Gabriel Zieger

Toward high-sensitivity and high-resolution submillimeter-wave video imaging

Against a background of newly emerged security threats, the well-established idea of utilizing submillimeter-wave radiation for personal security screening applications has recently evolved into a promising technology. Possible application scenarios demand sensitive, fast, flexible and high-quality imaging techniques. At present, best results are obtained by passive imaging using cryogenic microbolometers as radiation detectors. Building upon the concept of a passive submillimeter-wave stand-off video camera introduced previously, we present the evolution of this concept into a practical application-ready imaging device. This has been achieved using a variety of measures such as optimizing the detector parameters, improving the scanning mechanism, increasing the sampling speed, and enhancing the image generation software. The camera concept is based on a Cassegrain-type mirror optics, an optomechanical scanner, an array of 20 superconducting transition-edge sensors operated at a temperature of 450 to 650 mK, and a closed-cycle cryogen-free cooling system. The main figures of the system include: a frequency band of 350±40 GHz, an object distance of 7 to 10 m, a circular field of view of 1.05 m diameter, and a spatial resolution in the image center of 2 cm at 8.5 m distance, a noise equivalent temperature difference of 0.1 to 0.4 K, and a maximum frame rate of 10 Hz.

Development of passive submillimeter-wave video imaging systems for security applications

Passive submillimeter-wave imaging is a concept that has been in the focus of interest as a promising technology for security applications for a number of years. It utilizes the unique optical properties of submillimeter waves and promises an alternative to millimeter-wave and X-ray backscattering portals for personal security screening in particular. Possible application scenarios demand sensitive, fast, and flexible high-quality imaging techniques. Considering the low radiometric contrast of indoor scenes in the submillimeter range, this objective calls for an extremely high detector sensitivity that can only be achieved using cooled detectors. Our approach to this task is a series of passive standoff video cameras for the 350 GHz band that represent an evolving concept and a continuous development since 2007. The cameras utilize arrays of superconducting transition-edge sensors (TES), i. e. cryogenic microbolometers, as radiation detectors. The TES are operated at temperatures below 1 K, cooled by a closed-cycle cooling system, and coupled to superconducting readout electronics. By this means, background limited photometry (BLIP) mode is achieved providing the maximum possible signal to noise ratio. At video rates, this leads to a pixel NETD well below 1K. The imaging system is completed by reflector optics based on free-form mirrors. For object distances of 3–10 m, a field of view up to 2m height and a diffraction-limited spatial resolution in the order of 1–2 cm is provided. Opto-mechanical scanning systems are part of the optical setup and capable frame rates up to 25 frames per second. Both spiraliform and linear scanning schemes have been developed. Several electronic and software components are used for system control, signal amplification, and data processing. Our objective is the design of an application-ready and user-friendly imaging system. For application in real world security screening scenarios, it can be extended using image processing and automated threat detection software.

Progress report on Safe VISITOR: approaching a practical instrument for terahertz security screening

As reported before,1, 2 Safe VISITOR (Safe VISible, Infrared and Terahertz Object recognition) is a German project to build a passive security camera which visualizes sub-mm wavelengths using cooled bolometer arrays. This camera could be used for a variety of application scenarios, such as airport screenings or to protect military camps. In all cases, a practical instrument requires ease of use, in particular a flexible installation and a straightforward usage by the security personnel. Here we present a new generation of Safe VISITOR designed to meet these requirements. The main condition for an effective operation is a high frame rate of the imager. Safe VISITOR is able to record videos up to 10 Hz, using a small array of superconducting bolometers in combination with an opto-mechanical scanner. The required cooling of the detector array is provided by a commercial pulse tube cooler with a second, self-contained cooling stage. The cooling cycle is completely automated; after 10 hours of initial cooling from room temperature the system can operate quasi-continuously. For imaging, a 50 cm diameter optics is used which is able to provide an object resolution of approximately 1.5 cm at 8 m distance. For a flexible installation, the object distance can be tuned manually between 7 and 10 m. Additionally, video streams from two commercial cameras are fused with the sub-mm stream: a CCD for visible light and a microbolometer for far infrared (14 μm). This combines the ability of identification of the person under test with the unprecedented temperature resolution at infrared and the almost perfect transmission at sub-mm. To assist a security official, all image data are displayed in various graphic renditions by a unified system software.

