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Featured researches published by Xi Ke.


ACS Applied Materials & Interfaces | 2013

Porous Co3O4 Nanorods–Reduced Graphene Oxide with Intrinsic Peroxidase-Like Activity and Catalysis in the Degradation of Methylene Blue

Zhe Zhang; Jinhui Hao; Wenshu Yang; Baoping Lu; Xi Ke; Bailin Zhang; Jilin Tang

A facile two step process was developed for the synthesis of porous Co3O4 nanorods-reduced graphene oxide (PCNG) hybrid materials based on the hydrothermal treatment cobalt acetate tetrahydrate and graphene oxide in a glycerol-water mixed solvent, followed by annealing the intermediate of reduced graphene oxide-supported Co(CO3)0.5(OH)·0.11H2O nanorods in a N2 atmosphere. The morphology and microstructure of the composites were examined by X-ray diffraction, X-ray photoelectron spectroscopy, transmission electron microscopy and Raman spectroscopy. It is shown that the obtained PCNG have intrinsic peroxidase-like activity. The PCNG are utilized for the catalytic degradation of methylene blue. The good catalytic performance of the composites could be attributed to the synergy between the functions of porous Co3O4 nanorods and reduced graphene oxide.


Journal of Materials Chemistry | 2013

In situ controllable growth of CoFe2O4 ferrite nanocubes on graphene for colorimetric detection of hydrogen peroxide

Jinhui Hao; Zhe Zhang; Wenshu Yang; Baoping Lu; Xi Ke; Bailin Zhang; Jilin Tang

A facile method is proposed for the synthesis of cubic CoFe2O4 ferrite–reduced graphene oxide nanocomposite sheets (rGO–CFs), using poly(N-vinyl-2-pyrrolidone) as the reductant and stabilizer. The rGO–CFs functioned as efficient peroxidase mimetics and were successfully applied for colorimetric assay. The morphology and composition of the rGO–CFs were characterized by transmission electron microscopy, X-ray photoelectron spectroscopy, and X-ray diffraction. Significantly, the peroxidase-like activity of the rGO–CFs followed typical Michaelis–Menten kinetics and showed a good affinity to 3,3,5,5-tetramethyl benzidine. Under optimum conditions, the colorimetric assay showed a lower detection limit (S/N = 3) of 0.3 μM when compared with that of other nanoparticle based colorimetric assays. Furthermore, the cubic nanostructured rGO–CFs exhibited better stability than horseradish peroxidase when they were exposed to solutions with different solvents and temperatures. These excellent properties made the cubic nanostructured rGO–CFs an ideal candidate for a wide range of potential applications as peroxidase mimetics.


Journal of Colloid and Interface Science | 2013

One-pot solvothermal synthesis of graphene-supported TiO2 (B) nanosheets with enhanced lithium storage properties

Zhe Zhang; Qingxin Chu; Huiyan Li; Jinhui Hao; Wenshu Yang; Baoping Lu; Xi Ke; Jing Li; Jilin Tang

A facile process was developed for the synthesis of graphene-supported TiO2 (B) nanosheets (GTBN) composite based on the hydrothermal treatment titanium (III) chloride and graphene oxide in an ethylene glycol. The morphology and microstructure of the composites were examined by X-ray diffraction, X-ray photoelectron spectroscopy, transmission electron microscopy, and Raman spectroscopy. The obtained GTBN show a high thermal stability and the phase transformation of TiO2 (B) to anatase can be prevented by graphene after pyrolysis of GTBN at 350°C for 2h. Furthermore, GTBN exhibited high rate performance and stability of lithium ion batteries, due to the enhanced conductivity of the electrode and accommodation to volume/strain changes during lithium insertion-extraction.


Journal of Colloid and Interface Science | 2014

Facile synthesis of three dimensional hierarchical Co-Al layered double hydroxides on graphene as high-performance materials for supercapacitor electrode.

Jinhui Hao; Wenshu Yang; Zhe Zhang; Baoping Lu; Xi Ke; Bailin Zhang; Jilin Tang

A facile simple hydrothermal method combined with a post-solution reaction is developed to grow interconnected three dimensional (3D) hierarchical Co-Al layered double hydroxides (LDHs) on reduced graphene oxide (rGO). The obtained 3D hierarchical rGO-LDHs are characterized by field emission scanning electron microscopy, X-ray diffraction, and X-ray photo-electron spectroscopy. As LDHs nanosheets directly grow on the surface of rGO via chemical covalent bonding, the rGO could provide facile electron transport paths in the electrode for the fast Faradaic reaction. Moreover, benefiting from the rational 3D hierarchical structural, the rGO-LDHs demonstrate excellent electrochemical properties with a combination of high charge storage capacitance, fast rate capability and stable cycling performance. Remarkably, the 3D hierarchical rGO-LDHs exhibit specific capacitance values of 599 F g(-1) at a constant current density of 4 A g(-1). The rGO-LDHs also show high charge-discharge reversibility with an efficiency of 92.4% after 5000 cycles.


ChemPhysChem | 2012

Facile Fabrication of SERS Arrays through Galvanic Replacement of Silver onto Electrochemically Deposited Copper Micropatterns

Xi Ke; Baoping Lu; Jinhui Hao; Jing Zhang; Haiyan Qiao; Zhe Zhang; Chunyan Xing; Wenshu Yang; Bailin Zhang; Jilin Tang

Scatter me: A fast and cost-effective approach for the fabrication of surface-enhanced Raman scattering (SERS) arrays is developed. The method applied combines microcontact printing, electrodeposition, and galvanic replacement without the need for expensive instruments and intricate processing. The as-prepared arrays show excellent SERS activity and high reproducibility for Rhodamine 6G.


