John M. Moreland

A microfabricated atomic clock

Fabrication techniques usually applied to microelectromechanical systems (MEMS) are used to reduce the size and operating power of the core physics assembly of an atomic clock. With a volume of 9.5mm3, a fractional frequency instability of 2.5×10−10 at 1s of integration, and dissipating less than 75mW of power, the device has the potential to bring atomically precise timing to hand-held, battery-operated devices. In addition, the design and fabrication process allows for wafer-level assembly of the structures, enabling low-cost mass-production of thousands of identical units with the same process sequence, and easy integration with other electronics.

Chip-scale atomic magnetometer

Using the techniques of microelectromechanical systems, we have constructed a small low-power magnetic sensor based on alkali atoms. We use a coherent population trapping resonance to probe the interaction of the atoms’ magnetic moment with a magnetic field, and we detect changes in the magnetic flux density with a sensitivity of 50pTHz−1∕2 at 10Hz. The magnetic sensor has a size of 12mm3 and dissipates 195mW of power. Further improvements in size, power dissipation, and magnetic field sensitivity are immediately foreseeable, and such a device could provide a hand-held battery-operated magnetometer with an atom shot-noise limited sensitivity of 0.05pTHz−1∕2.

Microfabricated alkali atom vapor cells

We describe the fabrication of chip-sized alkali atom vapor cells using silicon micromachining and anodic bonding technology. Such cells may find use in highly miniaturized atomic frequency references or magnetometers. The cells consist of cavities etched in silicon, with internal volumes as small as 1 mm3. Two techniques for introducing cesium and a buffer gas into the cells are described: one based on chemical reaction between cesium chloride and barium azide, and the other based on direct injection of elemental cesium within a controlled anaerobic environment. Cesium optical absorption and coherent population trapping resonances were measured in the cells.

Electron tunneling experiments using Nb-Sn ''break'' junctions

An Nb‐Sn filament mounted on a flexible glass beam can be broken to form an electron tunneling junction between the fracture elements. Breaking the filament in liquid helium prevents oxidation of the freshly exposed fracture surfaces. A sharp superconducting energy gap in the I‐V characteristics measured at 4 K indicates the formation of a high‐quality tunneling barrier between the fracture elements. The resistance of the junction can be continuously adjusted by varying the surface bending strain of the beam. An estimated 0.1 nm change in the barrier thickness produces about an order of magnitude change in the resistance over the range from 105 to 108 Ω. The exponential character of this dependence shows that the tunnel junction is freely adjustable without intimate contact of the junction elements. ‘‘Break’’ junctions made in this way offer a new class of tunneling experiments on freshly exposed surfaces of a fractured sample without the oxide barrier previously required for junction stability. Such expe...

A chip-scale atomic clock based on 87Rb with improved frequency stability.

We demonstrate a microfabricated atomic clock physics package based on coherent population trapping (CPT) on the D1 line of 87Rb atoms. The package occupies a volume of 12 mm3 and requires 195 mW of power to operate at an ambient temperature of 200 degrees C. Compared to a previous microfabricated clock exciting the D2 transition in Cs [1], this 87Rb clock shows significantly improved short- and long-term stability. The instability at short times is 4 x?10-11 / tau?/2 and the improvement over the Cs device is due mainly to an increase in resonance amplitude. At longer times (tau?> 50 s), the improvement results from the reduction of a slow drift to ?5 x 10-9 / day. The drift is most likely caused by a chemical reaction of nitrogen and barium inside the cell. When probing the atoms on the D1 line, spin-exchange collisions between Rb atoms and optical pumping appear to have increased importance compared to the D2 line.

Integrated microfluidic isolation platform for magnetic particle manipulation in biological systems

We have developed a micromachined fluid-cell platform that consists of patterned magnetic thin-film elements supported on a thin silicon–nitride membrane. In the presence of an external magnetic field, the field gradients near the magnetic elements are sufficiently large to trap magnetic particles that are separated from the patterned films by a 200 nm thick nitride membrane. The two main applications of this fluid-cell platform are to provide a means to control and position magnetic microparticles, which can be tethered to biological molecules, and also to sort superparamagnetic microparticles based on their size and magnetic susceptibility. We determine the characteristic trapping forces of each trap in the array by measuring the Brownian motion of the microparticle as a function of applied external field. Typical force constants and forces on the superparamagnetic particles are 4.8×10−4±0.7×10−4 N/m and 97±15 pN, respectively.

Scanning tunneling microscopy of the surface morphology of YBa2Cu3Ox thin films between 300 and 76 K

Scanning tunneling microscopy (STM) images of YBa2Cu3Ox (YBCO) thin films show different growth mechanisms depending on the deposition method and substrate material. We present images of YBCO films sputter deposited onto MgO and SrTiO3, and laser ablated onto LaAlO3 showing screw dislocation and ledge growth mechanisms. At room temperature we observed an anomalous tunneling conductance near the edge of growth steps which causes a large apparent step‐edge height in the STM image. This effect decreases with decreasing temperature, so that the step height approaches the expected value for one unit cell of 1.2 nm at 76 K. This phenomenon reflects changes in either the surface tunneling barrier or tunneling density of states upon cooling.

Wafer-level filling of microfabricated atomic vapor cells based on thin-film deposition and photolysis of cesium azide

The thin-film deposition and photodecomposition of cesium azide are demonstrated and used to fill arrays of miniaturized atomic resonance cells with cesium and nitrogen buffer gas for chip-scale atomic-based instruments. Arrays of silicon cells are batch fabricated on wafers into which cesium azide is deposited by vacuum thermal evaporation. After vacuum sealing, the cells are irradiated with ultraviolet radiation, causing the azide to photodissociate into pure cesium and nitrogen in situ. This technology integrates the vapor-cell fabrication and filling procedures into one continuous and wafer-level parallel process, and results in cells that are optically transparent and chemically pure.

Manipulation and sorting of magnetic particles by a magnetic force microscope on a microfluidic magnetic trap platform

We have integrated a microfluidic magnetic trap platform with an external magnetic force microscope (MFM) cantilever. The MFM cantilever tip serves as a magnetorobotic arm that provides a translatable local magnetic field gradient to capture and move magnetic particles with nanometer precision. The MFM electronics have been programmed to sort an initially random distribution of particles by moving them within an array of magnetic trapping elements. We measured the maximum velocity at which the particles can be translated to be 2.2mm∕s±0.1mm∕s, which can potentially permit a sorting rate of approximately 5500particles∕min. We determined a magnetic force of 35.3±2.0pN acting on a 1μm diameter particle by measuring the hydrodynamic drag force necessary to free the particle. Release of the particles from the MFM tip is made possible by a nitride membrane that separates the arm and magnetic trap elements from the particle solution. This platform has potential applications for magnetic-based sorting, manipulati...

Microfabricated atomic clocks and magnetometers

We demonstrate the critical subsystems of a compact atomic clock based on a microfabricated physics package. The clock components have a total volume below 10 cm3, a fractional frequency instability of 6 × 10−10/τ1/2, and consume 200 mW of power. The physics package is easily adapted to function as a magnetometer with sensitivity below 50 pT Hz−1/2 at 10 Hz.