Rudy Soenoko

Morphology, Structure, and Mechanical Properties of Natural Cellulose Fiber from Mendong Grass (Fimbristylis globulosa)

This study was to investigate the morphology, structure, and chemical properties of the Mendong fibers extracted from Mendong grass (Fimbristylis globulosa) in the form of raw and treated fiber by alkali-included chemical content and functional group and to evaluate the strength and properties of Mendong fibers compared with other natural fibers. These studies explore the chemical properties of the fiber including fiber composition and functional group by FTIR, mechanical properties of fiber, and the structural and morphological analysis of the fiber using SEM and XRD. The results showed that the chemical contents of Mendong fibers were 72.14% cellulose, 20.2% hemicellulose, 3.44% lignin, 4.2% extractive, and moisture of 4.2%–5.2%. Mechanical properties of the fiber were a strong character with tensile strength of 452 MPa, and modulus of 17 GPa. The structural properties of Mendong fiber such as crystallinity, crystalline index, microfibril angle, and crystalline size were 70.17% and 58.6%, 22.9°, and 14.3 nm, respectively. This fiber has competitive advantages compared with other natural fibers and can be developed further as a potential reinforcement of polymer matrix composites.

Effect of Alkali Treatment on Crystalline Structure of Cellulose Fiber from Mendong (Fimbristylis globulosa) Straw

The research aim is to investigate the effect of alkali treatment on the crystalline structure of Mendong fiber. The experiment was conducted by immerse fibers in 100 ml NaOH solution by a concentration of 2.5%, 5%, 7.5%, and 10% for 2 hours at the room temperature. The specimens were characterized by X-ray diffraction method. The morphology of fiber treated by alkali was observed by Scanning Electron Microscope. The result shows that the crystalline structure of cellulose in Mendong fiber was changed in alkali treatment. It was found that both the degree of crystallinity and crystalline index of Mendong fiber was increased until alkali treatment concentration of 7.5%.

Improvement of Interfacial Shear Strength of Mendong Fiber (Fimbristylis globulosa) Reinforced Epoxy Composite Using the AC Electric Fields

The effects of the AC electric field treatment on the interfacial shear strength of mendong fiber-reinforced epoxy composites were investigated. For this purpose, the epoxy (DGEBA) with a cycloaliphatic amine curing agent was treated by the AC electric field during the curing process. The heat generated during the epoxy polymerization process was monitored. Structure of the epoxy was studied by X-ray diffraction, Fourier transform infrared spectroscopy (FTIR), and Scanning Electron Microscope, respectively. The interfacial shear strength (IFSS) was also measured using a single fiber pull-out test. XRD analyzes indicated that the treatment of AC electric fields was able to form a crystalline phase of epoxy. IFSS of the mendong fiber-reinforced epoxy composites was optimum increased by 38% in the AC electric fields treatment of 750 V/cm.

Bee Wax Propolis Extract as Eco-Friendly Corrosion Inhibitors for 304SS in Sulfuric Acid

The inhibition properties of bee wax propolis (BWP) extract on the 304SS in 0.5 M sulfuric acid were conducted using potentiodynamic polarization, EIS, and XRD. Quercetin (2-(3.4-dihydroxy phenyl)-3.5.7-trihydroxy-4H-chromen-4-one) was identified as the main compound in the BWP extract based on FTIR and HPLC analysis. The results showed that the inhibitor could retard the corrosion rate of 304SS in 0.5 M sulfuric acid which reached 97.29% and 91.42% at 2000 ppm based on potentiodynamic polarization and EIS measurement, respectively. The inhibition efficiency decreased with increasing temperature. The inhibition mechanism of BWP extract on the 304SS was physisorption and obeyed Temkin adsorption isotherm equation. The thin protective layer on the 304SS surface was confirmed by XRD.