Development of passive submillimeter-wave video imaging systems

Passive submillimeter wave imaging is a concept that has been in the focus of interest as a promising technology for security applications for a number of years. It utilizes the unique optical properties of submillimeter waves and promises an alternative to millimeter-wave and X-ray backscattering portals for personal security screening in particular. Possible application scenarios demand sensitive, fast, and fleixible high-quality imaging techniques. Considering the low radiometric contrast of indoor scenes in the submillimeter range, this objective calls for an extremely high detector sensitivity that can only be achieved using cooled detectors. Our approach to this task is a series of passives standoff video cameras for the 350 GHz band that represent an evolving concept and a continuous development since 2007. The cameras utilize arrays of superconducting transition-edge sensors (TES), i.e. cryogenic microbolometers, as radiation detectors. The TES are operate at temperatures below 1K, cooled by a closed-cycle cooling system, and coupled to superconducting readout electronics. By this means, background limited photometry (BLIP) mode is achieved providing the maximum possible signal to noise ratio. At video rates, this leads to a pixel NETD well below 1K. The imaging system is completed by reflector optics based on free-form mirrors. For object distances of 3–10m, a field of view up to 2m height and a diffraction-limited spatial resolution in the order of 1–2cm is provided. Opto-mechanical scanning systems are part of the optical setup and capable frame rates up to 25 frames per second. Both spiraliform and linear scanning schemes have been developed.

Progress in passive submillimeter-wave video imaging

Since 2007 we are developing passive submillimeter-wave video cameras for personal security screening. In contradiction to established portal-based millimeter-wave scanning techniques, these are suitable for stand-off or stealth operation. The cameras operate in the 350GHz band and use arrays of superconducting transition-edge sensors (TES), reflector optics, and opto-mechanical scanners. Whereas the basic principle of these devices remains unchanged, there has been a continuous development of the technical details, as the detector array, the scanning scheme, and the readout, as well as system integration and performance. The latest prototype of this camera development features a linear array of 128 detectors and a linear scanner capable of 25Hz frame rate. Using different types of reflector optics, a field of view of 1×2m2 and a spatial resolution of 1–2 cm is provided at object distances of about 5–25m. We present the concept of this camera and give details on system design and performance. Demonstration videos show its capability for hidden threat detection and illustrate possible application scenarios.

Towards high-sensitivity and high-resolution submillimeter-wave video imaging

Against a background of newly emerged security threats the well-established idea of utilizing submillimeter-wave radiation for personal security screening applications has recently evolved into a promising technology. Possible application scenarios demand sensitive, fast, flexible and high-quality imaging techniques. At present, best results are obtained by passive imaging using cryogenic microbolometers as radiation detectors. Building upon the concept of a passive submillimeter-wave stand-off video camera introduced previously, we present the evolution of this concept in a practical application-ready imaging device. This has been achieved using a variety of measures such as optimizing the detector parameters, improving the scanning mechanism, increasing the sampling speed, and enhancing the camera software. The image generation algorithm has been improved and an automatic sensor calibration technique has been implemented taking advantage of redundancy in the sensor data. The concept is based on a Cassegrain-type mirror optics, an opto-mechanical scanner providing spiraliform scanning traces, and an array of 20 superconducting transition-edge sensors (TES) operated at a temperature of 450-650 mK. The TES are cooled by a closed-cycle cooling system and read out by superconducting quantum interference devices (SQUIDs). The frequency band of operation centers around 350 GHz. The camera can operate at an object distance of 7-10 m. At 9m distance it covers a field of view of 110 cm diameter, achieves a spatial resolution of 2 cm and a pixel NETD (noise equivalent temperature difference) of 0.1-0.4 K. The maximum frame rate is 10 frames per second.

Chemical and Electrochemical Synthesis of Platinum Black

We present electrochemical and chemical synthesis of platinum black at room temperature in aqueous and non-aqueous media. X-ray analysis established the purity and crystalline nature. The electron micrographs indicate that the nanostructures consist of platinum crystals that interconnect to form porous assemblies. Additionally, the electron micrographs of the platinum black thin layer, which was electrochemically deposited on different metallic and semiconductive substrates (aluminium, platinum, silver, gold, tin-cooper alloy, indium-tin-oxide, stainless steel, and copper), indicate that the substrate influences its porous features but not its absorbance characteristics. The platinum black exhibited a broad absorbance and low reflectance in the ultraviolet, visible, and infrared regions. These characteristics make this material suitable for use as a high-temperature resistant absorber layer for the fabrication of microelectronics.

