Linda Mosecker

Nitrogen in chromium-manganese stainless steels : a review on the evaluation of stacking fault energy by computational thermodynamics

Abstract Nitrogen in austenitic stainless steels and its effect on the stacking fault energy (SFE) has been the subject of intense discussions in the literature. Until today, no generally accepted method for the SFE calculation exists that can be applied to a wide range of chemical compositions in these systems. Besides different types of models that are used from first-principle to thermodynamics-based approaches, one main reason is the general lack of experimentally measured SFE values for these steels. Moreover, in the respective studies, not only different alloying systems but also different domains of nitrogen contents were analyzed resulting in contrary conclusions on the effect of nitrogen on the SFE. This work gives a review on the current state of SFE calculation by computational thermodynamics for the Fe–Cr–Mn–N system. An assessment of the thermodynamic effective Gibbs free energy, , model for the phase transformation considering existing data from different literature and commercial databases is given. Furthermore, we introduce the application of a non-constant composition-dependent interfacial energy, бγ/ε, required to consider the effect of nitrogen on SFE in these systems.

Characterization and Prediction of Flow Behavior in High-Manganese Twinning Induced Plasticity Steels: Part I. Mechanism Maps and Work-Hardening Behavior

Thermodynamic stacking fault energy (SFE) maps were developed using the subregular solution model for the Fe-Mn-Al-C system. These maps were used to explain the variations in the work-hardening behavior of high-manganese steels, both through experiments and by comparison with the published data. The suppression of the transformation induced plasticity (TRIP) mechanism, the similarity between the shape of the work-hardening rate diagrams for the produced iso-SFE materials, and an earlier onset of stage C of work hardening by decreasing SFE were shown to be efficiently predictable by the given mechanism maps. To overcome the limitations arising from studying the deformation response of high-manganese steels by SFE values alone, for example, the different work-hardening rate of iso-SFE materials, an empirical criterion for the occurrence of short-range ordering (SRO) and the consequently enhanced work-hardening, was proposed. The calculated values based on this criterion were superimposed on the thermodynamics-based mechanism maps to establish a more accurate basis for material design in high-manganese iron-based systems. Finally, the given methodology is able to clarify the work-hardening behavior of high-manganese twinning induced plasticity (TWIP) steels across an extensive range of chemical compositions.

Deformation Mechanisms of Ti6Al4V Sheet Material during the Incremental Sheet Forming with Laser Heating

ncremental sheet metal forming (ISF) is a suitable process for the production of small batch sizes. Due to the minor tooling effort and low forming forces, ISF enables the production of large components with inexpensive and light machine set-ups. Hence, ISF is an interesting manufacturing technique for aeronautical applications. Sheet metal parts in aircrafts are often made of titanium and its alloys like the high strength alloy Ti Grade5 (Ti6Al4V). The characteristic low formability of Ti6Al4V at room temperature requires forming operations on this material to be carried out at the elevated temperatures. The interaction of heating and deformation cycles results in a microstructure evolution, which is believed to have a high impact on formability and product quality. In the present work, the temperature-dependent microstructural evolution of the as-deformed parts was investigated. Longitudinal pockets with different depths were formed using a laser-assisted ISF process. The microstructural evolution and hardening of the material were analyzed with respect to the local strain in different forming depths and pocket zones. The formability of the material together with the deformation depth and the sheet thickness-reduction were found to be strongly dependent on the applied process temperatures and the activated deformation mechanisms like dislocation glide and dynamic recrystallization.

Influence of the Process Temperature on the Properties of Friction Stir Welded Blanks Made of Mild Steel and Aluminum

Hybrid components made of steel and aluminum sheet metal are a promising approach for weight reduction for automotive applications. However, lightweight components made of steel and aluminum require suitable joining technologies, particularly if forming operations follow after the welding process. Friction Stir Welding (FSW) is a promising solid-state welding technology for producing dissimilar joints of steel and aluminum. Within this work dissimilar butt joints were produced using sheet metals of mild steel DC04 and the aluminum alloy AA6016 with a thickness of about 1 mm. The FSW joints show approximately 85 % of the tensile strength of the aluminum base material. In metallographic investigations of the produced FSW blanks it was found that the microstructure in the area of the weld seam changes in the aluminum alloy due to the process temperature and plastic deformation. Due to temperature dependent changes of precipitations of the aluminum alloy, temperature measurements have been carried out during the welding process. To find an explanation of the reduction in tensile strength of the FSW joints, short time heat treatment experiments in the temperature range between 250 °C and 450 °C were performed using the aluminum base material. Heat treatments in the temperature range of the measured process temperature result in a reduction of the tensile strength of about 20 % regardless the annealing time.

Properties of Friction Stir Welded Blanks Made from DC04 Mild Steel and Aluminum AA6016

Due to increasing demands for lightweight structures in automotive applications the use of sheet metal components made from aluminium alloys is a promising approach for weight reduction. The combination of steel and aluminium in car bodies may be an interesting alternative compared to a monolithic material design. The weight of structural parts of a car body shell can be reduced if dedicated parts consist of aluminium instead of steel. This approach allows for an optimal exploitation of the material properties of both materials, bringing high strength into highly loaded areas while areas subject to lower loads are equipped with lower strength and weight. However, a multi-material design combining steel and aluminium demands for suitable joining methods, especially if a forming operation is applied to the welded sheets. In conventional fusion welding processes the formation of intermetallic phases due to the metallurgical affinity of aluminium and iron is a serious problem. Recent developments in regulated cold metal transfer (CMT) welding technologies at the Institute of Welding Technology and Joining Technology (ISF) at the RWTH Aachen promise an appropriate solution to this problem. Due to a digitally regulated arc technology, the heat input in CMT is reduced to a minimum. However, the inevitable formation of a welding bead in arc processes with filler material is a criterion of exclusion in the case of production of welds for car body shells. To achieve an optimal appearance of the body shell, the welding beads need to be removed from both sides of the sheet in a second manufacturing step. Hence, to avoid further costs, it seems expedient to search for alternative welding technologies. Friction stir welded (FSW) joints show relatively even welding beads. Furthermore, this joining method is characterised by a low process temperature, which is considerably below the melting temperature of the base materials. Hence, FSW is a promising joining technique to produce tailored blanks out of aluminium and steel. The main objective of the present paper is the evaluation of suitable process parameters for the production of FSW butt joints with a thickness of 1 mm made from the aluminium alloy AA6016-T4 and the mild steel DC04. Welding experiments using a varying rotational speed, tool offset, tool velocity, tool plunge depth and tool tilt angle were carried out. To identify the best parameters in terms of the strength of the joint, tensile tests were performed. It is shown, that an amount of approximately 85% of the tensile strength of the base material AA6016 can be achieved. Using SEM the formation of the fracture surfaces was analysed. Different fracture types were identified and the possible reasons for their occurrence are discussed. It is shown that in the case of optimal joining procedure the failure occurs in the thermomechanically affected zone in the aluminium sheet, were the plastic deformation is low. Additionally, thermography has been employed to evaluate the temperature distribution during the process. In metallographic investigations it was found that during welding the microstructure of the aluminium base material changes due to plastic deformation and temperature increase in the area of the weld seam. Using hardness measurements the change of the mechanical properties in the contact zone of both base materials and in the heat affected zone was examined. Finally, an outlook is given with respect to the possibilities of producing FSW welded sheets that can be formed using conventional deep-drawing.