Mechanical properties of untreated and alkaline treated fibers from zalacca midrib wastes

The environmental concern has been raised due to the abundance of waste from synthetic materials which cannot be biodegraded after their life-time. It provides opportunity to exploit natural resources which are neglected. For example, midrib wastes from zalacca plants after cutting are able to utilize as composite reinforcement. The aim of this research was to characterize the mechanical properties of zalacca midrib fibers. As other ones, zalacca midrib fibers consisted of cellulose, hemicellulose and lignin, which their compositions were 42.54, 34.35 and 28.01 % respectively. To raise their cellulose content, the zalacca fibers were alkaline treated by immersion in the sodium hydroxide for 2 hours and rinsing in the distilled water. The concentration of sodium hydroxide was varied 1 and 5%. To investigate the influence of alkaline treatment, the mechanical testing and morphological analysis was performed. The tensile testing was done to obtain ultimate strength, elastic modulus and strain to fracture. Th...

Experimental Study of the Cross Flow Turbine

The experimental study was intended to investigate characteristics of the cross flow turbine based to the three models designed on the same runner diameter with different runner length of each. The Flow rates were measured by magnetic flow meter, the forces were detected by using spring balance and turbine speeds were detected by tachometer. The performance characteristics are shown by the relation of Power and efficiency versus jet entry arc, as well as the relation of Power and efficiency versus ratio between diameter and width of runner. The study indicated that the efficiency of the models were slightly difference, the highest efficiency indicated by the turbine with the ratio between length of runner and the diameter of the runner was 2; It was corresponding to the 75 degree entry arc.

Effect of Low Temperature Sintering on the Porosity and Microstructure of Porous Zeolite Ceramic

Manufacturing a porous ceramic specimen from natural zeolite materials mined in Malang, Indonesia was conducted by using a low temperature sintering. In this study, a porous ceramic property with rectangular shaped and prism shaped fillets at each end were sintered at 800-900°C and finally were investigated. Density and porosity measurements were performed using Archimedes method. The microstructure photos were used to measure the neck diameter and the contact angle between the two grains particles and two-dimensional porosity. The result of the zeolite ceramic measurement shows that the higher the sintering temperature the higher the density value and the smaller the open porosity. While from the microstructure photo it is shown that the neck diameter was larger the contact angle was wider. This phenomenon was happened because of the flux diffusion on the grain boundaries. This diffusion flow condition would influence the specimen surface, volume and grain boundary so that the porous ceramic density increases.

Optimizing Multi Response Green Machining using Taguchi Method Based on Grey Relational Analysis

This paper presents an optimization of multi response green machining of aluminum 6061 valve. The research is started with study literature and early survey to identify various factors that may likely influence in the green machining.The next step is investigating and collecting experiment data of the control factors (working in 3 levels) for depth of cut, feeding, and cutting speed factor on two responses; power consumption and surface roughness (Ra). The data were evaluated using Taguchi method based on grey relational anaylisis. Statistic tools coupled together with Taguchi design to process the output of the experiment. Finally, the research has successfully to deliver knowledges of the cutting speed and feeding factors have a dominant influence in power consumption and surface roughness of the green machining process

THE POSITION OF THE JOINTS WITH ANGLE OF 90° AT FRICTION STIR WELDING (FSW)

This research was use aluminum 6061 with 150 mm length, 50 mm wide, and 10 mm thick. The probe was made from EMS 45 simple design. Three variations used of feedrate speed is 10 mm/min, 15 mm/min, and 30 mm/min. Spindle rotation constantly set 2000 rpm, the heat generated was recorded. Corner-Butt (C-B)joint determined, the lowest heat generated from 2200C3200C and the tensile test was60 MPa. The highest tensile testwas 163 MPa, achieved by Corner-butt 45 (CB 45) joint on 10 mm/min feedrate speed. It was verified by the heat temperature from 3000C-4200C and clarified by its micro and macrostructure.

The Influence of Chemical Treatments on Cantala Fiber Properties and Interfacial Bonding of Cantala Fiber/Recycled High Density Polyethylene (rHDPE)

ABSTRACT The influence of chemical treatments on the properties of cantala fiber as well as on the quality of the interfacial bonding of cantala fiber/rHDPE was investigated. The fibers were treated with alkali, silane, and a combination of both. The results showed that the loss of hemicellulose and lignin after the alkali treatment, and the presence of a silane layer on the fiber surface after the silane or alkali-silane treatment, improved the thermal stability, surface energy, and IFSS. The highest surface energy of 45.37 mN/m was obtained during the alkali treatment (NF12). The alkali-silane treatment with 0.75% wt of silane (NSF075) gave the highest thermal stability and IFSS value.