Wei Min Mao

An OIM Analysis on the Deformation Mechanism in Hot Compressed AZ31 Magnesium Alloy

Orientation mapping based on EBSD technique was applied to analyze the rules of orientation evolution of grains in AZ31 magnesium alloy. Results show that not only under deformation strain rate of 1×10-2s-1, but under 4×10-4s-1(the superplastic deformation condition), grains in all samples with initial textures rotate gradually to near basal orientation ({0002} || compression plane) at different ways, and basal texture becomes stronger with increasing strain, which indicates plastic slip plays an important role during hot deformation. Otherwise, no evident non-basal pyramidal slip of as some studies mentioned was observed in the sample with the initial basal texture, and the basal orientation is kept unchanged during the deformation process, which suggests that basal slip is the uppermost plastic slip mechanism in this sample. In addition, the phenomenon of viscous laminar flow was observed in the sample with initial basal texture.

Inspection of Adiabatic Shear Bands in High Manganese TRIP Steels

Adiabatic shear bands (ASBs) develop generally during high strain rates. This paper investigates the transformation induced plasticity (TRIP) effect during ASBs formation at high strain rates in high manganese TRIP steels containing initial austenite and ferrite by EBSD technique. Results show that TRIP effect takes place mainly before the formation of ASBs. After ASBs formation, TRIP effect is strongly restricted by the size effect, the increase of stacking fault energy (SFE) and even inverse martensitic transformation due to the rise of temperature. The TRIP effect before ASBs formation contributes to the resistance of adiabatic shear failure. Dynamic recrystallization driven by subgrains rotation occurs within ASBs, and ultrafine grains often show strong shear textures with twin relationship owing to slip mechanism.

Abnormal Growth Mechanisms of Goss Grains in Grain-Oriented Electrical Steels

The possible mechanisms concerning abnormal growth of Goss grains in grain oriented electrical steels were investigated. The density of inhibitor particles near sheet surface, where the Goss grains located, was lower than that in center layer before secondary recrystallization, and the grains near surface could grow more easily because of reduced pinning effect. Few Goss grains could survive the growth competition and reach the sheet surface, after which the inhibitor particles inside the Goss grains coarsened slower. The phenomenon resulted in easy growth of the Goss grains at the expense of smaller neighboring grains while they could hardly be consumed by larger neighboring grains during the high temperature secondary recrystallization. Very large final size of the Goss grains was then obtained. The mechanisms were discussed based on the hot rolling characteristics and the elastic anisotropy of the ferrite matrix.

Characteristics of Hot Compressed Magnesium Alloy AZ31 with Initial Textures Analyzed by Orientation Mapping

Orientation mapping based on EBSD technique was applied to reveal the orientations of new grains and their relationships to the surrounding matrices, to analyze Kikuchi band contrast and the influence of strain rates on local orientation evolution. This information is used to understand the dynamic recrystallization mechanism and the relative contribution of plastic slip versus grain boundary glide or grain rotation related with super-plasticity. For this purpose samples with different initial textures were deformed by (quasi-)plain strain compression at two strain rates. It is suggested that the dynamic recrystallization in this alloy proceeds in continuous way by progressive subgrain rotation. No evident non-basal slip of was observed by referring texture evolution in the sample with initial basal texture. A high strain rate promotes more contribution of plastic slip accompanied by fast orientation changes. The fact that groups of grains with very similar orientations in basal oriented samples is discussed in terms of viscous flow.

Reaction Stress Model and Relaxation of Reaction Stress among the Grains during Tensile Deformation of fcc Metals

A reaction stress model is introduced in this paper and its applications for the crystallographic texture simulation are also discussed with the comparison to the classic Taylor type model and the self consistent model. This model took the external deformation stress tensor as an initial point, and the activation process of slip systems as well as the orientation evolutions was simulated step by step. Certain relaxation of reaction stress were introduced during tensile or drawing deformation, which predicts the tensile direction distribution along the orientation line between <111> and <100> in the inverse pole figure besides the <111> and <100> fiber texture. The simulation agrees with the common experimental observations. The model supplies a simple way to follow the deformation process in the main part of polycrystals, in which the effect of grain orientation and its interaction with the surrounding matrix are considered.

