Casey T. DeRoo

First results from a next-generation off-plane X-ray diffraction grating

Future NASA X-ray spectroscopy missions will require high throughput, high resolving power grating spectrometers. Off-plane reflection gratings are capable of meeting the performance requirements needed to realize the scientific goals of these missions. We have identified a novel grating fabrication method that utilizes common lithographic and microfabrication techniques to produce the high fidelity groove profile necessary to achieve this performance. Application of this process has produced an initial pre-master that exhibits a radial (variable line spacing along the groove dimension), high density (> 6000 grooves/mm), laminar profile. This pre-master has been tested for diffraction efficiency at the BESSY II synchrotron light facility and diffracts up to 55 % of incident light into usable spectral orders. Furthermore, tests of spectral resolving power show that these gratings are capable of obtaining resolving powers well above 1300 (λ/Δλ) with limitations due to the test apparatus, not the gratings. Obtaining these results has provided confidence that this fabrication process is capable of producing off-plane reflection gratings for the next generation of X-ray observatories.

Lynx Mission concept status

Lynx is a concept under study for prioritization in the 2020 Astrophysics Decadal Survey. Providing orders of magnitude increase in sensitivity over Chandra, Lynx will examine the first black holes and their galaxies, map the large-scale structure and galactic halos, and shed new light on the environments of young stars and their planetary systems. In order to meet the Lynx science goals, the telescope consists of a high-angular resolution optical assembly complemented by an instrument suite that may include a High Definition X-ray Imager, X-ray Microcalorimeter and an X-ray Grating Spectrometer. The telescope is integrated onto the spacecraft to form a comprehensive observatory concept. Progress on the formulation of the Lynx telescope and observatory configuration is reported in this paper.

Thermal forming of glass substrates for adjustable optics (Conference Presentation)

The proposed Lynx telescope is an X-ray observatory with Chandra-like angular resolution and about 30 times larger effective area. The technology under development at SAO is based on the deposition of piezoelectric material on the back of glass substrates, used to correct longer wavelength figure errors. This requires a large number (about 8000) of figured segments with sufficient quality to be in the range of correctibility of the actuators. Thermal forming of thin glass offers a convenient approach, being based on intrinsically smooth surfaces (which doesn’t require polishing or machining), available in large quantity and at a low cost from flat display industry. Being a replica technique, this approach is particularly convenient both for development and for the realization of modular/segmented telescopes. In this paper we review the current status and the most recent advances in the thermal forming activities at SAO, and the perspectives for the employment of these substrates for the adjustable X-Ray optics.

Line spread functions of blazed off-plane gratings operated in the Littrow mounting

Abstract. Future soft x-ray (10 to 50 Å) spectroscopy missions require higher effective areas and resolutions to perform critical science that cannot be done by instruments on current missions. An x-ray grating spectrometer employing off-plane reflection gratings would be capable of meeting these performance criteria. Off-plane gratings with blazed groove facets operating in the Littrow mounting can be used to achieve excellent throughput into orders achieving high resolutions. We have fabricated two off-plane gratings with blazed groove profiles via a technique that uses commonly available microfabrication processes, is easily scaled for mass production, and yields gratings customized for a given mission architecture. Both fabricated gratings were tested in the Littrow mounting at the Max Planck Institute for Extraterrestrial Physics (MPE) PANTER x-ray test facility to assess their performance. The line spread functions of diffracted orders were measured, and a maximum resolution of 800±20 is reported. In addition, we also observe evidence of a blaze effect from measurements of relative efficiencies of the diffracted orders.

Performance testing of an off-plane reflection grating and silicon pore optic spectrograph at PANTER

Abstract. An x-ray spectrograph consisting of aligned, radially ruled off-plane reflection gratings and silicon pore optics (SPO) was tested at the Max Planck Institute for Extraterrestrial Physics PANTER x-ray test facility. SPO is a test module for the proposed Arcus mission, which will also feature aligned off-plane reflection gratings. This test is the first time two off-plane gratings were actively aligned to each other and with an SPO to produce an overlapped spectrum. We report the performance of the complete spectrograph utilizing the aligned gratings module and plans for future development.

Pushing the boundaries of X-ray grating spectroscopy in a suborbital rocket

The Off-Plane Grating Rocket Experiment (OGRE) will greatly advance the current capabilities of soft X-ray grating spectroscopy and provide an important technological bridge towards future X-ray observatories. The OGRE sounding rocket will fly an innovative X-ray spectrograph operating at resolving powers of R ~ 2000 and effective areas < 100 cm2 in the 0.2–1.5 keV bandpass. This represents a factor of two improvement in spectral resolution over currently operating instruments. OGRE will observe the astrophysical X-ray calibration source Capella, which has a linedominated spectrum and will showcase the full capabilities of the OGRE spectrograph. We outline the mission design for OGRE and provide detailed overviews of relevant technologies to be integrated into the payload, including slumped glass mirrors, blazed reflection gratings customized for the off-plane mount, and electron-multiplying CCDs (EMCCDs). The OGRE mission will bring these components to a high technology readiness level, paving the way for the use of such a spectrograph on future X-ray observatories or Explorer-class missions.