Electro-architected porous platinum on metallic multijunction nanolayers to optimize their optical properties for infrared sensor application

Tailoring the physicochemical properties of the metallic multijunction nanolayers is a prerequisite for the development of microelectronics. From this perspective, a desired lower reflectance of infrared radiation was achieved by an electrochemical deposition of porous platinum in nonaqueous media on silver mirror supported nickel-chrome and nickel-titanium metallic films with incremental decreasing thicknesses from 80-10 nm. The electro-assembled architectures were examined by means of scanning electron microscopy and Fourier transform infrared spectroscopy and it was observed that the layer and sublayer thicknesses and resistivities have a substantial effect upon the porous platinum morphology and its optical properties. It is here reported that the augmentation of the metallic layer electrical conductivity determines the electroformation of more compact platinum nanolayers. Moreover, the platinum black coating of metallic nanolayers causes a considerable decrease of the reflectance in the region from 1000-8000 cm-1.Tailoring the physicochemical properties of the metallic multijunction nanolayers is a prerequisite for the development of microelectronics. From this perspective, a desired lower reflectance of infrared radiation was achieved by an electrochemical deposition of porous platinum in nonaqueous media on silver mirror supported nickel-chrom and nickel-titanium metallic films with incremental decreasing thicknesses from 80 nm to 10 nm. The electroassembled architectures were examined by means of SEM and FTIR and it was observed that the layer and sublayer thicknesses and resistivities have a substantial effect upon the porous platinum morphology and its optical properties. It is here reported that the augmentation of the metallic layer electrical conductivity determines the electroformation of more compact platinum nanolayers. Moreover, the platinum black coating of metallic nanolayers causes a considerable decrease of the reflectance in the region from 1000 cm-1 to 8000 cm-1.

Optical Assets of In situ Electro-assembled Platinum Black Nanolayers

Optoelectronic technology has been increasingly driven towards miniaturization. In this regard, maintaining the optical properties of the bulk materials while reducing their size is a critical need. How thin must the film be to preserve the bulk material´s optical absorbance and reflectance characteristics? This is the central question for our study of the in situ electro-assembly broad band optical absorber films of platinum in non-aqueous solution of PtCl4. By reducing the in situ constructed film to sub-visible-wavelength thicknesses, the measured reflectance in the region from the ultraviolet to the infrared remained close to that exhibited by the micrometre-width films. These platinum black films broadly absorb electromagnetic waves at a sub-incident-wavelength thickness owing to their plasmonically increased absorbance cross-section. Simulation of various incident energy electron trajectories gives insights into the electron depth through the porous platinum black of ρ = 1.6 g/cm3 and previews the optical behaviour close to the atomic thickness.

Optimization of the Microwave Properties of the Kinetic-Inductance Bolometer (KIBO)

Silicon nitride membrane based cryogenic bolometers exhibit high sensitivity and enable ultra-sensitive detector applications. Multi-pixel instruments were already introduced as devices for submillimeter-wave imaging. Nevertheless, the numbers of pixels are limited by the readout process which is typically a time-division multiplexing or code-division multiplexing technique. To overcome this challenge, a replacement of the transition-edge sensor as thermometer by a lumped-element resonance circuit seems to be a promising solution. Therefore, one can benefit from the intrinsic capability of frequency-division multiplexing that allows the readout of large detector arrays simultaneously and in real-time. The number of pixels is then limited by the available readout bandwidth and the quality factors of each individual resonance circuit. We successfully demonstrated, based on our feasibility study, the principal operation of such a device, what we call kinetic-inductance bolometer (KIBO). But the overall performance of the achievable noise-equivalent power (NEP) was limited by implementation and operation temperature of KIBO. Therefore, improved KIBO designs were developed and fabricated with niobium thin-film technology. In this paper, we describe the improvement procedure and estimate the expected NEP value.