Solomon I. Woods

Absolute cryogenic radiometer and solid-state trap detectors for IR power scales down to 1 pW with 0.1% uncertainty

Commercially available absolute cryogenic radiometers (ACRs) have combined uncertainties that grow rapidly above 1% (k = 1) at power levels below 10 nW. There are solid state detectors, however, used in sensors and radiometers that cannot be calibrated at levels as high as 10 nW because they begin to saturate. For this reason new detector-based standards are being developed to provide the low-background infrared calibration community with absolute traceability to powers down to 1 pW with ~0.1% (k = 1) combined uncertainty. The scale will be established using an ACR with a combined uncertainty of the order of 1 fW and a trap detector based on arsenic-doped silicon blocked impurity band devices with similar noise floor performance.

Planar electrical-substitution carbon nanotube cryogenic radiometer*

We have developed a fully-lithographic electrical-substitution planar bolometric-radiometer (PBR) that employs multiwall vertically-aligned carbon nanotubes (VACNT) as the absorber and thermistor, micro-machined Si as the weak thermal link and thin-film Mo as the electrical heater. The near-unity absorption of the VACNT over a broad wavelength range permits a planar geometry, compatible with lithographic fabrication. We present performance results on a PBR with an absorption of 0.999 35 at 1550 nm, a thermal conductance of 456 µW K−1 at 4 K and a time constant (1/e) of 7.7 ms. A single measurement of approximately 100 µW optical power at 1550 nm achieved in less than 100 s yields an expanded uncertainty of 0.14% (k = 2). We also observe an elevated superconducting transition temperature of 3.884 K for the Mo heater, which opens the possibility of future devices incorporating more sensitive thermistors and superconducting thin-film wiring.

Calibration of IR test chambers with the missile defense transfer radiometer

The Missile Defense Transfer Radiometer (MDXR) is designed to calibrate infrared collimated and flood sources over the fW/cm2 to W/cm2 power range from 3 μm to 28μ m in wavelength. The MDXR operates in three different modes: as a filter radiometer, a Fourier-transform spectrometer (FTS)-based spectroradiometer, and as an absolute cryogenic radiometer (ACR). Since 2010, the MDXR has made measurements of the collimated infrared irradiance at the output port of seven different infrared test chambers at several facilities. We present a selection of results from these calibration efforts compared to signal predictions from the respective chamber models for the three different MDXR calibration modes. We also compare the results to previous measurements made of the same chambers with a legacy transfer radiometer, the NIST BXR. In general, the results are found to agree within their combined uncertainties, with the MDXR having 30 % lower uncertainty and greater spectral coverage.

Cryogenic Fourier transform infrared spectrometer from 4 to 20 micrometers

We describe the design and performance of a cryogenic Fourier transform spectrometer (Cryo-FTS) operating at a temperature of approximately 15 K. The instrument is based on a porch-swing scanning mirror design with active alignment stabilization using a fiber-optic coupled diode laser and voice-coil actuator mechanism. It has a KBr beamsplitter and has been integrated into an infrared radiometer containing a calibrated Si:As blocked impurity band (BIB) detector. Due to its low operating temperature, the spectrometer exhibits very small thermal background signal and low drift. Data from tests of basic spectrometer function, such as modulation efficiency, scan jitter, spectral range, and spectral resolution are presented. We also present results from measurements of faint point-like sources in a low background environment, including background, signal offset and gain, and spectral noise equivalent power, and discuss the possible use of the instrument for spectral characterization of ground-based infrared astronomy calibration sources. The Cryo-FTS is presently limited to wavelengths below 25 micrometers but can be in principle extended to longer wavelengths with changes in beamsplitter and detector.

Picowatt infrared power measurement using an absolute cryogenic radiometer

We report on initial measurements of the low-temperature thermal properties of a device that is similar to the experimental apparatus used for absolute cryogenic radiometry (ACR) within the Low Background Infrared Radiometry (LBIR) facility at NIST. The device consists of a receiver cavity mechanically and thermally connected to a temperature-controlled stage through a thin-walled polyimide tube which serves as a weak thermal link. In order to evaluate the functionality of the device for use in a cryogenic radiometer, we measured the thermal resistance and thermal time constant of the system within the temperature range of 1.8 - 4.4 K. The measured thermal resistance and thermal time constant at 1.883 K were 2400 ± 500 (K/mW) and 24 ± 6 (s). This value for the thermal resistance should result in about an order-of-magnitude increase in radiometer sensitivity compared with the present ACR within LBIR. Although the sensitivity should increase by about an order-of-magnitude, the measured time constant is nearly unchanged with respect to previous ACRs within LBIR, due to the reduced dimensions of the receiver cavity. Finally, the thermal conductivity inferred from the measured thermal resistance and geometrical parameters was computed, with an average value of 0.015 (W/m-K), and compared with other measurements of polyimide from the literature.

