the low‐translucency grade L‐DIS were milled. Eighty monolithic crowns were made from 2 CAD files, corresponding to thicknesses of 1.0 and 1.5 mm, and subdivided (n=20) into 4 groups: UT1.0, UT1.5, ST1.0, and L‐DIS1.5. All groups were shaded using A2 color standard. Translucency of the crowns was measured by total transmission, using a photoradiometer in a dark chamber; furthermore, the contrast ratio was analyzed using a dental spectrophotometer applied to the buccal surface of the crowns. Data were analyzed using the Kruskal‐Wallis and post hoc multiple Mann‐Whitney U tests with Bonferroni correction (&agr;=.05 divided by the number of tests performed in each set). Results. When the ceramic types were analyzed, using total transmission and contrast methods, they showed significantly different translucency levels: UT1.0>ST1.0>UT1.5>L‐DIS1.5 (total transmission P<.001). Contrast ratio evaluation yielded similar results (P≤.006); however, the differences between ST1.0 and UT1.5 were not significant. Conclusions. Both the ST1.0 and UT1.0 crowns, even at the maximum thickness tested (UT1.5), showed significantly higher translucency than L‐DIS. Zirconia translucency was improved by eliminating the tetragonal phase, which is responsible for the toughening effect; thus, further studies are advocated to investigate the mechanical resistance of cubic zirconia.

Influence of zirconia surface treatments on resin cement bonding and phase transformation

Abstract It evaluated the effects of different zirconia surface treatments on the bond strength of a resin cement to Y-TZP (yttria-stabilized tetragonal zirconia) ceramics, as well as their phase-transformations. 75 blocks (5 mm × 5 mm × 4 mm) of Y-TZP were assigned into five groups (n = 15): (tribochemical silica coating - TBS) zirconia surface was abraded by silica coated alumina particles followed by silanization; (GLZ1) zirconia surface received the application of a thin layer of low-fusing porcelain glaze, followed by hydrofluoric acid (HF) etching for 1 min; (GLZ5) glaze application + HF etching by 5 min; (GLZ10) glaze application + HF etching by 10 min; (GLZ15) glaze application + HF etching by 15 min. After etching, all the specimens were washed, dried and silanized. Cylinders of composites (diameter: 3.25 mm; height: 3 mm) were cemented to the Y-TZP blocks using a resin cement. All the specimens were subjected to aging (10,000 thermal cycles and 90 days storage), tested under shear conditions, and finally analyzed by a stereomicroscope (failure analysis). In addition, we also performed topographical and phase transformation analyses of the treated zirconia surfaces. The TBS group presented the highest bond strength value (23.34 MPa). The glazed groups presented low bond values and high prevalences of pretest failures. X-ray diffraction analysis showed a phase transformation for the TBS group (13.14%); however, there was no clear phase change observed for the GLZ groups. From our results, we concluded that tribochemical silica coating is the main Y-TZP surface conditioning for resin bond improvements.

Mechanical behavior of yttria-stabilized tetragonal zirconia polycrystal: Effects of different aging regimens

This study aimed to characterize and compare the effect of different aging regimens on surface characteristic (topography and roughness), structural stability (phase transformation) and mechanical performance (Weibull analysis) of a Y-TZP ceramic. Discs (15 × 1.2 mm; VITA In-Ceram YZ) were prepared according to ISO 6872-2015 for biaxial flexural strength testing and randomly assigned into five groups (n = 30): as-sintered, no aging treatment (CTRL); 20 h in autoclave at 134°C, 2 bar pressure (AUT); intermittent mechanical loading at 20 Hz/106 load pulses (MechLoad); AUT followed by MechLoad (AUT+MechLoad); and storage in distilled water at 37°C, for 1 year (STO). The following analyses were performed: roughness (n = 30), surface topography (n = 2), phase transformation (n = 2) and biaxial flexure strength (n = 30). Phase transformation (increase of m-phase content) was shown to be a spontaneous, unavoidable and time-dependent process, occurring even under ambient conditions (dry storage after 1 year = 6.0% increase), and is considerably accelerated in the presence of moisture (STO = 17.6%; AUT= 63.1%; and AUT+MechLoad = 59.9%). For roughness parameters, only Ra was affected by aging, and the highest values were observed for AUT+MechLoad (0.25 ± 0.07 µm). For Weibull analysis, structural reliability (Weibull moduli) and characteristic strength were not impaired after aging, and some aging conditions led to increased values (highest weibull moduli in AUT, and highest characteristic strength in STO). Phase transformation proves to be a time-dependent spontaneous mechanism that is accelerated in the presence of different stimuli. However, none of the aging regimens had a negative effect on the characteristic strength and structural reliability of Y-TZP ceramic.