Meysam Toozandehjani

Influence of rotational speed on mechanical properties of friction stir lap welded 6061-T6 Al alloy

The effect of rotational speed on macro and microstructures, hardness, lap shear performance and failure mode of friction stir lap welding on AA6061-T6 Al alloy with 5 mm in thickness was studied by field-emission scanning electron microscopy (FE-SEM). The results represent much closer hardness distribution in the upper and lower plates at the lowest rotational speed. It indicates the Fe-compounds in the fracture surface of the nugget zone by EDX.

Effect of Milling Time on the Microstructure, Physical and Mechanical Properties of Al-Al2O3 Nanocomposite Synthesized by Ball Milling and Powder Metallurgy

The effect of milling time on the morphology, microstructure, physical and mechanical properties of pure Al-5 wt % Al2O3 (Al-5Al2O3) has been investigated. Al-5Al2O3 nanocomposites were fabricated using ball milling in a powder metallurgy route. The increase in the milling time resulted in the homogenous dispersion of 5 wt % Al2O3 nanoparticles, the reduction of particle clustering, and the reduction of distances between the composite particles. The significant grain refining during milling was revealed which showed as a reduction of particle size resulting from longer milling time. X-Ray diffraction (XRD) analysis of the nanocomposite powders also showed that designated ball milling contributes to the crystalline refining and accumulation of internal stress due to induced severe plastic deformation of the particles. It can be argued that these morphological and microstructural variations of nanocomposite powders induced by designated ball milling time was found to contribute to an improvement in the density, densification, micro-hardness (HV), nano-hardness (HN), and Young’s modulus (E) of Al-5Al2O3 nanocomposites. HV, HN, and E values of nanocomposites were increased by ~48%, 46%, and 40%, after 12 h of milling, respectively.

On the correlation between microstructural evolution and ultrasonic properties: a review

The characterization and optimization of the microstructures of materials pertaining to material properties is a primitive necessity to ensure the performance and service life of the materials and components. In the demand of new characterization and evaluation techniques, nondestructive ultrasonic techniques have shown a good potential to characterize the microstructures and mechanical properties of a wide variety of materials. Measurements of ultrasonic parameters such as velocity and attenuation can provide information on the structural and microstructural variations of those materials that have undergone the heat-treatment procedure. In the current review, the correlation of ultrasonic parameters with microstructural features of ferrous and nonferrous metals such as steels, aluminum, and superalloys is investigated. It is proven that ultrasonic parameters are closely correlated to the microstructural evolutions which frequently occur during the heat-treatment procedures in practical situations. To conclude, the ultrasonic measurements contribute to a feasible and accurate characterization of the materials and evaluation of their microstructures and mechanical properties in a straightforward, reliable, and fast, nondestructive manner for practical applications.

Nanomechanical Behavior of Multi-Walled Carbon Nanotubes Particulate Reinforced Aluminum Nanocomposites Prepared by Ball Milling

The nanomechanical properties of carbon nanotubes particulate-reinforced aluminum matrix nanocomposites (Al-CNTs) have been characterized using nanoindentation. Bulk nanocomposite specimens containing 2 wt % multiwalled CNTs (MWCNTs) were synthesized by a combination of ball milling and powder metallurgy route. It has been tried to understand the correlation between microstructural evolution particularly carbon nanotubes (CNTs) dispersion during milling and mechanical properties of Al-2 wt % nanocomposites. Maximum enhancement of +23% and +44% has been found in Young’s modulus and hardness respectively, owing to well homogenous dispersion of CNTs within the aluminum matrix at longer milling time.

Microstructural evaluation of ball-milled nano Al2O3 particulate-reinforced aluminum matrix composite powders

Abstract A mechanically alloyed mixture of Al-1 wt.% nano-alumina (n-Al2O3) composite powders was produced using a planetary ball milling machine. Different milling times were applied to investigate the effect of milling time on the dispersion and microstructure of n-Al2O3 particulate reinforcement within the aluminum matrix. A good homogeneous dispersion of n-Al2O3 particulates was observed after 8 h of milling. Longer milling times had no significant effect on the dispersion and morphology of n-Al2O3 particulates within the aluminum matrix because a steady state had been reached.

Effect of Artificial Aging on the Microstructure and Mechanical Properties of Aluminum Alloy AA6061-T6

The properties of aluminum alloy AA6061-T6 after aging at 220°C for 0.5 – 8 h are studied by the methods of light and scanning electron microscopy and fractography. The mechanical characteristics of the alloy are determined by tensile tests.

Fabrication, Characterization, and Functionalization of Single-Walled Carbon Nanotube Conjugated with Tamoxifen and Its Anticancer Potential against Human Breast Cancer Cells

In this experiment, we aimed to fabricate SWCNT conjugated with tamoxifen and evaluated its anticancer potential against human breast cancer cells (MCF-7). The results showed that SWCNT was synthetized successfully using chemical vapor deposition (CVD) method. The results of Raman spectroscopy, SEM, and TEM analyses confirmed the synthesis of highly pure SWCNT. The functionalization of SWCNT was performed by oxidizing of SWCNT, attachment of polyethylene glycol (PEG) to oxidized SWCNT, and attachment of azelaic acid to the polyethylene glycol group. As a result, the SWCNT with free functional carboxylic acid and hydroxyl groups (SWCNT-PEG) was developed. The SWCNT-PEG was then conjugated with tamoxifen (SWCNT-PEG-TAM). The FT-IR together with NMR results confirmed the conjugation of tamoxifen to functionalized SWCNT (SWCNT-PEG-TAM). The cytotoxic concentrations (CC50) of SWCNT-PEG, tamoxifen, and SWCNT-PEG-TAM were >100, , and μg/ml, respectively. Linking tamoxifen to functionalized SWCNT enhanced the cytotoxic action of tamoxifen against breast cancer cells up to 2.3 times. The results of the morphological examination and caspase-3 activity confirmed the higher cytotoxic action of SWCNT-PEG-TAM as compared to free tamoxifen. The results obtained in this study indicated that this delivery system enhanced the therapeutic effects and anticancer potential of tamoxifen against human breast cancer cells.

Investigation of the Structure and Hardness of Quenched Sintered Materials Produced from Iron-Base Alloyed Powders (Astaloy E)

The effect of heat treatment on the microstructure, hardness and density of sintered (1129°C, 45 min) specimens of iron-base powder alloys containing 0.8 – 2.5% C, 2% Cu and additives of chromium- and molybdenum-alloyed Astaloy E iron powder is studied.