Zbigniew Mitura

The Use of ADINA Software to Simulate Thixocasting Processes

The main purpose of work was to develop a methodology of physical and numerical simulation of the thixocasting processes. For the purpose of the studies an experiment was conducted using a GLEEBLE 3800 simulator. In this work, the GLEEBLE 3800 system was adapted for physical simulation of the processes of light metal alloy forming in the solid-liquid state. The physical simulations of thixoforming processes and characterization of thixotropic materials were supported by computer simulations using ADINA software. The numerical model of thixoforming processes was developed in order to estimate values of the rheological model parameters.

Algorithms for determining the phase of RHEED oscillations

Oscillations of reflection high-energy electron diffraction (RHEED) intensities are computed using dynamical diffraction theory. The phase of the oscillations is determined using two different approaches. In the first, direct, approach, the phase is determined by identifying the time needed to reach the second oscillation minimum. In the second approach, the phase is found using harmonic analysis. The two approaches are tested by applying them to oscillations simulated using dynamical diffraction theory. The phase of RHEED oscillations observed experimentally is also analysed. Experimental data on the variation of the phase as a function of the glancing angle of incidence, derived using the direct method, are compared with the values computed using both the direct and harmonic methods. For incident-beam azimuths corresponding to low-symmetry directions, both approaches produce similar results.

Computer studies on reflection high‐energy electron diffraction from the growing surface of Ge(001)

The results of calculations of reflection high-energy electron diffraction intensities, measured at different stages of the homoepitaxial growth of Ge(001), are described. A two-dimensional Bloch wave approach was used in calculations of the Schrodinger equation with a one-dimensional potential. The proportional model was used for partially filled layers, i.e. the scattering potential was taken to be proportional to the coverage and the potential of the fully filled layer. Using such an approach, it was shown that it is possible to obtain valuable information for the analysis of experimental data. The results of these calculations were compared with data for off-symmetry azimuths from the literature, and satisfactory agreement between the theoretical and experimental data was found. Also assessed was whether developing more advanced models (i.e. going beyond the proportional model), to make a more detailed account of the diffuse scattering, might be important in achieving a fully quantitative explanation of the experimental data.

Computer Investigations of Features of RHEED Oscillations for GaAs and for Ge

During molecular beam epitaxy regular oscillations of the intensity of the specularly reflected beam often occur. The phenomenon of such oscillations is still theoretically explained only partially. For example it is not clear why usually the oscillation phase depends strongly on the glancing angle of the incident beam. However, quite recently interesting results were shown in the literature on the features of RHEED oscillations observed during the growth of Ge layers. The phase of oscillations practically stays constant for a wide range of angles. So in this paper, we show results of RHEED dynamical calculations for Ge. They are presented together with results of calculations for GaAs to make analysis executed more complete. It is concluded that experimental findings for Ge for off-symmetry azimuths can be explained using dynamical diffraction theory employing the proportional model (for which the scattering potential of the layer is determined as the potential of the completed layer multiplied by the coverage).

Microstructure evolution in hot worked steel after heating to semi-solid state

Metal alloys can be formed successfully in a partially liquid state if they display a particular globular microstructure. The article presents an analysis of a study carried out of the development, by means of the strain‐induced melt‐activated method, of such a microstructure for an X210CrW12 steel. Hot rolled samples, with subsequent cooling, were heated to the temperature range at which the liquid and solid phases coexist in the material. The spheroidal shapes for solid particles, required for semi‐solid processing, were found. The investigations were carried out using scanning electron microscopy in combination with energy dispersive spectroscopy.