Zen-ichiro Morita

Measurement of bubble characteristics in a molten iron bath at 1600 °C using an electroresistivity probe

A two-needle, electroresistivity probe was developed to measure bubble characteristics such as gas holdup, bubble frequency, and bubble rising velocity in a molten iron bath at 1600 °C. The probe’s electrode was made of a 0.5-mm platinum wire coated with ZrO2 cement and an outer coat of alumina as insulator. The life of this probe at 1600 °C was 15 to 20 minutes, making it possible to systematically measure bubble characteristics. The measured values of the bubble characteristics were compared with their respective empirical correlations derived from cold model experiments. Good agreement between the measured values and the empirical correlations was seen for each bubble characteristic. This electroresistivity probe allows us to measure bubble characteristics in actual metallurgical reactors with gas injection at high bath temperatures.

Velocity and turbulence measurements in a cylindrical bath subject to centric bottom gas injection

Laser Doppler velocimeter (LDV) measurements were made to clarify the fluid flow behavior in a bath subject to centric bottom gas injection. Correlations of the axial mean velocity and turbulence components in the gas-liquid two-phase flow region,i.e., in the bubbling jet region, were proposed as functions of the inner diameter of nozzle, gas flow rate, and densities of gas and liquid. Measured values of the flow rate, momentum, and kinetic energy of water rising upward were approximated satisfactorily by these empirical correlations. In addition, the Reynolds shear stress was calculated and compared with measured values.

Water model experiment on the liquid flow behavior in a bottom blown bath with top layer

Water model experiments were performed to study the effect of top slag on the mean flow and turbulence characteristics in a steel bath agitated by bottom gas injection. The slag was modeled by silicone oil with a density of 0.968 g/cm3 and a kinematic viscosity 100 times larger than that of water at 25 °C. Velocity measurements were made using a two-dimensional (2-D) laser Doppler velocimeter (LDV) in the absence of swirl motions. The output signals of the LDV system were processed on a personal computer to obtain the axial and radial mean velocity components, the root-mean-square (rms) values of the axial and radial turbulence fluctuations, the Reynolds shear stress, and the turbulence production for two cases with and without top slag. The bubbling jet (or the bubble dispersion) region was localized near the centerline of the bath by the presence of the top oil layer. The mean flow and turbulence motions in the recirculation region located outside the bubbling jet region were also suppressed significantly by the top layer. This result could be attributed to the entrainment of top slag into steel in a real system.

Model Study of Bubble and Liquid-Flow Characteristics in a Bottom Blown Bath under Reduced Pressure

Gas injection techniques are widely used in metals refining processes. Pressure on the bath surface of reactors is sometimes highly reduced to enhance the efficiency of refining. Many fundamental and practical investigations have been made to clarify the effects of reduced surface pressure on the mixing time and reaction rates of decarburization or desulfurization in the bath. However, details of these effects are not fully understood yet. Since the mixing time and chemical reaction rates are closely associated with fluid flow phenomena in the bath, information on, for example, the total surface area of bubbles rising in the bath and liquid flow induced by the buoyancy force of the bubbles should be accumulated as much as possible. In this study, the so-called water-model experiments were carried out to reveal the effects of reduced surface pressure on the bubble and liquidflow characteristics using a two-needle electroresistivity probe and a two-dimensional laser Doppler velocimeter. At an axial position near the nozzle, each bubble expanded to a volume corresponding to the hydrostatic pressure. The bubble and liquid-flow characteristics in the axial region located farther than this axial position were found to be approximately the same as those obtained under an atmospheric surface pressure.