Marie-Anne Descalle

Demonstration of multilayer reflective optics at photon energies above 0.6 MeV

Focusing optics operating in the soft gamma-ray photon energy range can advance a range of scientific and technological applications that benefit from the large improvements in sensitivity and resolution that true imaging provides. An enabling technology to this end is multilayer coatings. We show that very short period multilayer coatings deposited on super-polished substrates operate efficiently above 0.6 MeV. These experiments demonstrate that Bragg scattering theory established for multilayer applications as low as 1 eV continues to work well into the gamma-ray band.

Hard x-ray/soft gamma-ray telescope designs for future astrophysics missions

We present several concept designs of hard X-ray/soft λ-ray focusing telescopes for future astrophysics missions. The designs are based on depth graded multilayer coatings. These have been successfully employed on the NuSTAR mission for energies up to 80 keV. Recent advances in demonstrating theoretical reflectivities for candidate multilayer material combinations up to 400 keV including effects of incoherent scatter has given an experimental base for extending this type of designs to the soft λ-ray range. At the same time, the calibration of the in-flight performance of the NuSTAR mission has given a solid understanding and modelling of the relevant effects influencing the performance, including optical constants, roughness, scatter, non-uniformities and figure error. This allows for a realistic extension for designs going to much higher energies. Similarly, both thin slumped glass and silicon pore optics has been developed to a prototype stage which promises imaging resolution in the sub 10 arcsecond range. We present designs based on a 20 m and 50 m focal lengths with energy ranges up to 200 keV and 600 keV.

Recent Advances in Multilayer Reflective Optics for EUV/X-Ray Sources

This paper discusses the development of (i) corrosion-resistant multilayers for the 25–80 nm region (ii) multilayer mirrors for the first 0.5-NA Micro-Exposure Tools at 13.5 nm and (iii) multilayer mirrors for the soft gamma-ray range.

An x-ray optic calibration facility for high energy density diagnostics

A facility to calibrate x-ray imaging optics was built at Lawrence Livermore National Laboratory to support high energy density (HED) and inertial confinement fusion (ICF) diagnostics such as those at the National Ignition Facility and the Sandia Z-Machine. Calibration of the spectral reflectivity and resolution of these x-ray diagnostics enable absolute determination of the x-ray flux and wavelengths generated in the HED and ICF experiments. Measurement of the optic point spread function is used to determine spatial resolution of the optic. This facility was constructed to measure (1) the x-ray reflectivity to ±5% over a spectral range from 5 to 60 keV; (2) point spread functions with a resolution of 50 μm (currently) and 13 μm (future) in the image plane; and (3) optic distance relative to the x-ray source and detector to within ±100 μm in each dimension. This article describes the capabilities of the calibration facility, concept of operations, and initial data from selected x-ray optics.

Reflective multilayer optic as hard X-ray diagnostic on laser-plasma experiment

A multilayer-based optic was tested for use as an X-ray diagnostic on a laser-plasma experiment. The multilayer optic was employed to selectively pass X-rays between 55 and 100 keV. An order of magnitude improvement in signal-to-noise ratio is achieved compared to a transmission crystal spectrometer. A multilayer response model, taking into account the source size and spectral content, is constructed and the outlook for application above 500 keV is briefly discussed. LLNL-JRNL-664311.

Design and raytrace simulations of a multilayer-coated Wolter x-ray optic for the Z machine at Sandia National Laboratories

Recent breakthroughs in the fabrication of small-radii Wolter optics for astrophysics allow high energy density facilities to consider such optics as novel x-ray diagnostics at photon energies of 15-50 keV. Recently, the Lawrence Livermore National Laboratory, Sandia National Laboratories (SNL), the Smithsonian Astrophysical Observatory, and the NASA Marshall Space Flight Center jointly developed and fabricated the first custom Wolter microscope for implementation in SNLs Z machine with optimized sensitivity at 17.5 keV. To achieve spatial resolution of order 100-200 microns over a field of view of 5 × 5 × 5 mm3 with high throughput and narrow energy bandpass, the geometry of the optic and its multilayer required careful design and optimization. While the geometry mainly influences resolution and the field of view of the diagnostic, the mirror coating determines the spectral response and throughput. Here we outline the details of the design and fabrication process for the first multilayer-coated Wolter I optic for SNLs Z machine (Z Wolter), including its W/Si multilayer, and present results of raytrace simulations completed to predict and verify the performance of the optic.

Characterization and simulation of soft gamma-ray mirrors for their use with spent fuel rods at reprocessing facilities

The use of a grazing incidence optic to selectively reflect K-shell fluorescence emission and isotope-specific lines from special nuclear materials is a highly desirable nondestructive analysis method for use in reprocessing fuel environments. Preliminary measurements have been performed, and a simulation suite has been developed to give insight into the design of the x ray optics system as a function of the source emission, multilayer coating characteristics, and general experimental configurations. The experimental results are compared to the predictions from our simulation toolkit to illustrate the ray-tracing capability and explore the effect of modified optics in future measurement campaigns.

Optical instrument design of the high-energy x-ray probe (HEX-P)

The High-Energy X-ray Probe (HEX-P) is a probe-class next-generation high-energy X-ray mission concept that will vastly extend the reach of broadband X-ray observations. Studying the 2-200 keV energy range, HEXP has 40 times the sensitivity of any previous mission in the 10-80 keV band, and will be the first focusing instrument in the 80-200 keV band. A successor to the Nuclear Spectroscopic Telescope Array (NuSTAR), a NASA Small Explorer launched in 2012, HEX-P addresses key NASA science objectives, and will serve as an important complement to ESA’s L-class Athena mission. HEX-P will utilize multilayer coated X-ray optics, and in this paper we present the details of the optical design, and discuss the multilayer prescriptions necessary for the reflection of hard X-ray photons. We consider multiple module designs with the aim of investigating the tradeoff between high- and low-energy effective area, and review the technology development necessary to reach that goal within the next decade.

New simulation capability for gamma ray mirror experiments

This report provides a description of the simulation toolkit developed at Lawrence Livermore National Laboratory to support the design of nuclear safeguards experiments using grazing incidence multilayer mirrors in the energy band of uranium (U) and plutonium (Pu) emission lines. This effort was motivated by the data analysis of a scoping experiment at the Irradiated Fuels Examination Facility (IFEL) at Oak Ridge National Laboratory in FY13 and of a benchmark experiment at the Idaho National Laboratory (INL) in FY14 that highlighted the need for predictive tools built around a ray-tracing capability. This report presents the simulation toolkit and relevant results such as the simulated spectra for TMI, MOX, and ATM106 fuel rods based on spent fuel models provided by Los Alamos National Laboratory and for a virgin high 240Pu-content fuel plate, as well as models of the IFEL and INL experiments implemented in the ray tracing tool. The beam position and height were validated against the INL ~60 keV americium data. Examples of alternate configurations of the optics or experimental set-up illustrate the future use of the simulation suite to guide the next IFEL experimental campaign.

Next generation hard X-ray/soft gamma-ray optic design and implementation

We discuss necessary improvements and further studies relevant to the design and eventual implementation of an accurately modeled multilayer coated X-ray optic operating in the hard X-ray/soft gamma-ray regime. The process improvements are substantiated through lessons learnt from NuSTAR.