Sanjay G. Sapate

Evaluation of Microstructure, Mechanical Properties and Corrosion Resistance of Friction Stir-Welded Aluminum and Magnesium Dissimilar Alloys

Microstructure, mechanical properties and corrosion resistance of dissimilar friction stir-welded aluminum and magnesium alloys were investigated by applying three different rotational speeds at two different travel speeds. Sound joints were obtained in all the conditions. The microstructure was examined by an optical and scanning electron microscope, whereas localized chemical information was studied by energy-dispersive spectroscopy. Stir zone microstructure showed mixed bands of Al and Mg with coarse and fine equiaxed grains. Grain size of stir zone reduced compared to base metals, indicated by dynamic recrystallization. More Al patches were observed in the stir zone as rotational speed increased. X-ray diffraction showed the presence of intermetallics in the stir zone. Higher tensile strength and hardness were obtained at a high rotational speed corresponding to low travel speed. Tensile fractured surface indicated brittle nature of joints. Dissimilar friction stir weld joints showed different behaviors in different corrosive environments, and better corrosion resistance was observed at a high rotational speed corresponding to low travel speed (FW3) in a sulfuric and chloride environments. Increasing travel speed did not significantly affect on microstructure, mechanical properties and corrosion resistance as much as the rotational speed.

ABRASIVE WEAR BEHAVIOUR OF COPPER-SiC AND COPPER-SiO2 COMPOSITES

The present paper reports abrasive wear behaviour of copper matrix composites reinforced with silicon carbide and silica particles. Copper – SiC (12%) and Copper-SiO2 (9%) composites were prepared by powder metallurgical technique. Metallography, image analysis and hardness studies were carried out on copper composites. The abrasive wear experiments were carried out using pin on disc apparatus. The effect of sliding distance and load was studied on Copper – SiC (12%) and Copper-SiO2 (9%) composites. The abrasive wear volume loss increased with sliding distance in both the composites although the magnitude of increase was different in each case. Copper – SiC (12%) composites exhibited relatively better abrasion resistance as compared to and Copper-SiO2 (9%) composites. The abraded surfaces were observed under scanning electron microscope to study the morphology of abraded surfaces and operating wear mechanism. The analysis of wear debris particles was also carried out to substantiate the findings of the investigation.

Effect of Tribo-Oxidation on Friction and Wear Behaviour of HVOF Sprayed WC–10Co–4Cr Coating

The effect of tribo-chemical reactions under varying sliding speed and load conditions on the friction and abrasive wear response of high-velocity oxy-fuel-sprayed WC–10Co–4Cr coating was studied. The abrasive wear rate and friction coefficient decreased with the increase in sliding speed while friction coefficient displayed increasing trend with increase in load. The decrease in friction coefficient and wear rate was attributed to formation of tribo-oxides and surface films with good lubricating properties. Severity of abrasive wear increased with increasing load which was associated with transition in wear mechanisms from plastic deformation and fatigue to delamination cracking, intergranular fracture and splat fracture. Increase in friction coefficient with load irrespective of sliding speed was due to increasing contribution of fracture-assisted mechanical wear as compared to oxidative wear. The nature, composition and properties of tribo-films imparted crucial role to influencing friction and abrasive wear of WC–10Co–4Cr coating.

Influence of Surface Treatment of High Carbon Steel on the Reciprocating Wear in Comparison With the 316 Stainless Steel

Diffusion treatments such as chromising and aluminising of high carbon steel results in the formation of Cr and Al rich layers on the surface. These layers will be responsible for formation of protective Cr2 O3 and Al2 O3 scale on exposure to corrosive environment. In view of extensive application of 316 Stainless Steel in biomedical engineering, present work is undertaken to examine the influence of diffusion treatment of high carbon steel on the reciprocating wear in Hank’s solution and to compare the same behavior with that of 316 SS. In order to achieve the above mentioned objectives, the wear rates of 316 SS, 304 SS, high carbon steel in aluminised and chromised condition have been evaluated. Though the general characteristics of the wear behavior, such as higher wear rate at higher load and at higher reciprocating speed, for all the materials are similar, aluminised and chromised high carbon steel exhibited best wear resistance especially at high and intermediate load. In simulated body fluid condition, 316 SS exhibited two different material removal mechanisms. In the first case, which is observed at higher load, material loss is by nucleation and propagation of crack. In the second mechanism which is prevalent at low and intermediate load, wear takes place by deterioration of composite layer formed on the surface by mixing the corrosion product and the substrate. Consequently it is noted that wear rate decreases with increase of hardness at higher load. At intermediate and at low load wear rate is less dependent of hardness.Copyright

Effect of composition and microstructure on slurry abrasion response of hardfaced martensitic stainless steel

Hardfaced martensitic stainless steel alloy was deposited on mild steel substrate by flux cored arc welding method. The slurry abrasion studies of weld-deposited hardfaced steel were performed using slurry abrasion test rig with 250–300 μm silica sand particles. The effect of weld compositional gradation on the abrasive wear resistance of hardfaced stainless steel at a distance of 0.6, 1.2, 2.4, 3.0 and 3.6 mm from the top surface was studied. The observed abrasion rates were rationalized in terms of mass loss, hardness and distance from the top surface i.e. diluted surfaces beneath the top surface. The abrasive wear mass loss increased with increasing distance beneath the top surface, which was attributed to the coarsening and morphology change in martensite phase. The results of the present work indicated change in morphology of martensite with increase in the distance beneath the top surface. The operating abrasive wear mechanisms involved ploughing, microcutting and indentation.

Scaling Laws of Wear by Slurry Abrasion of Mild Steel

Wear by slurry abrasion is very expansive problem that must be taken into consideration while selecting the material for the transportation of slurry through pipeline. Abrasive wear generally occurs when abrasive slurries come in contact with the industrial engineering components or slurry transporting pipes. The abrasive particles carried by slurries eventually remove the material from the encountering surfaces which results in the early failure of the component in service. In present investigation an attempt is made to study the effect of load, slurry concentration, sliding distance on the abrasive wear behaviour of mild steel. The slurry abrasion experiments were carried out using slurry abrasion test apparatus with silica sand slurry. The findings of the present investigation indicate that slurry abrasion volume increased with slurry concentration, load and sliding distance, although the magnitude of increase was different in each case. The SEM observation of worn out surfaces revealed micro ploughing and micro cutting as wear mechanisms.