Effects of Driving Force and Boundary Migration Velocity on Formation of Recrystallization Texture in Cold Rolled Pure Aluminum Sheets

The effects of net driving force for migration of high angle grain boundaries were emphasized beside many other factors which could influence the process of texture formation during recrystallization annealing of 95% cold rolled pure aluminum sheets. The net driving force consists basically of stored energy. However, it could be reduced by recovery, boundary drag, solute drag and Zener drag in different extents, in which only boundary drag is mis-orientation dependent. It was indicated that both oriented nucleation and oriented growth have obvious influence on recrystallization texture, and how far they influence the texture depends also on the level of net driving force when the grain growth starts during annealing. Oriented growth, which is induced by the differences in boundary drag of differently oriented grains, and the corresponding texture formation, could be observed easily when the recrystallization proceeds under relative higher solute drag and Zener drag in commercial purity aluminum. The oriented nucleation process prevails during recrystallization of sufficiently recovered high purity aluminum with very low solute drag and Zener drag, after which strong cube texture forms. In this case the oriented growth indicates limited effect. Both the oriented growth and oriented nucleation will fail if high purity deformation matrix without clear solute drag and Zener drag has not experienced an obvious recovery before recrystallization grain growth, since extremely high net driving force leads to very small critical nucleus size and multiplicity of growing grains, which results in randomization of recrystallization texture.

Research on the Composite Slurry Preparation and Rheocasting of Aluminum Alloy

The study on new rheoforming technologies of semisolid alloys has recently been one main subject interesting many professors, experts and industrials, and so many new methods about preparing semisolid alloy slurry and rheoforming process have been put forward. The semisolid slurry of AlSi7Mg alloy was prepared by being poured at a low superheat and stirred by an electromagnetic field at a low power for a short time, and then the slurry was further soaked for proper time and finally rheoformed into a key-shaped die cavity in this paper. The influence of slurry temperature, injection specific pressure and injection speed on the rheoforming process was also studied. The experimental results show that if AlSi7Mg alloy melt is poured at 630°C or 650°C and meanwhile stirred by an electromagnetic field at a low power for a short time, the most primary α-Al grains solidified in the slurry are spherical and only a few are rosette-like. If the slurry after made is then soaked in the liquidus-solidus range for some time, the ripening of primary α-Al grains is developed further and they become more spherical and larger. The experimental results also show that the slurry temperature, injection pressure and speed have a great influence on filling ability. The higher the slurry temperature, injection pressure and speed, the higher the slurry filling ability, and the shorter the core distance from the ingate, the more easily the die cavity is filled. With the given key-shaped casting, if only the slurry temperature should be equal to or more than 585,, or the injection pressure is equal to or more than 20 MPa, or the injection speed should be equal to or more than 1.73m/s, the key-shaped die cavity can be filled completely. The microstructural distribution in the casting is very homogeneous and it shows that the slurry prepared by the new method is very suitable for rheoforming and helpful to obtaining high quality castings.

Residual Stress Analysis of Microwave Plasma CVD Diamond Films

The residual stress and crystallographic texture of diamond films were investigated in the present work. The diamond films were synthesized on (100) silicon wafer by Microwave Plasma Chemical Vapor deposition (MPCVD). Then the residual stresses of the films were measured by X-ray diffractometer equipped with the two-dimensional detector. The residual stresses can be classified into two categories, i.e., the intrinsic stresses and the thermal stresses. It was shown that the thermal stresses were compressive in the temperature range studied and the intrinsic stresses were tensile. The crystallographic textures of the films were measured by X-ray diffractometer with the method of pole figure and orientation distribution function (ODF). The experimental results suggest that the crystallographic textures of the films depend upon the deposition temperature and methane flow rates, and the components and intensity of crystallographic textures have effect on the residual stresses in diamond films to a certain extent.

Microstructure and Texture in Free-Standing CVD Diamond Films

Free-standing CVD diamond films were prepared under the substrate temperature in the range of 850-1050oC. Macro- and micro-textures of the films were investigated based on the SEM observation as well as on the ODF and EBSD analysis. It was found that certain growth selection process appeared during diamond deposition which, however, did not lead to a strong film texture. It is indicated that strong fluctuation of growth ratio V<100>/V<111> and frequent growth twinning during film deposition resulted in randomization effect of grain orientations, which can be transformed by adjusting the parameters of film preparation.

Effect of Mechanical Stirring and Air Pressure on the Fluidity of SiCp/A357 Composites

Stir casting is a near net shape process that can cast the composite components directly. Fluidity is an important factor for mold filling in casting process, but the fluidity of composite slurry is poor due to the addition of SiCp. In this research, SiCp/A357 composites with 20wt.% SiCp were manufactured by mechanical stir casting. Effect of mechanical stirring and air pressure on the fluidity of SiCp/A357 composites were investigated with eight thin flow channels. The fluidity was compared at different rotating speed and air pressure. The results showed that the fluidity increased with rotating speed, which was more obvious in semi-solid interval. It was noticed that the fluidity decreased with air pressure, the gas involving and the cooling speed were aggravated with air pressure increasing, which reduced the fluidity.