Infrared transfer radiometer for broadband and spectral calibration of space chambers

The Low-Background Infrared (LBIR) facility at NIST has recently completed construction of an infrared transfer radiometer with an integrated cryogenic Fourier transform spectrometer (Cryo-FTS). This mobile system can be deployed to customer sites for broadband and spectral calibrations of space chambers and low-background HWIL testbeds. The Missile Defense Transfer Radiometer (MDXR) has many of the capabilities of a complete IR calibration facility and will replace our existing filter-based transfer radiometer (BXR) as the NIST standard detector deployed to MDA facilities. The MDXR features numerous improvements over the BXR, including: a cryogenic Fourier transform spectrometer, an on-board absolute cryogenic radiometer (ACR), an internal blackbody reference, and an integrated collimator. The Cryo-FTS can be used to measure high resolution spectra from 4 to 20 micrometers, using a Si:As blocked-impurity-band (BIB) detector. The on-board ACR can be used for self-calibration of the MDXR BIB as well as for absolute measurements of infrared sources. A set of filter wheels and a rotating polarizer within the MDXR allow for filter-based and polarization-sensitive measurements. The optical design of the MDXR makes both radiance and irradiance measurements possible and enables calibration of both divergent and collimated sources. Details of the various MDXR components will be presented as well as initial testing data on their performance.

Calibration of ultra-low infrared power at NIST

The Low Background Infrared (LBIR) facility has developed and tested the components of a new detector for calibration of infrared greater than 1 pW, with 0.1 % uncertainty. Calibration of such low powers could be valuable for the quantitative study of weak astronomical sources in the infrared. The pW-ACR is an absolute cryogenic radiometer (ACR) employing a high resolution transition edge sensor (TES) thermometer, ultra-weak thermal link and miniaturized receiver to achieve a noise level of around 1 fW at a temperature of 2 K. The novel thermometer employs the superconducting transition of a tin (Sn) core and has demonstrated a temperature noise floor less than 3 nK/Hz1/2. Using an applied magnetic field from an integrated solenoid to suppress the Sn transition temperature, the operating temperature of the thermometer can be tuned to any temperature below 3.6 K. The conical receiver is coated on the inside with infrared-absorbing paint and has a demonstrated absorptivity of 99.94 % at 10.6 μm. The thermal link is made from a thin-walled polyimide tube and has exhibited very low thermal conductance near 2x10-7 W/K. In tests with a heater mounted on the receiver, the receiver/thermal-link assembly demonstrated a thermal time constant of about 15 s. Based on these experimental results, it is estimated that an ACR containing these components can achieve noise levels below 1 fW, and the design of a radiometer merging the new thermometer, receiver and thermal link will be discussed.

Broadband emissivity calibration of highly reflective samples at cryogenic temperatures

We have developed a technique for measuring the broadband optical emissivity of high reflectivity samples at cryogenic temperatures. This measurement method employs a primary standard optical detector with high absorptance from visible wavelengths to beyond 200 µm. Background subtraction and quantification allow determination of the emissivity with total absolute uncertainty (k = 1) between approximately 0.0002 and 0.002 (for emissivities between 0.0035 and 0.092) over the temperature range from 80 K to 300 K. Using the irradiance data at the detector, precise measurements of the experimental geometry and diffraction calculations, the optical power emitted by the sample can be determined. Contact thermometry measurements for the sample can then be used to find its emissivity. The emissivity calibration technique is demonstrated for large plate samples made from polished stainless steel and is also extended to calculate the separate emissivities of multiple distinct regions on a more complex sample assembly.

Characterization of the optical properties of an infrared blocked impurity band detector

Si:As blocked impurity band detectors have been partially deprocessed and measured by Fourier transform spectroscopy to determine their transmittance and reflectance at cryogenic temperatures over the wavelength range 2 μm to 40 μm. A method is presented by which the propagation constants can be extracted from an inversion of the transmittance and reflectance data. The effective propagation constants for the active layer from 2 μm to 20 μm were calculated as well as the absorption cross section of arsenic in silicon, which agrees well with previous results from the literature. The infrared absorptance of the full detector was determined, and the analytical method also provides an estimate of absorption in the active layer alone. Infrared absorptance of the active layer is compared to the quantum yield measured by photoelectric means on similar detectors. The optical methods outlined here, in conjunction with standard electronic measurements, could be used to predict the performance of such detectors from measurements of the blanket films from which they are to be fabricated.

Infrared Absolute Calibrations Down to 10 fW in Low-Temperature Environments at NIST

The Low Background Infrared (LBIR) facility at the National Institute of Standards and Technology (NIST) is responsible for absolute IR radiometric calibrations (SI traceable) in low-background temperature (below 80 K) environments. IR radiometric test hardware that needs to be operated in cryogenic environments is calibrated in cryogenic vacuum chambers maintained by the facility to create environments that simulate the low-temperature background of space. Transfer radiometers have also been developed to calibrate IR radiometric test hardware this is too large to ship to NIST from their own IR test facilities. The first generation transfer radiometer, the BXR, is a filter-based radiometer that uses an As-doped Si Blocked Impurity Band detector, and can calibrate IR test chambers to a total uncertainty of less than 3 % (1 σ ) at powers as low as to 10-14 W/cm2. The BXR has evaluated 9 chambers and the performance of a subset of these chambers will be discussed to a limited extent to demonstrate the need for calibrating IR test chambers. The second generation transfer radiometer, the MDXR, and new primary standards allowing absolute calibrations as low as 10-15 W/cm2 are in the final stages of development. The MDXR will have all the functionality of the BXR and it will have a cryogenic Fourier transform spectrometer (FTS) for high resolution spectral capability. Performance specifications and test results from development activity on the new primary standards will be discussed.