X-ray verification of an optically aligned off-plane grating module

Off-plane x-ray reflection gratings are theoretically capable of achieving high resolution and high diffraction efficiencies over the soft x-ray bandpass, making them an ideal technology to implement on upcoming x-ray spectroscopy missions. To achieve high effective area, these gratings must be aligned into grating modules. X-ray testing was performed on an aligned grating module to assess the current optical alignment methods. Results indicate that the grating module achieved the desired alignment for an upcoming x-ray spectroscopy suborbital rocket payload with modest effective area and resolving power. These tests have also outlined a pathway towards achieving the stricter alignment tolerances of future x-ray spectrometer payloads, which require improvements in alignment metrology, grating fabrication, and testing techniques.

Design and fabrication of adjustable x-ray optics using piezoelectric thin films

Piezoelectric adjustable optics are being developed for high throughput, high resolution, low mass Xray mirror assemblies. These optics require robust piezoelectric thin films and reproducible lithographic patterning on curved glass substrates. This work details the cleaning of Corning Eagle XG glass substrates for thin shell X-ray mirrors by a three stage acid and solvent cleaning procedure before a 0.02 μm Ti adhesion layer and a 0.1 μm Pt bottom electrode layer was deposited using DC magnetron sputtering. Piezoelectric Pb(Zr0.52Ti0.48)0.99Nb0.01O3 thin films with a thickness of 1.5 μm were then deposited by radio frequency magnetron sputtering in three 0.5 µm layers with intermittent annealing steps in a rapid thermal annealing furnace at 650°C for 60 seconds. Defects observed in the piezoelectric thin films were linked to residue remaining on the glass after cleaning. 112 piezoelectric cells and 100 μm wide conductive Pt traces were patterned using bilayer photolithography. The photoresist layers were deposited using spin coating at 2000 and 4000 RPM to achieve uniform 1 μm thick layers, resulting in reproducibly resolved features with limiting resolutions of approximately >25 μm. The resulting mirror pieces achieved a 100% yield, with average relative permittivity of 1270, dielectric loss 0.047, coercive field 30 kV/cm and remanent polarization of 20 μC/cm2 . While the defects observed in the films appeared to have not influence on the electrical properties, additional cleaning steps using DI water were proposed to further reduce their presence.

X-RAY SPECTROSCOPY OF POTENTIAL SMALL MAGELLANIC CLOUD TYPE Ia SUPERNOVA REMNANTS AND THEIR ENVIRONMENTS

We examine three supernova remnants in the SMC, IKT 5 (supernova remnant (SNR) 0047-73.5), IKT 25 (SNR 0104-72.3), and DEM S 128 (SNR 0103-72.4), which are designated as Type Ia in the literature due to their spectra and morphology. This is troublesome because of their asymmetry, a trait not usually associated with young Type Ia remnants. We present Chandra X-ray Observatory data on these three remnants and perform a maximum likelihood analysis on their spectra. We find that the X-ray emission is dominated by interactions with the interstellar medium. In spite of this, we find a significant Fe overabundance in all three remnants. Through examination of radio, optical, and infrared data, we conclude that these three remnants are likely not Type Ia SNRs. We detect potential point sources that may be members of the progenitor systems of both DEM S 128 and IKT 5, which could suggest these could be Fe-rich core-collapse remnants.

Advancements in ion beam figuring of very thin glass plates (Conference Presentation)

The high-quality surface characteristics, both in terms of figure error and of micro-roughness, required on the mirrors of a high angular resolution x-ray telescope are challenging, but in principle well suited with a deterministic and non-contact process like the ion beam figuring. This process has been recently proven to be compatible even with very thin (thickness around 0.4mm) sheet of glasses (like D263 and Eagle). In the last decade, these types of glass have been investigated as substrates for hot slumping, with residual figure errors of hundreds of nanometres. In this view, the mirrors segments fabrication could be envisaged as a simple two phases process: a first replica step based on hot slumping (direct/indirect) followed by an ion beam figuring which can be considered as a post-fabrication correction method. The first ion beam figuring trials, realized on flat samples, showed that the micro-roughness is not damaged but a deeper analysis is necessary to characterize and eventually control/compensate the glass shape variations. In this paper, we present the advancements in the process definition, both on flat and slumped glass samples.