David B. Haviland

Intermodulation atomic force microscopy

A mode of atomic force microscopy AFM is demonstrated where an oscillating AFM cantileverhaving linear response is driven with two frequencies in the vicinity of a resonance. Newfrequencies in th ...

Nonlinearities and parametric amplification in superconducting coplanar waveguide resonators

Experimental investigations of the nonlinear properties of superconducting niobium coplanar waveguide resonators are reported. The nonlinearity due to a current dependent kinetic inductance of the center conductor is strong enough to realize bifurcation of the nonlinear oscillator. When driven with two frequencies near the threshold for bifurcation, parametric amplification with a gain of +22.4dB is observed.

Fabrication and measurement of a Nb based superconducting single electron transistor

A new four‐layer resist system was developed to fabricate small capacitance niobium tunnel junctions. Nb/AlOx/Al junctions were used to make a superconducting single electron transistor composed of two dc SQUIDs in series. The current‐voltage characteristics were measured and two types of resonant tunneling of Cooper pairs were observed at different magnetic fields.

Interaction imaging with amplitude-dependence force spectroscopy

Knowledge of surface forces is the key to understanding a large number of processes in fields ranging from physics to material science and biology. The most common method to study surfaces is dynamic atomic force microscopy (AFM). Dynamic AFM has been enormously successful in imaging surface topography, even to atomic resolution, but the force between the AFM tip and the surface remains unknown during imaging. Here we present a new approach that combines high-accuracy force measurements and high-resolution scanning. The method, called amplitude-dependence force spectroscopy (ADFS), is based on the amplitude dependence of the cantilevers response near resonance and allows for separate determination of both conservative and dissipative tip-surface interactions. We use ADFS to quantitatively study and map the nano-mechanical interaction between the AFM tip and heterogeneous polymer surfaces. ADFS is compatible with commercial atomic force microscopes and we anticipate its widespread use in taking AFM toward quantitative microscopy.

Experimental evidence for the Coulomb blockade of Cooper pair tunneling and Bloch oscillations in single Josephson junctions

We report on measurements of the current-voltage characteristics of ultrasmall Josephson junctions. The junctions were made of either Al or Pb alloy, and the leads connecting the junctions to the outside world were high resistance thin film microstrips fabricated on the chip very close to the junction. The high frequency impedance of these leads was sufficiently large to enable the observation in a single Josephson junction of the Coulomb blockade of Cooper pair tunneling, as well as evidence for the time correlation of Cooper pair tunneling (Bloch Oscillations).

Spin injection and relaxation in a mesoscopic superconductor.

We study spin transport in a superconducting nanowire using a set of closely spaced magnetic tunnel contacts. We observe a giant enhancement of the spin accumulation of up to 5 orders of magnitude on transition into the superconducting state, consistent with the expected changes in the density of states. The spin relaxation length decreases by an order of magnitude from its value in the normal state. These measurements, combined with our theoretical model, allow us to distinguish the individual spin-flip mechanisms present in the transport channel. Our conclusion is that magnetic impurities rather than spin-orbit coupling dominate spin-flip scattering in the superconducting state.

Superconducting and Insulating Behavior in One-Dimensional Josephson Junction Arrays

Experiments on one-dimensional small capacitance JosephsonJunction arrays are described. The arrays have a junctioncapacitance that is much larger than the stray capacitance ofthe electrodes, which we argue is important for observation ofCoulomb blockade. The Josephson energy can be tuned in situand an evolution from Josephson-like to Coulomb blockadebehavior is observed. This evolution can be described as asuperconducting to insulating, quantum phase transition. Inthe Coulomb blockade state, hysteretic current-voltagecharacteristics are described by a dynamic model which is dualto the resistively shunted junction model of classicalJosephson junctions.

Modulation of Cell Adhesion Complexes by Surface Protein Patterns

Cell adhesion is an important process in several biological phenomena. To investigate the formation and organization of focal adhesions, we developed a patterning approach based on electron beam lithography. Nanodots (radius <1230 nm) and nanorings (inner radius <320 nm) of fibronectin (FN) were patterned on a K-Casein background. Intracellular vinculin immunofluorescence mirrored the FN nanopatterns. Atomic force microscopy showed that FN nanodots and nanorings organize the immediate cytoskeleton into straight fibrils and diverging fibril bundles, respectively. Our results suggest that a minimum of approximately 40 FN molecules is required for a cell to form a focal adhesion.

Improving image contrast and material discrimination with nonlinear response in bimodal atomic force microscopy

Atomic force microscopy has recently been extented to bimodal operation, where increased image contrast is achieved through excitation and measurement of two cantilever eigenmodes. This enhanced material contrast is advantageous in analysis of complex heterogeneous materials with phase separation on the micro or nanometre scale. Here we show that much greater image contrast results from analysis of nonlinear response to the bimodal drive, at harmonics and mixing frequencies. The amplitude and phase of up to 17 frequencies are simultaneously measured in a single scan. Using a machine-learning algorithm we demonstrate almost threefold improvement in the ability to separate material components of a polymer blend when including this nonlinear response. Beyond the statistical analysis performed here, analysis of nonlinear response could be used to obtain quantitative material properties at high speeds and with enhanced resolution.

Coulomb blockade and coherent single-cooper-pair tunneling in single Josephson junctions.

We have measured the current-voltage characteristics of small-capacitance single Josephson junctions at low temperatures ( T< or =0.04 K), where the strength of the coupling between the single junction and the electromagnetic environment was controlled with one-dimensional arrays of dc SQUIDs. We have clearly observed Coulomb blockade of Cooper-pair tunneling and even a region of negative differential resistance, when the zero-bias resistance of the SQUID arrays is much higher than the quantum resistance h/e(2) approximately 26 kOmega. The negative differential resistance is evidence of coherent single-Cooper-pair tunneling in the single Josephson junction.