Journal of Structural Biology | 2013

Study of the interactions between the key spore coat morphogenetic proteins CotE and SpoVID.

Haiyan Qiao; Daniela Krajcikova; Chunyan Xing; Baoping Lu; Jinhui Hao; Xi Ke; Hongda Wang; Imrich Barák; Jilin Tang

The capability of Bacillus subtilis spores to withstand extreme environmental conditions is thought to be conferred especially by their outermost proteinaceous protective layer, called the spore coat. Of the over 70 proteins that form the spore coat, only a small subset of them affect its morphogenesis, they are referred to as morphogenetic proteins. In this study we investigated the interaction between two spore coat morphogenetic proteins SpoVID and CotE. SpoVID is involved in the process of spore surface encirclement by individual coat proteins, these include CotE, which controls the assembly of the outer coat layer. Both proteins were proposed to be recruited to a common protein scaffold, but their direct association has not been previously shown. Here we studied the interactions between CotE and SpoVID in vitro for the first time by using molecule recognition force spectroscopy, which allows the detection of piconewton forces between conjugated biological pairs and also facilitates the investigation of dynamic processes. The most probable CotE-CotE unbinding force was 49.4±0.1pN at a loading rate of 3.16×10³ pN/s while that of SpoVID-CotE was 26.5±0.6pN at a loading rate of 7.8×10² pN/s. We further analyzed the interactions with the bacterial two hybrid system and pull-down experiments, which also indicate that SpoVID interacts directly with CotE. In combination with the previously identified direct contacts among SpoIVA, SpoVID and SafA, our data imply that the physical association of key morphogenetic proteins forms a basic skeleton where other coat proteins could be attached.


Talanta | 2013

Label-free detection of single-stranded DNA binding protein based on a cantilever array

Hui Hou; Xiaojing Bai; Chunyan Xing; Baoping Lu; Jinhui Hao; Xi Ke; Ningyu Gu; Bailin Zhang; Jilin Tang

We report a simple and sensitive method for label-free detection of single-stranded DNA-binding protein (SSBP) based on an array of microfabricated cantilevers. The single-stranded DNA (ssDNA) was immobilized on the surface of the sensing cantilevers to detect SSBP, while the reference cantilevers were modified with 6-mercapto-1-hexanol to detect any unwanted cantilever deflection. The differential deflection signals that reveal specific SSBP-ssDNA binding have been found to depend on the SSBP concentration. Using the cantilever array sensor we can detect SSBP in the concentration range from 0.01 to 7 μg mL(-1). Other proteins, such as thrombin or bovine serum albumin induced no significant deflection of the cantilevers. Our results show the potential for the application of cantilever array sensor system as a powerful tool to detect proteins with high sensitivity and specificity.


ChemPhysChem | 2013

A simple method for fabricating patterned curvilinear microstructures in poly(dimethylsiloxane) by selective wetting.

Xi Ke; Jilin Tang

The fabrication of patterned microstructures in poly(dimethylsiloxane) (PDMS) is a prerequisite for soft lithography. Herein, curvilinear surface relief microstructures in PDMS are fabricated through a simple three-stage approach combining microcontact printing (μCP), selective surface wetting/dewetting and replica molding (REM). First, using an original PDMS stamp (first-generation stamp) with linear relief features, a chemical pattern on gold substrate is generated by μCP using hexadecanethiol (HDT) as an ink. Then, by a dip-coating process, an ordered polyethylene glycol (PEG) polymer-dot array forms on the HDT-patterned gold substrate. Finally, based on a REM process, the PEG-dot array on gold substrate is used to fabricate a second-generation PDMS stamp with microcavity array, and the second-generation PDMS stamp is used to generate third-generation PDMS stamp with microbump array. These fabricated new-generation stamps are utilized in μCP and in micromolding in capillaries (MIMIC), allowing the generation of surface micropatterns which cannot be obtained using the original PDMS stamp. The method will be useful in producing new-generation PDMS stamps, especially for those who want to use soft lithography in their studies but have no access to the microfabrication facilities.


Nanoscale | 2013

Hierarchical flower-like Co3-xFexO4 ferrite hollow spheres: facile synthesis and catalysis in the degradation of methylene blue

Jinhui Hao; Wenshu Yang; Zhe Zhang; Shunhao Pan; Baoping Lu; Xi Ke; Bailin Zhang; Jilin Tang


Carbon | 2013

Amine-assisted solvothermal approach for the in situ synthesis of metal telluride/reduced graphene oxide

Baoping Lu; Xi Ke; Zhe Zhang; Jinhui Hao; Bailin Zhang; Jilin Tang

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Jilin Tang

Chinese Academy of Sciences

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Baoping Lu

Chinese Academy of Sciences

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Jinhui Hao

Chinese Academy of Sciences

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Bailin Zhang

Chinese Academy of Sciences

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Zhe Zhang

Chinese Academy of Sciences

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Wenshu Yang

Chinese Academy of Sciences

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Chunyan Xing

Chinese Academy of Sciences

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Haiyan Qiao

Chinese Academy of Sciences

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Jing Zhang

Chinese Academy of Sciences

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Hongda Wang

Chinese Academy of Sciences

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